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Book Characterisation of Mixed metal Oxides Prepared by Hydrothermal Synthesis

Download or read book Characterisation of Mixed metal Oxides Prepared by Hydrothermal Synthesis written by Mohammad H. Harunsani and published by . This book was released on 2013 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Hydrothermal Synthesis and Characterization of Transition Metal Oxides

Download or read book Hydrothermal Synthesis and Characterization of Transition Metal Oxides written by Aytaç Şahin and published by . This book was released on 2004 with total page 136 pages. Available in PDF, EPUB and Kindle. Book excerpt: Hydrothermal method has proven to be an excellent method for the synthesis of novel metal oxides and vanadates. This research pertains to the synthesis of novel lead chlorovanadate compound and of a known alkali metal trivanadate compound, KV3O8 by hydrothermal method This method has been used to synthesize many inorganic oxide compounds Hydrothermal synthesis is the use of aqueous solvents under high temperature and high pressure to dissolve and recrystallize materials. Compounds with interesting structure and physical properties are often obtained from this technique that is known as one of the low-temperature synthesis techniques for solid state compounds. There are many studies that have been done on oxides in the Pb-V-O systems There are also many vanadium oxides containing Pb, V, O elements in Pb-V-O system such as Pb1.32V8.35O16.7, PbV6O11, PbV2O6, Pb2V3O8.5, and .-PbxV2O5 bronzes (x = 0.3). In an attempt to synthesize vanadium oxides at low temperature, we were able to obtain needle shaped yellow crystals of PbVO3Cl. In the nature, there is a kombatite mineral, Pb14(VO4)2O9Cl4, with the same composition of elements. A new lead chlorovanadate, PbVO3Cl, was obtained from the reaction of NaVO3 and PbCl2 in aqueous solution of B(OH)3. The compound was prepared in an autoclave that was filled with aqueous solution of B(OH)3 and heated at 170oC for 3 days. The compound crystallizes in the space group Pnma of the orthorhombic system with formula units in a cell of dimensions a = 10.022(2)

Book Sextus liber Decretalium casus litterales et notabilia domini Helie Regnier complexus  cum additionibus ex novella Johannis Andree depromptis

Download or read book Sextus liber Decretalium casus litterales et notabilia domini Helie Regnier complexus cum additionibus ex novella Johannis Andree depromptis written by and published by . This book was released on 1511 with total page 12 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Perovskite Materials

Download or read book Perovskite Materials written by Likun Pan and published by BoD – Books on Demand. This book was released on 2016-02-03 with total page 652 pages. Available in PDF, EPUB and Kindle. Book excerpt: The book summarizes the current state of the know-how in the field of perovskite materials: synthesis, characterization, properties, and applications. Most chapters include a review on the actual knowledge and cutting-edge research results. Thus, this book is an essential source of reference for scientists with research fields in energy, physics, chemistry and materials. It is also a suitable reading material for graduate students.

Book Synthesis and Characterisation of Some Mixed Metal Oxides

Download or read book Synthesis and Characterisation of Some Mixed Metal Oxides written by Sang-Hyun Kim and published by . This book was released on 1993 with total page 424 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Synthesis  Characterization and Catalytic Applications of Mixed Metal Oxides

Download or read book Synthesis Characterization and Catalytic Applications of Mixed Metal Oxides written by Malama Chibwe and published by . This book was released on 1990 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Synthesis and Characterisation of Mixed metal Oxides

Download or read book Synthesis and Characterisation of Mixed metal Oxides written by Siân E. Dutton and published by . This book was released on 2008 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Synthesis and Characterisation of Mixed metal Oxides

Download or read book Synthesis and Characterisation of Mixed metal Oxides written by Siân E. Dutton and published by . This book was released on 2008 with total page 412 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Synthesis and Characterisation of Layered Inorganic Mixed Metal Oxides and Hydroxides

Download or read book Synthesis and Characterisation of Layered Inorganic Mixed Metal Oxides and Hydroxides written by Sharon Jane Mitchell and published by . This book was released on 2009 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Synthesis and Characterization of Solid Metal Oxide Nanaostructures for Biodiesel Production

Download or read book Synthesis and Characterization of Solid Metal Oxide Nanaostructures for Biodiesel Production written by Lai-Fan Man and published by Open Dissertation Press. This book was released on 2017-01-27 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: This dissertation, "Synthesis and Characterization of Solid Metal Oxide Nanaostructures for Biodiesel Production" by Lai-fan, Man, 文麗芬, was obtained from The University of Hong Kong (Pokfulam, Hong Kong) and is being sold pursuant to Creative Commons: Attribution 3.0 Hong Kong License. The content of this dissertation has not been altered in any way. We have altered the formatting in order to facilitate the ease of printing and reading of the dissertation. All rights not granted by the above license are retained by the author. Abstract: Solid basic metal oxides have been extensively studied for biodiesel production via transesterification, researches are now focused on attaining high catalytic activity and durability towards one-step alkali transesterification, as well as high stability towards high free fatty acids (FFAs) and water content in oils for simultaneous esterification and transesterification, to enable their commercialization in industry. This work encompasses the design and characterization of three mixed metal oxide systems, with a detailed evaluation of their potential application in catalyzing transesterification of camelina oil to yield biodiesel. Na0.1Ca0.9TiO3 nanorods were synthesized via a simple alkaline hydrothermal pathway with ethanol as a co-solvent. Owing to their high basic strength of 11A new class of mesoporous Zn/MgO catalyst was synthesized by a simple alkaline hydrothermal method. Zn/MgO calcinated at 600 ℃ exhibited 88.7% biodiesel conversion at 120 ℃ with 3% w/w catalyst, 24:1 methanol to oil molar ratio for 8 h. The catalyst could be reused for five runs without significant loss of activity (>=84.0% biodiesel conversion). The excellent catalyst performance is possibly attributed to its high surface area and large mesopores. The higher surface basic sites density as compared to mesoporous MgO, as indicated by higher total basicity determined from benzoic titration and an increased lattice O2- percentage as revealed from XPS, attributing to its superior catalytic activity. A series of nano-sized MgO-ZnO catalysts with precise stoichiometry were successfully prepared by a simple EDTA complexing approach. Mg0.5Zn0.5 calcinated at 600 ℃ gave a maximum biodiesel conversion of 89.3% at 120 ℃ with 3% w/w catalyst, 24:1 methanol to oil molar ratio for 8 h. Its superior catalytic performance to MgO is mainly associated with the high basic sites density as determined from benzoic titration and XPS. The biodiesel conversion retained over 83.0% for five runs. The enhanced catalyst activity and stability might be contributed by the incorporation of Zn2+ for Mg2+ in MgO lattice and a high homogeneous distribution of MgO particles on ZnO, with the formation of Mg-O-Zn bond as evidenced by Fourier transform infrared spectroscope (FTIR) and XPS. The catalyst also demonstrated high tolerance to FFAs (10% w/w) and water (2% w/w) content, which make it desirable for direct conversion of oils with high FFAs level to biodiesel in a single-step process. Lastly, a Zn/La2O3 catalyst was synthesized by a simple hydrothermal pathway. It exhibits a higher basic strength than La2O3, as evidenced by the slightly lower O1s binding energy determined by XPS, leading to a higher catalytic activity. The enhanced catalytic activity and stability is likely contributed by the incorporation of Zn2+ for La3+ in the lattice. Using 1% w/w Zn/La2O3 as catalyst, the highest biodiesel conversion of 92.7% was obtained at 120 ℃ for 16 h with 36:1 methanol to oil molar ratio. The effective catalyst displayed a biodiesel conversion greater than 84.0% for four runs. DOI: 10.5353/th_b5204899 Subjects:

Book Synthesis and structural characterisation of mixed metal oxide pigment systems

Download or read book Synthesis and structural characterisation of mixed metal oxide pigment systems written by Craig Owens and published by . This book was released on 2004 with total page 230 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Metal Oxides in Heterogeneous Catalysis

Download or read book Metal Oxides in Heterogeneous Catalysis written by Jacques C. Vedrine and published by Elsevier. This book was released on 2018-01-11 with total page 620 pages. Available in PDF, EPUB and Kindle. Book excerpt: Metal Oxides in Heterogeneous Catalysis is an overview of the past, present and future of heterogeneous catalysis using metal oxides catalysts. The book presents the historical, theoretical, and practical aspects of metal oxide-based heterogeneous catalysis. Metal Oxides in Heterogeneous Catalysis deals with fundamental information on heterogeneous catalysis, including reaction mechanisms and kinetics approaches.There is also a focus on the classification of metal oxides used as catalysts, preparation methods and touches on zeolites, mesoporous materials and Metal-organic frameworks (MOFs) in catalysis. It will touch on acid or base-type reactions, selective (partial) and total oxidation reactions, and enzymatic type reactions The book also touches heavily on the biomass applications of metal oxide catalysts and environmentally related/depollution reactions such as COVs elimination, DeNOx, and DeSOx. Finally, the book also deals with future trends and prospects in metal oxide-based heterogeneous catalysis. - Presents case studies in each chapter that provide a focus on the industrial applications - Includes fundamentals, key theories and practical applications of metal oxide-based heterogeneous catalysis in one comprehensive resource - Edited, and contributed, by leading experts who provide perspectives on synthesis, characterization and applications

Book Chemically Deposited Nanocrystalline Metal Oxide Thin Films

Download or read book Chemically Deposited Nanocrystalline Metal Oxide Thin Films written by Fabian I. Ezema and published by Springer Nature. This book was released on 2021-06-26 with total page 926 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book guides beginners in the areas of thin film preparation, characterization, and device making, while providing insight into these areas for experts. As chemically deposited metal oxides are currently gaining attention in development of devices such as solar cells, supercapacitors, batteries, sensors, etc., the book illustrates how the chemical deposition route is emerging as a relatively inexpensive, simple, and convenient solution for large area deposition. The advancement in the nanostructured materials for the development of devices is fully discussed.

Book Iron Oxides in the Laboratory

Download or read book Iron Oxides in the Laboratory written by Udo Schwertmann and published by John Wiley & Sons. This book was released on 2000-07-06 with total page 216 pages. Available in PDF, EPUB and Kindle. Book excerpt: Dieses Buch bietet * zuverlässige, streng geprüfte und aktuelle Methoden zur Synthese der wichtigsten Eisenoxide, * eine ausführliche Beschreibung der Verfahren zur Charakterisierung der Eisenoxide, * Laborverfahren und -materialien, die dem Naturwissenschaftler allgemein zugänglich sind, * Hinweise auf mögliche Fehlerquellen bei der Synthese, * Informationen bezogen auf Chemie, Bodenkunde, Medizin, Korrosionswissenschaft und Umweltchemie.