Download or read book Trace Analytical Techniques for Nuclear Forensics written by and published by . This book was released on 1999 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Over the history of the Savannah River Site, the Savannah River Technology Center (SRTC) has developed high sensitivity analytical capabilities in support of the Site's Environmental Monitoring Program and nuclear material protection process. Many of these techniques are applicable to the developing need for nuclear forensic analysis capabilities. Radiological and critically control procedures are in place at the SRTC, as well as clean room practices, to minimize the potential for a radiological evidentiary sample to contaminate personnel and the facility, as well as to minimize contaminating the sample thus rendering it useless by law enforcement agencies. Some of the trace analytical techniques available at the SRTC include ultra-low-level gamma and alpha spectrometry, high-sensitivity thermal ionization mass spectrometry, time-of-flight secondary ion mass spectrometry and trace organic analyses. These techniques have been tested during a planned domestic smuggling exercise and in the analysis of an unknown sample. In the event of an interdiction involving the illegal use or movement of radioactive material by U.S. law enforcement agencies (local, state or federal) forensic analyses will be used in developing and building a legal case against the perpetrators. The Savannah River Technology Center (SRTC) at the U.S. Department of Energy's Savannah River Site, a former nuclear production site currently conducting nuclear material stabilization missions, located in Aiken South Carolina, has a long history of performing trace analytical analyses for environmental monitoring. Many of these techniques are also applicable to nuclear forensic analyses. A summary of the trace analytical techniques used at the SRTC, which are applicable to Nuclear Forensics, is presented in this paper. Contamination control, of facilities and personnel involved in the analytical analyses, as well as preventing contamination of the sample, is a unique challenge for nuclear forensic analyses. A discussion of sample handling and contamination control procedures is included in this paper. Some of the applicable analytical techniques available at the SRTC for nuclear forensic analyses include: ultra-low-level gamma and alpha spectroscopy, high-sensitivity thermal-ionization mass spectrometry (TIMS), time-of-flight secondary ion mass spectrometry (TOF-SIMS), and trace organic analyses. Results from analyses of special nuclear material (SNM) standards, materials from nuclear smuggling exercises, and materials of unknown origin will be presented.
Download or read book Analytical Methods for Nonproliferation written by Edward C. Morse and published by Springer. This book was released on 2016-04-04 with total page 254 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is intended to be used as a textbook and research reference for the field of nuclear nonproliferation. The book is primarily technical and focussed on methods of detecting clandestine nuclear material that might be illicitly transported. The book also touches on nuclear forensics, i.e. methods for identification, attribution, and establishment of transport pathways for illicit nuclear material. Also covered are topics of methods used for arms control and treaty verification, and an assessment of technologies under development for all of the above. A description of the government and international agencies involved in nuclear terrorism prevention, nuclear safeguards, and arms control is also included.
Download or read book Nuclear Forensics of Special Nuclear Material at Los Alamos written by and published by . This book was released on 2010 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Nuclear forensics of special nuclear materials is a highly specialized field because there are few analytical laboratories in the world that can safely handle nuclear materials, perform high accuracy and precision analysis using validated analytical methods. The goal of nuclear forensics is to establish an unambiguous link between illicitly trafficked nuclear material and its origin. The Los Alamos National Laboratory Nuclear Materials Signatures Program has implemented a graded 'conduct of operations' type approach for determining the unique nuclear, chemical, and physical signatures needed to identify the manufacturing process, intended use, and origin of interdicted nuclear material. In our approach an analysis flow path was developed for determining key signatures necessary for attributing unknown materials to a source. This analysis flow path included both destructive (i.e., alpha spectrometry, ICP-MS, ICP-AES, TIMS, particle size distribution, density and particle fractionation) and non-destructive (i.e., gamma-ray spectrometry, optical microscopy, SEM, XRD, and x-ray fluorescence) characterization techniques. Analytical techniques and results from three recent cases characterized by this analysis flow path along with an evaluation of the usefulness of this approach will be discussed in this paper.
Download or read book Nuclear Forensic Analysis written by Kenton J. Moody and published by CRC Press. This book was released on 2005-02-28 with total page 510 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides a primary reference source for nuclear forensic science, including the vastly disciplinary nature of the overall endeavor for questioned weapons of mass-destruction specimens. Nothing like this exists even in the classified material. For the first time, the fundamental principles of radioforensic analysis, all pertinent protocols and procedures, computer modeling development, interpretational insights, and attribution considerations are consolidated into one convenient source. The principles and techniques so developed are then demonstrated and discussed in their applications to real-world investigations and casework conducted over the past several years.
Download or read book Nuclear Analytical Techniques in Medicine written by R. Cesareo and published by Elsevier. This book was released on 2011-09-22 with total page 415 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book will acquaint the interested physician or physicist with the fundamental principles and the instrumentation relevant to analytical techniques based on atomic and nuclear physics, as well as present and future biomedical applications. Besides providing a theoretical description of the physical phenomena, a large part of the book is devoted to applications in the medical and biological field, particularly in haematology, forensic medicine and environmental science.Analysis of the elemental composition of human tissues and cells and in particular trace elements has attracted increasing interest over the last few years, due to the increase in knowledge on the role of some elements and the possible correlations between abnormal concentrations of one or more trace elements and pathological conditions. This has stimulated the development of analytical techniques which allow the detection of trace elements simultaneously and at very low concentrations. Particularly in methods involving nuclear principles or nuclear apparatus, many techniques have been largely and successfully developed in recent years and applied in the medical field. This volume reviews methods such as the possibility of carrying out rapid multi-element analysis of trace elements on biomedical samples, in vitro and in vivo, by XRF-analysis; the ability of the PIXE-microprobe to analyze in detail and to map trace elements in fragments of biomedical samples or inside the cells; the potentiality of in vivo nuclear activation analysis for diagnostic purposes. Finally, techniques are described such as radiation scattering (elastic and inelastic scattering) and attenuation measurements which will undoubtedly see great development in the immediate future.
Download or read book Methods for Environmental Trace Analysis written by John R. Dean and published by John Wiley and Sons. This book was released on 2003-04-18 with total page 298 pages. Available in PDF, EPUB and Kindle. Book excerpt: Table of contents
Download or read book Handbook of Trace Analysis written by Irena Baranowska and published by Springer. This book was released on 2015-08-13 with total page 458 pages. Available in PDF, EPUB and Kindle. Book excerpt: This handbook is unique in its comprehensive coverage of the subject and focus on practical applications in diverse fields. It includes methods for sample preparation, the role of certified reference materials, calibration methods and statistical evaluation of the results. Problems concerning inorganic and bioinorganic speciation analysis, as well as special aspects such as trace analysis of noble metals, radionuclides and volatile organic compounds are also discussed. A significant part of the content presents applications of methods and procedures in medicine (metabolomics and therapeutic drug monitoring); pharmacy (the analysis of contaminants in drugs); studies of environmental samples; food samples and forensic analytics – essential examples that will also facilitate problem solving in related areas.
Download or read book Nuclear Forensic Analysis Second Edition written by Kenton J. Moody and published by CRC Press. This book was released on 2014-12-10 with total page 526 pages. Available in PDF, EPUB and Kindle. Book excerpt: Now in its second edition, Nuclear Forensic Analysis provides a multidisciplinary reference for forensic scientists, analytical and nuclear chemists, and nuclear physicists in one convenient source. The authors focus particularly on the chemical, physical, and nuclear aspects associated with the production or interrogation of a radioactive sample. They consolidate fundamental principles of nuclear forensic analysis, all pertinent protocols and procedures, computer modeling development, interpretational insights, and attribution considerations. The principles and techniques detailed are then demonstrated and discussed in their applications to real-world investigations and casework conducted over the past several years. Highlights of the Second Edition include: A new section on sample analysis considerations and interpretation following a post-detonation nuclear forensic collection New case studies, including the most wide-ranging and multidisciplinary nuclear forensic investigation conducted by Lawrence Livermore National Laboratory to date Expanded treatments of radiologic dispersal devices (RDDs) and statistical analysis methodologies The material is presented with minimal mathematical formality, using consistent terminology with limited jargon, making it a reliable, accessible reference. The broad-based coverage provides important insight into the multifaceted changes facing this recently developed science.
Download or read book Establishing a Nuclear Forensic Capability Application of Analytical Techniques written by International Atomic Energy Agency and published by . This book was released on 2023-06-15 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nuclear forensics supports national nuclear security measures and criminal investigations by providing information on the identity, origin and history of nuclear or other radioactive material found out of regulatory control. This publication provides information for States on the use of nuclear forensics in response to criminal or other unauthorized acts involving nuclear or other radioactive material, based on the guidance provided in IAEA Nuclear Security Series No. 2-G (Rev. 1), Nuclear Forensics in Support of Investigations. It is intended for technical and non-technical personnel responsible for developing nuclear forensic analytical capabilities within the context of a broader national nuclear forensic programme stemming from national legislation. It provides technical information that describes the application of specific methods, analytical techniques and technical expertise used for nuclear forensic analysis in support of investigations of criminal or other unauthorized acts involving nuclear or other radioactive material.
Download or read book Analytical Applications of Nuclear Techniques written by and published by IAEA. This book was released on 2004 with total page 224 pages. Available in PDF, EPUB and Kindle. Book excerpt: The IAEA has compiled this overview of current applications of nuclear analytical techniques (NATs). The contributions included in this book describe a variety of nuclear techniques and applications, such as those in the fields of environment and health, industrial processes, non-destructive testing, forensic and archaeological investigations, cosmochemistry and method validation. The techniques covered range from classical instrumental neutron activation analysis (INAA), its radiochemical derivative RNAA, in-beam methods such as prompt y neutron activation analysis (PGNAA) and accelerator mass spectrometry (AMS), to X ray fluorescence (XRF) and proton induced X ray emission (PIXE) spectroscopy. Isotopic techniques to investigate element behaviour in biology and medicine, and also to validate other non-nuclear analytical techniques, are described. Destructive and non-destructiveapproaches are presented, along with their use to investigate very small and very large samples, archaeological samples and extraterrestrial samples. Several nuclear analytical applications in industry are described that have considerable socioeconomic impact wherever they can be implemented.
Download or read book Nuclear Analytical Methods in the Life Sciences written by Rolf Zeisler and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 750 pages. Available in PDF, EPUB and Kindle. Book excerpt: The book is very readable and serves as an excellent reference source for research in the fields of analytical methodology and application for a wide range of biological, medical, and environmental samples ... a very good compilation of technical papers.-Analyst.
Download or read book Nuclear Analytical Techniques for Metallomics and Metalloproteomics written by Chunying Chen and published by Royal Society of Chemistry. This book was released on 2010 with total page 428 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nuclear analytical techniques have many advantages over other techniques, such as high sensitivity and precision. They couple powerful selective separation with sensitive element-specific detection. The uses of metalloproteomics studies are restricted to the fields of analytical and nuclear chemistry. They also have great potential to elucidate the origins of certain diseases and assist in their diagnosis and treatment via the development of new drugs. Nuclear Analytical Techniques for Metallomics and Metalloproteomics provides readers with a comprehensive view of this relatively new and exciting area of bioanalytical and inorganic chemistry. It contains contributions from experts in disciplines as diverse as analytical chemistry, nuclear chemistry, environmental science, molecular biology and medicinal chemistry. Various nuclear analytical techniques are covered including neutron activation analysis, X-ray fluorescence, isotope tracer, M÷ssbauer spectrometry, X-ray absorption spectrometry, and neutron scattering and diffraction. They provide useful information both for chemical speciation analysis and structural characterization of metalloproteins and metals in biological systems. Consequently, the book is not only relevant for chemists involved in nuclear techniques and speciation, but also environmental, nutritional and clinical researchers and drug developers. The book includes many illustrations, tables and documents to support the coverage of the latest developments. It also offers a well-organized bibliography to facilitate further reading.
Download or read book Nuclear Forensic Analysis written by Kenton J. Moody and published by CRC Press. This book was released on 2014-12-10 with total page 516 pages. Available in PDF, EPUB and Kindle. Book excerpt: Now in its second edition, Nuclear Forensic Analysis provides a multidisciplinary reference for forensic scientists, analytical and nuclear chemists, and nuclear physicists in one convenient source. The authors focus particularly on the chemical, physical, and nuclear aspects associated with the production or interrogation of a radioactive sample.
Download or read book India United States Cooperation on Global Security written by Committee on India-United States Cooperation on Global Security: Technical Aspects of Civilian Nuclear Materials Security and published by National Academies Press. This book was released on 2013-10-14 with total page 186 pages. Available in PDF, EPUB and Kindle. Book excerpt: The U.S. government has made safeguarding of weapons-grade plutonium and highly enriched uranium an international policy priority, and convened The 2010 Nuclear Security Summit in Washington, D.C., on April 12 and 13, 2010. Forty six governments sent delegations to the summit and twenty nine of them made national commitments to support nuclear security. During the Summit, India announced its commitment to establish a Global Centre for Nuclear Energy Partnership. The Centre is to be open to international participation through academic0 exchanges, training, and research and development efforts. India-United States Cooperation on Global Security is the summary of a workshop held by the U.S. National Academy of Sciences (NAS) together with its partner of more than 15 years, the National Institute for Advanced Studies (NIAS) in Bangalore, India. The workshop identified and examined potential areas for substantive scientific and technical cooperation between the two countries on issues related to nuclear material security. Technical experts from India and the United States focused on topics of nuclear material security and promising opportunities for India and the United States to learn from each other and cooperate. This report discusses nuclear materials management issues such as nuclear materials accounting, cyber security, physical security, and nuclear forensics.
Download or read book Forensic Analytical Methods written by Thiago R L C Paixão and published by Royal Society of Chemistry. This book was released on 2019-08-16 with total page 312 pages. Available in PDF, EPUB and Kindle. Book excerpt: Forensic analysis relates to the development of analytical methods from laboratory applications to in-field and in situ applications to resolve criminal cases. There has been a rapid expansion in the past few years in this area, which has led to an increase in the output of literature. This is the first book that brings together the understanding of the analytical techniques and how these influence the outcome of a forensic investigation. Starting with a brief introduction of the chemical analysis for forensic application, some forensic sampling and sample preparation, the book then describes techniques used in forensic chemical sensing in order to solve crimes. The techniques describe current forensic science practices in analytical chemistry and specifically the development of portable detectors to guide the authorities in the field. The book provides an excellent combination of current issues in forensic analytical methods for the graduates and professionals. It will cover the essential principles for students and directly relate the techniques to applications in real situations.
Download or read book Analytical Chemistry of Uranium written by Zeev Karpas and published by CRC Press. This book was released on 2014-11-21 with total page 328 pages. Available in PDF, EPUB and Kindle. Book excerpt: Accurate uranium analysis, and particularly for isotope measurements, is essential in many fields, including environmental studies, geology, hydrogeology, the nuclear industry, health physics, and homeland security. Nevertheless, only a few scientific books are dedicated to uranium in general and analytical chemistry aspects in particular. Analytical Chemistry of Uranium: Environmental, Forensic, Nuclear, and Toxicological Applications covers the fascinating advances in the field of analytical chemistry of uranium. Exploring a broad range of topics, the book focuses on the analytical aspects of industrial processes that involve uranium, its presence in the environment, health and biological implications of exposure to uranium compounds, and nuclear forensics. Topics include: Examples of procedures used to characterize uranium in environmental samples of soil, sediments, vegetation, water, and air Analytical methods used to examine the rigorous specifications of uranium and its compounds deployed in the nuclear fuel cycle Health aspects of exposure to uranium and the bioassays used for exposure assessment Up-to-date analytical techniques used in nuclear forensics for safeguards in support of non-proliferation, including single particle characterization Each chapter includes an overview of the topic and several examples to demonstrate the analytical procedures. This is followed by sample preparation, separation and purification techniques where necessary. The book supplies readers with a solid understanding of the analytical chemistry approach used today for characterizing the different facets of uranium, providing a good starting point for further investigation into this important element.
Download or read book The New Nuclear Forensics written by Vitaly Fedchenko and published by Oxford University Press. This book was released on 2015 with total page 310 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nuclear material changes its form and properties as it moves through the nuclear fuel cycle, from one facility to another. Each step of the fuel cycle or each use of the material will inevitably leave its mark. The science of determining the history of a sample of nuclear material through the study of these characteristics is known as nuclear forensics. While nuclear forensic analysis has normally been associated with investigations and prosecutions in the contextof trafficking of nuclear materials or nuclear terrorism, it had wider applications in in national security contexts, such as nuclear non-proliferation, disarmament, and arms control. The New Nuclear Forensics is the first book to give a definitive guide to this broader definition of nuclear forensic analysis. This book describes the various methods used in nuclear forensics, giving first a broad introduction to the process followed by details of relevant measurement techniques and procedures. In each case, the advantages and limitations are outlined. To put these methods in context, the book also recounts the history of the discipline anddescribes the diverse contemporary applications of nuclear forensics.
