Download or read book Determination of Volatile Organic Compounds in Solid Waste by Head Space Gas Chromatography and Gas Chromatography Mass Spectrometry written by Noraini Ahmad and published by . This book was released on 2007 with total page 46 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Headspace Solid Phase Microextraction Gas Chromatography Mass Spectrometry written by DJ. Tranthim-Fryer and published by . This book was released on 2001 with total page 13 pages. Available in PDF, EPUB and Kindle. Book excerpt: This paper describes the application of Headspace/Solid-Phase Microextraction/Gas Chromatography-Mass Spectrometry (HS/SPME/GC-MS) to the recovery and identification of volatile organic compounds in blood and viscera samples from decreased persons. The technique is used as a screening procedure to rapidly obtain information relating to toxicological investigations. The technique is suitable for the detection of volatiles (of wide boiling range) including butane, halothane, toluene, xylenes, and petrol residues in blood and viscera (lung, brain, and body fat).
Download or read book Comparison of Headspace Gas Chromatography with EPA SW 846 Method 8240 for Determination of Volatile Organic Compounds in Soil written by and published by . This book was released on 1991 with total page 16 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Static Headspace Gas Chromatography written by Bruno Kolb and published by John Wiley & Sons. This book was released on 2006-06-23 with total page 384 pages. Available in PDF, EPUB and Kindle. Book excerpt: The only reference to provide both current and thorough coverage of this important analytical technique Static headspace-gas chromatography (HS-GC) is an indispensable technique for analyzing volatile organic compounds, enabling the analyst to assay a variety of sample matrices while avoiding the costly and time-consuming preparation involved with traditional GC. Static Headspace-Gas Chromatography: Theory and Practice has long been the only reference to provide in-depth coverage of this method of analysis. The Second Edition has been thoroughly updated to reflect the most recent developments and practices, and also includes coverage of solid-phase microextraction (SPME) and the purge-and-trap technique. Chapters cover: * Principles of static and dynamic headspace analysis, including the evolution of HS-GC methods and regulatory methods using static HS-GC * Basic theory of headspace analysis-physicochemical relationships, sensitivity, and the principles of multiple headspace extraction * HS-GC techniques-vials, cleaning, caps, sample volume, enrichment, and cryogenic techniques * Sample handling * Cryogenic HS-GC * Method development in HS-GC * Nonequilibrium static headspace analysis * Determination of physicochemical functions such as vapor pressures, activity coefficients, and more Comprehensive and focused, Static Headspace-Gas Chromatography, Second Edition provides an excellent resource to help the reader achieve optimal chromatographic results. Practical examples with original data help readers to master determinations in a wide variety of areas, such as forensic, environmental, pharmaceutical, and industrial applications.
Download or read book Aqueous Extraction Headspace Gas Chromatographic Meth Od for Determination of Volatile Organic Compounds in Soils written by and published by . This book was released on 1992 with total page 20 pages. Available in PDF, EPUB and Kindle. Book excerpt: This study compares aqueous extraction-headspace/Gas Chromatography (GC) and the EPA SW-846 purge-and-trap-gas chromatography/mass spectrometry(Method 8240)for the determination of four common Volatile Organic Compounds (VOCs) in soils. Comparisons were made on two fortified soils and two contaminated field soils. In only two of the cases were consistent significant differences found-for the two most hydrophobic compounds in a high organic carbon soil, and for TCE in a field-contaminated soil that had previously shown slow aqueous VOC desorption. The findings strongly suggest that aqueous extraction-headspace/GC can be used not only to screen soils for VOCs giving same-day results, but often will provide results not significantly different from current laboratory based measurements.
Download or read book The Determination of Volatile Organic Compounds at the micro g 1 Level in Water by Gas Chromatography written by Thomas A. Bellar and published by . This book was released on 1974 with total page 44 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Innovations in Site Characterization written by and published by . This book was released on 2001 with total page 70 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Volatile Organic Compounds in Headspace Over Electrical Components written by Neil D. Paz and published by . This book was released on 2007 with total page 160 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Determination of Volatile Organic Compounds in Soils Using Equilibrum Headspace Analysis and Capillary Column Gas Chromatography mass Spectrometry evaluation of the Tekmar 7000 HA Analyzer written by Pedro Flores and published by . This book was released on 1993 with total page 4 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book GB T 2015 GB 2015 Chinese National Standard PDF English Catalog year 2015 written by https://www.chinesestandard.net and published by https://www.chinesestandard.net. This book was released on 2020-06-06 with total page 406 pages. Available in PDF, EPUB and Kindle. Book excerpt: This document provides the comprehensive list of Chinese National Standards - Category: GB, GB/T Series of year 2015.
Download or read book The Evaluation of Environmental Contaminants Using Static Headspace Gas Chromatography Mass Spectrometry Vacuum Ultraviolet Detection and Ionic Liquids written by Emmanuel Varona -Torres and published by . This book was released on 2021 with total page 149 pages. Available in PDF, EPUB and Kindle. Book excerpt: In analytical chemistry the term "headspace" refers to the vapor that forms above a sample (liquid or solid) in a closed container. Headspace (HS) sampling is the method to promote partition between volatile components from the sample matrix and then analyzed by gas chromatography (GC). HS is an excellent technique to introduce a"clean" vapor sample into the GC and avoids introduction of non-volatile components from the sample matrix and often used for determination of volatile organic compounds (VOCs) with minimal or no additional sample preparation. Concerns about the environmental impact of fossil fuel extraction techniques (i.e.,hydraulic fracturing and other well stimulation techniques) have risen due to its expansion in the United States and other countries. Robust atmospheric studies have attributed to the emissions of rogue greenhouse gases and VOCs to mechanical inefficiencies commonly found in the midstream production process, such as gas flaring stations, condensate tanks, and pipelines. However, the interplay between fossil fuel extraction activities and soil quality has not received much attention. Utilizing headspace gas chromatography mass spectrometry (HS-GC-MS) and an establish standard method by the Environmental Protection Agency (EPA), we present a study of soil near oil and gas production in verified emissions of volatile contaminants. The findings provide an initial indication of the interactions between atmospheric VOCs contamination events and the accumulation of those contaminants in soil where, varying soil texture was found to contribute to total amount detected. Room temperature ionic liquids (RTILs) have received significant attention in HS analysis due to their unique physiochemical properties (i.e., negligible vapor pressures, tunable thermal stabilities, tunable viscosities and wide liquid range). RTILs are salts in which ions are poorly coordinated, resulting in a liquid state at room temperature. The evaluation of RTILs as co-solvent in soil analysis, in an effort to increase sensitivity, reduce and normalized the matrix-effects associated with varying soil compositions. It was found that hydrophilic RTILs investigated, 1-ethyl-3-methylimidazolium ethylsulfate ([EMIM][ESO4]), 1-ethyl-3-methylimidazolium diethyl phosphate ([EMIM][DEP]), tris(2-hydroxyethyl)methylammonium methylsulfate ([MTEOA][MeOSO3]), reduced matrix-effect from varying soil composition thus, reducing the need to characterized and matrix-match soil textures for calibration purposes. It also reduced the analysis time and increased precision and accuracy for the quantification of VOCs in variable soil matrices relative to standard methods. Understanding the thermodynamic interactions between an analyte and the sample phase is of paramount importance when eliciting a co-solvent in HS analysis. The partition coefficient (KP) is an equilibrium constant that describes the distribution of the analyte between two phases (i.e., sample phase/ gas phase). Kp determinations by HSGC is acquired by two methods: vapor phase calibration (VPC) and phase ratio variation (PRV). Kp determinations of analytes in HS co-solvents can help guide the analyst in which to use for the analysis at hand. Here we demonstrate the ability of using a pressurized - loop HS system in conjunction with gas chromatography vacuum ultraviolet detection (HS-GC-VUV) to directly calculate the concentration of the analyte in the gas phase, by pseudo-absolute quantification (PAQ), thus allowing for quick determination of Kp and other thermodynamic properties such as enthalpy ( ∆H )and entropy (∆S ) of the system. The Kp determinations by PAQ were comparable to those obtained using theVP C method, with differences in the average values ranging
Download or read book Chinese Standard GB GB T GBT JB JB T YY HJ NB HG QC SL SN SH JJF JJG CJ TB YD YS NY FZ JG QB SJ SY DL AQ CB GY JC JR JT written by https://www.chinesestandard.net and published by https://www.chinesestandard.net. This book was released on 2018-01-01 with total page 7266 pages. Available in PDF, EPUB and Kindle. Book excerpt: This document provides the comprehensive list of Chinese National Standards and Industry Standards (Total 17,000 standards).
Download or read book Determination of Organic Compounds in Drinking Water by Liquid solid Extraction and Capillary Column Gas Chromatography mass Spectrometry written by and published by . This book was released on 1988 with total page 76 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book GC MS of Biologically and Environmentally Significant Organic Compounds written by Valery A. Isidorov and published by John Wiley & Sons. This book was released on 2020-03-30 with total page 714 pages. Available in PDF, EPUB and Kindle. Book excerpt: Provides a comprehensive guide to the use of gas chromatography–mass spectrometry (GC-MS) on environmentally significant organic compounds This book presents a library of mass spectra of 1,725 biologically and environmentally important organic compounds, in the form of their trimethylsilyl derivatives (TMS), as well as their linear temperature programmed chromatographic retention indices, RI, whose values are in the range of 700-4700 index units. Of the compounds presented, more than 60% of compounds have not previously been characterized by their mass spectra, and more than 70% not previously been characterized by their RI values. Some of these compounds, never before analysed via MS and GC, were detected by the author’s team in plant tissues. The first chapters of the book are devoted to the methodology and practice of sample preparation, as well as to mass spectrometry considerations. They contain the discussion of possible complications and limitations of the method. The book includes lists of chemical compounds in alphabetical order, as well as in the order of their retention indices which facilitates the search for parameters of interest. Every compound in the book includes a RI value, mass spectrum, CAS number (if available), molecular and structural formula, formula weight, chemical name and list of synonyms, as well the source of compounds used for registration of spectrum and RI value. Features mass spectra and chromatographic retention indices of 1,725 organic substances in the form of their trimethylsilyl derivatives (TMS) Includes the CAS number, molecular and structural formula, formula weight, mass spectrum, chemical name and list of synonyms, and more for every compound covered within The first publication containing analytical parameters of high-boiling compounds such as glycosides, lignans, and phenylpropenoid glycerides with RI values >4000 GC-MS of Biologically and Environmentally Significant Organic Compounds will appeal to specialists in phytochemical analysis, food, and environmental chemistry, as well as other investigators dealing with GC or GC/MS analysis complex mixtures of organic compounds. The accompanying electronic database, "Biologically and Environmentally Important Organic Compounds - GCMS Library", will be published in mid-2020, ISBN: 978-1-119-60170-8.
Download or read book Special Report written by and published by . This book was released on 1996 with total page 20 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Behavior and Determination of Volatile Organic Compunds in Soil written by Marti Minnich and published by . This book was released on 1993 with total page 122 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Handbook of Water Analysis written by Leo M.L. Nollet and published by CRC Press. This book was released on 2000-06-27 with total page 948 pages. Available in PDF, EPUB and Kindle. Book excerpt: This work details water sampling and preservation methods by enumerating the different ways to measure physical, chemical, organoleptical, and radiological characteristics. It provides step-by-step descriptions of separation, residue determination, and cleanup techniques for a variety of fresh- and salt-waters. It also discusses information regarding the analysis and detection of bacteria and algae.
