Download or read book Field Gas Chromatography thermionic Detector System for On site Determination of Explosives in Soils written by Alan Dole Hewitt and published by . This book was released on 2001 with total page 32 pages. Available in PDF, EPUB and Kindle. Book excerpt: On-site determination of nitroaromatic, nitramine, and nitrate ester explosives compounds in soils was performed using a field-portable gas chromatograph (GC)equipped with a thermionic ionization detector (TID)selective for compounds with nitro functional groups. Soil samples were extracted with acetone. A 1 microliter volume of the filtered soil extract was manually injected into the GC, allowing for the rapid qualification and quantification of the suite of explosives that often coexist in soils at military training facilities and other defense-related sites. Good agreement was established for the concentrations of several explosives analytes when this method of analysis was compared to either high-performance liquid chromatography (Method 8330)or GC electron capture (Method 8095)analysis. Comparisons were performed for sample extracts and for soil subsample replicates distributed for on-site preparation and analysis during a field verification test performed under the auspices of the U.S. Environmental Protection Agency's Environmental Technology Verification (ETV)Program.

Download or read book Trace Chemical Sensing of Explosives written by Ronald L. Woodfin and published by John Wiley & Sons. This book was released on 2006-12-15 with total page 396 pages. Available in PDF, EPUB and Kindle. Book excerpt: This timely book covers the most recent developments in the chemical detection of explosives in a variety of environments. Beginning with a broad view of the need for and the potential applications of chemical sensing, the book considers the issue of how to effectively include chemical sensing into systems designed to find hidden explosives devices. Offering a firsthand look at the latest technologies direct from those who are actively developing them, the book features: A look at the history of the field, including the contributions of recent programs A brief explanation of the chemistry of various explosives and differences in the place where they may be detected An introduction to the problems presented by trace element sensing An overview and comparison of the technologies currently being used and developed Case studies of field experiences with chemical sensors A look at the emerging threat of non-traditional explosives This book is an important reference for explosives engineers, systems engineers involved in the development of related devices, government agencies and NGOs involved in demining efforts, military and law enforcement specialists in mines and explosive ordinance disposal (EOD), as well as environmental scientists and chemists involved in explosives research. In addition to providing field workers with knowledge that will help them decide where and how to search for explosives using chemical sensors. It will provide them with an understanding of the potential and the limitations of chemical sensing in their search for and identification of dangerous devices.

Download or read book Biological Remediation of Explosive Residues written by Shree Nath Singh and published by Springer Science & Business Media. This book was released on 2013-08-04 with total page 406 pages. Available in PDF, EPUB and Kindle. Book excerpt: Microbial degradation, Phytoremediation, Remediation, Explosive residues, Biotransformation, Mineralization, Degradative Enzymes, Degradation Pathways, Energetics, Soil contamination, Water contamination.

Download or read book Detectors in Gas Chromatography written by and published by Elsevier. This book was released on 2011-10-10 with total page 193 pages. Available in PDF, EPUB and Kindle. Book excerpt: Detectors in Gas Chromatography

Download or read book Detector Dogs and Scent Movement written by Tom Osterkamp and published by CRC Press. This book was released on 2020-04-06 with total page 179 pages. Available in PDF, EPUB and Kindle. Book excerpt: Dogs detect scent from a source that is carried to them in a plume by the wind. The most important tool for a detector dog handler to have on searches is a knowledge of scent plume movement or "scent dynamics" (the science of scent movement). Such knowledge resides primarily in scientific journals that are largely inaccessible to detector dog handlers and written in language that is difficult to understand. Detector Dogs and the Science of Scent Movement: A Handler’s Guide to Environments and Procedures retrieves, reviews, and interprets the results of pertinent scientific research on scent dynamics and presents these results in terms that are easier for handlers to understand. Information on the physiology of the dog’s nose, their sense of smell, and the properties of scent provide the essential information on the process of scenting. The composition of training aids for explosives, narcotics, human remains and other sources is discussed. Recommendations are made on the use of training aids, their placement during training, and the resulting availability of scent. Potential problems and handler errors in the use of training aids are also examined. The characteristics of scent plumes and how wind influences their movement are a key focus of the book. The primary task for the handler is to get the dog into the scent plume so that the dog can detect the scent and follow it to the source the handler seeks. As such, a knowledge of scent and scent plume movement will vastly improve the ability of the handler to accomplish this task. The influence of weather and physical settings such as terrain, vegetation, ground cover, soil and water on scent movement are examined in detail. Strategies for searching, detecting, and locating sources in all physical settings are presented. Specific effects associated with hills and mountains, fields and forests, bare soils and soils covered by vegetation, different soil types, and lakes and rivers are examined in detail. This includes specific recommendations are made about weather and physical settings that result in higher probability of success on searches. Detector Dogs and the Science of Scent Movement will be a vital resource for K9 handles in the private and public sectors—including in Homeland Security, law enforcement, and military settings—as well as a useful guide for lawyers, forensic, and investigative professionals who need to better understand K9 operations.

Download or read book Chromatographic Detectors written by Raymond P.W. Scott and published by CRC Press. This book was released on 1996-07-17 with total page 544 pages. Available in PDF, EPUB and Kindle. Book excerpt: "Comprehensively covers the design, construction, and operation of gas chromatography, liquid chromatography, and thin-layer chromatography detectors--all in one convenient, up-to-date source. Emphasizes the essential use of common specifications to describe all detectors, allowing easy comparison of their attributes."

Download or read book Gas Chromatographic Detectors written by Donald Joseph David and published by Wiley-Interscience. This book was released on 1974 with total page 332 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal conductivity detectors; Flame ionization detection; Electron capture detection; The thermionic detector; The ultrasonic detector; Helium ionization detector; Flame photometric detection; Electrochemical detectors; Miscellaneous detectors.

Download or read book Environmental Technology Verification Report written by and published by . This book was released on 1997 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: The Bruker-Franzen EM640 GC/MS consists of a temperature-programmable gas chromatograph coupled to a mass spectrometer. The field transportable system used a small gas chromatographic column and accompanying mass spectrometer to provide separation, identification, and quantification of volatile and semi-volatile organic compounds in soils, liquids, and gases. In the demonstration, the system used a spray-and-trap technique for water analysis, as well as direct injection and head space analysis for soil gas and soil analyses, respectively. The column enables separation of individual analytes in complex mixtures. As these individual analytes exit the column, the mass spectrometer detects the analytes, providing a characteristic mass spectrum that identifies each compound. An external computer system provides quantitation by comparison of detector response with a calibration table constructed from standards of known concentration. The system provides very low detection limits for a wide range of volatile and semi-volatile organic contaminants.

Download or read book Environmental Technology Verification Report Field Portable Gas Chromatograph Mass Spectrometer Bruker Franzen Analytical Systems Inc EM640 T written by and published by . This book was released on 1997 with total page 108 pages. Available in PDF, EPUB and Kindle. Book excerpt: The Bruker-Franzen EM640 GC/MS consists of a temperature-programmable gas chromatograph coupled to a mass spectrometer. The field transportable system used a small gas chromatographic column and accompanying mass spectrometer to provide separation, identification, and quantification of volatile and semi-volatile organic compounds in soils, liquids, and gases. In the demonstration, the system used a spray-and-trap technique for water analysis, as well as direct injection and head space analysis for soil gas and soil analyses, respectively. The column enables separation of individual analytes in complex mixtures. As these individual analytes exit the column, the mass spectrometer detects the analytes, providing a characteristic mass spectrum that identifies each compound. An external computer system provides quantitation by comparison of detector response with a calibration table constructed from standards of known concentration. The system provides very low detection limits for a wide range of volatile and semi-volatile organic contaminants.

Download or read book Soil Screening Guidance written by and published by . This book was released on 1996 with total page 182 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Download or read book Risk Regulatory and Monitoring Considerations written by Godage B. Wickramanayake and published by . This book was released on 2000 with total page 456 pages. Available in PDF, EPUB and Kindle. Book excerpt: - Regulatory Perspectives and Decision-Making- Advances in Site Characterization- Environmental Data Management, Geostatistics, and GIS- Advances in Analytical and Detection Techniques- Risk-Based Analyses for Remediation- Human Health/Ecological Risk Assessment- Technical Impracticability- Long-Term Monitoring and Optimization- Innovative Monitoring and Control Systems.

Download or read book Chemical and Biological Terrorism written by Committee on R&D Needs for Improving Civilian Medical Response to Chemical and Biological Terrorism Incidents and published by National Academies Press. This book was released on 1999-02-26 with total page 303 pages. Available in PDF, EPUB and Kindle. Book excerpt: The threat of domestic terrorism today looms larger than ever. Bombings at the World Trade Center and Oklahoma City's Federal Building, as well as nerve gas attacks in Japan, have made it tragically obvious that American civilians must be ready for terrorist attacks. What do we need to know to help emergency and medical personnel prepare for these attacks? Chemical and Biological Terrorism identifies the R&D efforts needed to implement recommendations in key areas: pre-incident intelligence, detection and identification of chemical and biological agents, protective clothing and equipment, early recognition that a population has been covertly exposed to a pathogen, mass casualty decontamination and triage, use of vaccines and pharmaceuticals, and the psychological effects of terror. Specific objectives for computer software development are also identified. The book addresses the differences between a biological and chemical attack, the distinct challenges to the military and civilian medical communities, and other broader issues. This book will be of critical interest to anyone involved in civilian preparedness for terrorist attack: planners, administrators, responders, medical professionals, public health and emergency personnel, and technology designers and engineers.

Download or read book Detection Technologies for Chemical Warfare Agents and Toxic Vapors written by Yin Sun and published by CRC Press. This book was released on 2004-08-12 with total page 294 pages. Available in PDF, EPUB and Kindle. Book excerpt: While it is not possible to predict or necessarily prevent terrorist incidents in which chemical warfare agents (CWAs) and toxic industrial chemicals (TICs) are deployed, correctly chosen, fast, and reliable detection equipment will allow prepared rescue workers to respond quickly and minimize potential casualties. Detection Technologies

Download or read book Chemical Abstracts written by and published by . This book was released on 2002 with total page 2626 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Download or read book Handbook of Solid Phase Microextraction written by Janusz Pawliszyn and published by Elsevier. This book was released on 2011-12-01 with total page 497 pages. Available in PDF, EPUB and Kindle. Book excerpt: The relatively new technique of solid phase microextraction (SPME) is an important tool to prepare samples both in the lab and on-site. SPME is a "green" technology because it eliminates organic solvents from analytical laboratory and can be used in environmental, food and fragrance, and forensic and drug analysis. This handbook offers a thorough background of the theory and practical implementation of SPME. SPME protocols are presented outlining each stage of the method and providing useful tips and potential pitfalls. In addition, devices and fiber coatings, automated SPME systems, SPME method development, and In Vivo applications are discussed. This handbook is essential for its discussion of the latest SPME developments as well as its in depth information on the history, theory, and practical application of the method. Practical application of Solid Phase Microextraction methods including detailed steps Provides history of extraction methods to better understand the process Suitable for all levels, from beginning student to experienced practitioner

Download or read book Mapping the Chemical Environment of Urban Areas written by Christopher C. Johnson and published by John Wiley & Sons. This book was released on 2011-02-11 with total page 640 pages. Available in PDF, EPUB and Kindle. Book excerpt: This comprehensive text focuses on the increasingly important issues of urban geochemical mapping with key coverage of the distribution and behaviour of chemicals and compounds in the urban environment. Clearly structured throughout, the first part of the book covers general aspects of urban chemical mapping with an overview of current practice and reviews of different aspects of the component methodologies. The second part includes case histories from different urban areas around Europe authored by those national or academic institutions tasked with investigating the chemical environments of their major urban centers.

Download or read book Gas Chromatography and Mass Spectrometry A Practical Guide written by O. David Sparkman and published by Academic Press. This book was released on 2011-05-17 with total page 633 pages. Available in PDF, EPUB and Kindle. Book excerpt: The second edition of Gas Chromatography and Mass Spectrometry: A Practical Guide follows the highly successful first edition by F.G. Kitson, B.S. Larsen, and C.N. McEwen (1996), which was designed as an indispensible resource for GC/MS practitioners regardless of whether they are a novice or well experienced. The Fundamentals section has been extensively reworked from the original edition to give more depth of an understanding of the techniques and science involved with GC/MS. Even with this expansion, the original brevity and simple didactic style has been retained. Information on chromatographic peak deconvolution has been added along with a more in-depth understanding of the use of mass spectral databases in the identification of unknowns. Since the last edition, a number of advances in GC inlet systems and sample introduction techniques have occurred, and they are included in the new edition. Other updates include a discussion on fast GC and options for combining GC detectors with mass spectrometry. The section regarding GC Conditions, Derivatization, and Mass Spectral Interpretation of Specific Compound Types has the same number of compound types as the original edition, but the information in each section has been expanded to not only explain some of the spectra but to also explain why certain fragmentations take place. The number of Appendices has been increased from 12 to 17. The Appendix on Atomic Masses and Isotope Abundances has been expanded to provide tools to aid in determination of elemental composition from isotope peak intensity ratios. An appendix with examples on "Steps to follow in the determination of elemental compositions based on isotope peak intensities" has been added. Appendices on whether to use GC/MS or LC/MS, third-party software for use in data analysis, list of information required in reporting GC/MS data, X+1 and X+2 peak relative intensities based on the number of atoms of carbon in an ion, and list of available EI mass spectral databases have been added. Others such as the ones on derivatization, isotope peak patterns for ions with Cl and/or Br, terms used in GC and in mass spectrometry, and tips on setting up, maintaining and troubleshooting a GC/MS system have all been expanded and updated. Covers the practical instruction necessary for successful operation of GC/MS equipment Reviews the latest advances in instrumentation, ionization methods, and quantitation Includes troubleshooting techniques and a variety of additional information useful for the GC/MS practitioner A true benchtop reference A guide to a basic understanding of the components of a Gas Chromatograph-Mass Spectrometer (GC-MS) Quick References to data interpretation Ready source for information on new analyses