Download or read book Inorganic Ultramicroanalysis written by I. P. Alimarin and published by Elsevier. This book was released on 2013-10-22 with total page 168 pages. Available in PDF, EPUB and Kindle. Book excerpt: Inorganic Ultramicroanalysis focuses on the techniques and experimental methods used in ultramicroanalysis of inorganic compounds. Topics covered include the general apparatus used in the ultramicromethod of chemical analysis, qualitative and quantitative analysis, and methods of separation. This book consists of six chapters and opens with a review of the special features of the ultramicromethod of chemical analysis, paying particular attention to the use of the law of errors to calculate the limiting quantity of a substance necessary for the performance of chemical operations. The surface area of unit volume in the macro- and ultramicromethods of analysis is also compared. The next chapter deals with the general apparatus used in ultramicroanalysis, including the microscope and micromanipulators, and describes techniques of working with small volumes. The reader is then introduced to qualitative and quantitative analysis and methods of separation such as precipitation and electrolysis. The last chapter discusses future prospects for inorganic ultramicroanalysis. This monograph is written primarily for inorganic and analytical chemists.

Download or read book Organic Reagents in Metal Analysis written by K. Burger and published by Elsevier. This book was released on 2013-10-22 with total page 269 pages. Available in PDF, EPUB and Kindle. Book excerpt: International Series of Monographs in Analytical Chemistry, Volume 54: Organic Reagents in Metal Analysis focuses on the factors determining the analytical selectivity of complexation reactions. This book consists of three chapters. Chapter 1 deals with the effects of stability and electronic structure of complexes and formation of mixed ligand complexes on analytical selectivity. The analytical procedures for the accomplishment of many metal analytical tasks are reviewed in Chapter 2. The last chapter provides a tabulated data that facilitates experimental work in the field of metal analysis. This volume is useful to practical analysts and researchers engaged with developments in the field of analytical chemistry and routine metal analyses.

Download or read book U S Environmental Protection Agency Library System Book Catalog Holdings as of July 1973 written by United States. Environmental Protection Agency. Library Systems Branch and published by . This book was released on 1974 with total page 702 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Download or read book Chemical Analysis of Additives in Plastics written by T. R. Crompton and published by Elsevier. This book was released on 2016-07-29 with total page 381 pages. Available in PDF, EPUB and Kindle. Book excerpt: International Series in Analytical Chemistry, Volume 46: Chemical Analysis of Additives in Plastics, Second Edition brings together numerous investigations on the characterization, identification, and determination of various types of additives in plastics. This book is divided into five chapters. Chapters 1 and 2 describe first the methods for examining additives present in polymers based on either direct spectroscopy of a cast polymer film or on solvent extraction of total additives from the polymer followed by quantitative chemical or physical analysis for various components in the extract. Chapter 3 discusses the application of thin-layer and column chromatography to the separation and determination of known additives. Chapters 4 and 5 examine the application of combined chromatographic and spectroscopic techniques for the separation and determination of unknown plastics additives. This book will prove useful to plastics manufacturers, researchers, institutions, and universities.

Download or read book Isotope Dilution Analysis written by J. Tölgyessy and published by Elsevier. This book was released on 2013-10-22 with total page 197 pages. Available in PDF, EPUB and Kindle. Book excerpt: International Series of Monographs in Analytical Chemistry, Volume 49: Isotope Dilution Analysis focuses on the method of isotope dilution analysis (IDA). The book first discusses the principles, types, and theory of IDA. Classification of the methods of IDA; precision, accuracy, and sensitivity of IDA; and types of IDA are described. The text also examines experimental techniques, separation, and mass determination. The separation of components, reagents and tracers, and amount of substance separated are underscored. The text takes a look at the inorganic applications of IDA, including determination of elements and selected procedures. The text examines the applications of IDA in organic chemistry and biochemistry, particularly in the analysis of alcohols and ethers, steroids, penicillin, proteins and amino acids, and insecticides. The book discusses IDA with stable isotopes. Methods for the determination of isotopic composition, fundamentals and technique, and practical applications are underscored. The text also emphasizes the special applications of isotope dilution. Determination of the content of isotopic carriers in radioactive preparations; determination of the coefficient of self-absorption and specific activity; and determination of radioactive contaminants are discussed. The text is a vital reference for readers interested in isotope dilution analysis.

Download or read book Analytical Chemistry of Organic Halogen Compounds written by L. Mázor and published by Elsevier. This book was released on 2013-09-03 with total page 292 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Chemistry of Organic Halogen Compounds presents the procedures applied in the analysis of organic halogen compounds. This book is composed of eight chapters that discuss the methods involved in the production and application of organic halogen compounds and in overcoming contamination problems caused by these compounds. After briefly dealing with the preparation, characteristics, and reactions of organic halogen compounds, this book goes on discussing the fundamental concepts of methods for the detection of halogens in organic compounds, namely, chlorine, bromine, iodine, and fluorine. The following chapter describes the characteristic features, advantages, and disadvantages of ultramicro and submicro chemical methods. A chapter also examines the qualitative and quantitative studies of organic halogen compounds based on the thermal and chemical stability of these compounds. The concluding chapters discuss the interference or interfering effects of halogens and their elimination in the determination of other elements. A list of physical constants of organic halogen compounds of general pharmaceutical and industrial significance is provided. This book is an ideal source for analytical chemists and other workers who are interested in the theoretical bases of the methods.

Download or read book The Destruction of Organic Matter written by T. T. Gorsuch and published by Elsevier. This book was released on 2013-10-22 with total page 161 pages. Available in PDF, EPUB and Kindle. Book excerpt: International Series of Monographs in Analytical Chemistry, Volume 39: The Destruction of Organic Matter focuses on the identification of trace elements in organic compounds. The monograph first offers information on the processes involved in the determination of trace elements in organic matters, as well as the methods not involving complete destruction of these elements. The text surveys the sources of errors in the processes responsible in pinpointing elements in organic compounds. These processes include sampling, disruption of the samples, manipulation, and measurements. The book examines the processes of wet and dry oxidation, including their applications to sulfuric, nitric, and perchloric acids and hydrogen peroxide. The methods of dry ashing and oxidation with excited oxygen and oxidative fusion are elaborated. The text also underscores the varying methods in removing trace elements in organic compounds. The elements include zinc, copper, silver, gold, lead, germanium, titanium, arsenic, bismuth, and vanadium. The book also describes wet digestion methods and dry ashing procedures in the removal of trace elements in organic matters. The monograph is a vital source of information for readers interested in the identification of trace elements in organic compounds.

Download or read book Enzymatic Methods of Analysis written by George G. Guilbault and published by Elsevier. This book was released on 2013-10-22 with total page 367 pages. Available in PDF, EPUB and Kindle. Book excerpt: Enzymatic Methods of Analysis attempts to cover all the aspects of modern enzymatic analysis. Enzymes possess a great potential usefulness in analytical chemistry. The specificity of enzymes can solve the primary problem of most analytical chemists—the analysis of one substance in the presence of many similar compounds that interfere in the analysis. The book begins with two introductory chapters devoted to general considerations of enzymes as reagents and methods of analysis of enzymatic reactions. The next four chapters deal with methods for the assay of specific enzymes, and substrate, activator, and inhibitor analysis using enzymes. In the last two chapters the immobilization of enzymes and the automation of enzymatic reactions are discussed. In addition, a listing of all commercially available enzymes is given in an appendix. It is hoped that the information presented will prove interesting and stimulating to all individuals engaged in research and development.

Download or read book Substoichiometry in Radiochemical Analysis written by Jaromír Růžička and published by Elsevier. This book was released on 2013-10-22 with total page 165 pages. Available in PDF, EPUB and Kindle. Book excerpt: Substoichiometry in Radiochemical Analysis considers application of simple chemistry than the use of complicated instrumentation in studying radiochemical analysis. This book is divided into nine chapters; the first chapter gives an introduction to the content of this monograph. This text then examines the neutron-activation and isotope-dilution analyses, complemented with the general technique and preliminary experiments. Specifically, this book provides the methods for the substoichiometric determination of traces of various elements by the neutron-activation and isotope-dilution analyses. Copper, mercury, gallium, gold, and zinc are some of the elements featured in this particular topic. This topic is followed by the discussion on the analysis of radioactive materials. This text also tackles the automation and comparison with other radiometric methods of substoichiometric analysis, as well as trends in substoichiometry. This book will be helpful for those concerned with substoichiometry, especially those who need a book that presents non-complicated study of the subject.

Download or read book Analysis of Organoaluminium and Organozinc Compounds written by T. R. Crompton and published by Elsevier. This book was released on 2013-10-22 with total page 377 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analysis of Organoaluminum and Organozinc Compounds, Volume 31 presents information pertinent to the organo compound of aluminum and zinc. This book discusses the growing interest in organoaluminum compounds as intermediates in the manufacture of organic chemicals. Comprised of nine chapters, this volume begins with an overview of the methods for the determination of different functional groups and elements in organoaluminum compounds, viz. alkyle, alkozide, hydride, aluminum, halogens, amino and thio alkoxide groups. This text then explains the different solution methods of analysis of organoaluminum compounds, including various titrimetric procedures. Other chapters consider an iodometric titration method for analyzing organoaluminum compounds, which is particularly useful for rapid analysis of diluted samples. This book discusses as well the extensive work on the analysis of organoaluminum compounds by thermometric titrimetry with suitable reagents. The final chapter deals with the detailed procedures for carrying out different analyses. This book is a valuable resource for students of analytical chemistry.

Download or read book Analysis of Ancient Metals written by Earle R. Caley and published by Elsevier. This book was released on 2013-10-22 with total page 189 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analysis of Ancient Metals provides a guide to the identification and analysis of ancient metals and alloys. The title details the various analytical methods and procedures in dealing with different metals and alloys. The text first discusses the heterogeneity of ancient metals and the sampling problem, and then proceeds to covering preliminary observations and measurements, qualitative tests, and choice of quantitative method. The next series of chapters details the methods and procedures in the analysis of gold, silver, copper, iron, and steel, as well as various nonferrous metals. The last chapter discusses the concerns in reporting the findings. The book will be of great interest to materials engineers and metallurgists. Archeologists and museologists will also greatly benefit from the text.

Download or read book Inorganic Ultramicroanalysis written by I. P. Alimarin and published by . This book was released on 1964 with total page 151 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Download or read book Identification of Materials written by Anton A. Benedetti-Pichler and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 506 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book has been written for the practicing chemist whose occasional task may be qualitative analysis. It deals with the investigation of things as they are without any limitations to the scope. It emphasizes the identification of materials - inorganic, organic, organized (biological), common, rare, described or not described in the accessible literatur- as they actually occur in nature and industry, or are met in the investigation of mishaps and crime. The description of techniques - macro to submicro - and the practice exercises have been included since the teaching of these arts is rarely a part of academic curricula and it happens with increasing frequency that chemists have to acquire them "on the job". In the systematic procedure given, emphasis is placed upon the investiga tion of minute specimens and upon acute reasoning that continuously weighs all accumulating evi9.ence. The work begins with the consideration of the history of the material under investigation. Especially when specks of all organic substance shall be identified, it should be realized that the discovery of the source - and consequently of the possibilities involve- may be the most valuable clue to an efficient solution of the problem.

Download or read book Indicators written by Edmund Bishop and published by Elsevier. This book was released on 2013-10-22 with total page 759 pages. Available in PDF, EPUB and Kindle. Book excerpt: Indicators offers a comprehensive account of indicators and their applications in areas such as titrimetric analysis and the analysis of mineral waters. The theory and principles of visual indicators are discussed, along with acid-base indicators, indicators for non-aqueous acid-base titrations, and titrations with non-chelating ligands. Metallochromic indicators, adsorption indicators, oxidation-reduction indicators, and fluorescent and chemiluminescent indicators are also considered. This volume is comprised of 10 chapters and begins with a brief history of indicators, including the contribution of Robert Boyle in the field. The different kinds of indicators are also described, along with developments in indicators in the nineteenth century. The next chapter deals with the theory and principles of visual indicators, followed by a discussion on acid-base indicators such as organic dyes, inorganic substances, compounds capable of fluorescence, and chemiluminescent systems. Subsequent chapters explore other varieties of indicators, including indicators for non-aqueous acid-base titrations, metallochromic indicators, and adsorption indicators, as well as oxidation-reduction indicators and fluorescent and chemiluminescent indicators. This book will be of interest to chemists.

Download or read book Analytical Chemistry of Molybdenum and Tungsten written by W. T. Elwell and published by Elsevier. This book was released on 2013-10-22 with total page 290 pages. Available in PDF, EPUB and Kindle. Book excerpt: International Series of Monographs in Analytical Chemistry, Volume 47: Analytical Chemistry of Molybdenum and Tungsten describes the chemical and instrumental methods of analysis of molybdenum and tungsten. This book is composed of 15 chapters that particularly consider detailed methods for determining these metals in typical samples and their alloys by both classical and modern techniques. The opening chapters discuss the history, occurrence, physico-chemical properties, and applications of molybdenum and tungsten. The succeeding chapters deal with the metals’ sampling, decomposition, separation, and qualitative detection. Considerable chapters are devoted to various chemical and instrumental methods for their analysis, including gravimetry, titrimetry, colorimetry, polarography, amperometry, coulometry, emission and atomic absorption spectroscopy, X-ray spectrophotometry, mass spectrometry, and radiochemical methods. The concluding chapter examines the determination of impurities and alloying elements. This book will prove useful to analytical and inorganic chemists, as well as analytical and inorganic chemistry students.

Download or read book Analytical Applications of EDTA and Related Compounds written by R. Přibil and published by Elsevier. This book was released on 2013-09-17 with total page 391 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical Applications of EDTA and Related Compounds examines the analytical applications of ethylenediaminetetra-acetic acid (EDTA) and related compounds. This book also considers the “passive role of these substances, that is, their screening (masking) properties, which greatly improve the selectivity of the reactions in common use. This text consists of six chapters organized into two sections. The first part deals with the uses of EDTA and its derivatives in some fields of chemical analysis. After providing an overview of the history behind the development of EDTA as an analytical reagent, this book discusses to the nature of equilibria of complexes and the methods used in their investigation. The next chapter is dedicated to the reactions of “classical gravimetric analysis, including the precipitation reactions by means of organic reagents. The chapter on colorimetry includes a section on “colored complexing agents, which can be used also in colorimetric determinations of some elements. This text concludes by evaluating the use of EDTA as a masking agent in colorimetry. This book will be of interest to students and practitioners working in analytical chemistry and related disciplines, including polarography, chromatography, electrophoresis, flame photometry, and qualitative analysis.

Download or read book Principles of Field Ionization and Field Desorption Mass Spectrometry written by H. D. Beckey and published by Elsevier. This book was released on 2016-07-29 with total page 355 pages. Available in PDF, EPUB and Kindle. Book excerpt: Principles of Field Ionization and Field Desorption Mass Spectrometry delves deeper into field ionization and field desorption. The book covers the five main subareas of field ionization and field desorption mass spectrometry that has grown in importance. Coverage includes the theory of field ionization and field desorption; field ionization and field desorption techniques and sources; high field surface chemistry; kinetics and mechanisms of decompostion of field ions in the gas phase; and qualitative and mixture analysis with field ionization and field desorption mass spectrometry. The text is recommended for students, experts, and researchers in chemistry, especially those who wish to learn more or have an in-depth study about field ionization and field desorption, its principles, and its applications in chemistry.