Download or read book Use of IsoProbe for Uranium and Plutonium Analysis in Environmental Samples written by and published by . This book was released on 2000 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: The ability to detect and isotopically characterize uranium and plutonium in environmental samples is of primary importance in the search for nuclear proliferation. The utility of isotope ratio measurements for environmental monitoring is limited by sample preparation costs, measurement precision, and sensitivity. This is particularly true for wide-area monitoring where the number of samples required varies inversely with obtainable precision and sensitivity. This report summarizes an initial evaluation of the applicability of a new technique, magnetic-sector, multicollector, inductively-coupled-plasma mass spectrometry, to environmental sample analysis. This technique is embodied at Lawrence Livermore National Laboratory in the form of a commercially available instrument, the IsoProbe, manufactured by micromass, LTD. (United Kingdom). This is the second of the current generation of such instruments installed in the United States and the first within the Department of Energy complex. Inductively-coupled plasma mass spectrometry (ICPMS) using quadrupole mass filters has existed for roughly 15 years. Magnet sector instruments have also existed for about half that time and multicollector instruments have existed for nearly as long. Among the things that make the new generation of instruments, and the IsoProbe in particular, unique are (1) the use of a gas-collision cell to reduce the energy spread of the ions and to remove ions associated with the plasma gas and (2) the introduction of multiple electron-multiplier detection systems. The net effect of these features is to increase sensitivity and precision. Historically uranium and plutonium isotopic compositions have been determined by thermal ionization mass spectrometry (TIMS). While requiring extensive sample preparation, no other technique matched its precision and sensitivity for such measurements. The purposes of this project are to evaluate whether the IsoProbe can replace TIMS for environmental monitoring analyses, whether it can extend the state-of-the-art to higher precision, and whether costs savings can be achieved at the same time.
Download or read book Development and Comparison of Analytical Methods for the Determination of Uranium and Plutonium in Spent Fuel and Environmental Samples written by Dina Solatie and published by . This book was released on 2002 with total page 54 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Radiometric Method for the Determination of Uranium in Water written by Carl Thomas Bishop and published by . This book was released on 1979 with total page 64 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Determination of Pu 239 Th 232 and Natural Uranium Isotopic Concentrations in Biological Samples Using Photofission Track Analysis written by James Roswell Parry and published by . This book was released on 2005 with total page 308 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book NUSIMEP 8 Uranium and Plutonium Isotope Amount Ratios in Low level Synthetic Nitrate Solution written by and published by . This book was released on 2014 with total page 54 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Use of Eichrom s TRU Resin in the Determination of Americium Plutonium and Uranium in Air Filter and Water Samples written by Anna Berne and published by . This book was released on 1995 with total page 28 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Advancing the Analysis of Low Level Uranium and Plutonium in Bioassay Samples Using SF ICP MS written by Jade Danielle Burraston and published by . This book was released on 2015 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Staatistische Wohl gegr ndte Glaubens Articul written by and published by . This book was released on 1704 with total page 8 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Analysis of Uranium and Plutonium by MC ICPMS written by R. W. Williams and published by . This book was released on 2005 with total page 11 pages. Available in PDF, EPUB and Kindle. Book excerpt: This procedure is written as general guidance for the measurement of elemental isotopic composition by plasma-source inorganic mass spectrometry. Analytical methods for uranium and plutonium are given as examples.
Download or read book Environmental Radiochemical Analysis II written by Peter Warwick and published by Royal Society of Chemistry. This book was released on 2007-10-31 with total page 434 pages. Available in PDF, EPUB and Kindle. Book excerpt: Environmental Radiochemical Analysis II brings together comprehensive, up-to-date information from international experts in the field. Coverage includes information on new methods of radionuclide analyses, developments and improvements in existing methods, method comparisons, gamma detector performance and new software products, method uncertainty, underground laboratory facilities, method QA and QC, field studies covering colloid work, in-situ injection into rock strata and sampling of reduced waters for actinide assay. This stimulating, authoritative text makes essential reading for practising radioanalysts and provides valuable information for researchers and professionals in academia and industry.
Download or read book Environmental Radiochemical Analysis II written by Peter Warwick (Prof.) and published by . This book was released on 2003 with total page 440 pages. Available in PDF, EPUB and Kindle. Book excerpt: Development of an In-Vitro Procedure to Measure the Availability of Soil-Associated Radionuclides for Uptake After Inadvertent Ingestion by Humans; Separation of Iron-55/59 From Fisson and Activation Products Using Di Isobutylketone-Based Extraction Chromatographic Materials; Synthesis of a Novel Ion Exchanger, Zirconium Vanadate, For Immobilising 134,137 Cs Radionuclides; Investigation of a Method for Measuring Radon in Irish Domestic Groundwater Supplies; A comparison of Three Methodologies for the Determination of Gross Alpha Activity in Water Samples; Efficiency and Resolution of Germanium Detectors as a Function of Energy and Incident Geometry; New Method for Determination of Translutonium Isotopes by Using a PM-143 Tracer; Ultra Low-Background Gamma Spectrometry for the Monitoring of Environmental Neutrons; Estimation of Uncertainty in Radiochemical Analysis from Sub-Sampling Solid Matrices; A Rapid Determination of RA-226 and RA-224 Using Extraction Chromatograph; Construction of an Uncertainty Budget for Alpha Spectrometry: A Case Study (The Determination of Uranium Isotopic Activity Levels in Vegetation Samples Using Extraction Chromatography); Spatial and Temporal Variation of Tritium Activities in Coastal Marine Sediments of the Severn Estuary (UK); High Precision PU Isotope Ratio Measurements Using Multi-Collector ICP-MS; Measurement of Gross Alpha and Gross Beta Activity in Sediment: An Analysts' Intercomparison; The Radiological Significance of Foods Collected from the Wild; Natural Radionuclides Measurements in Drinking Water by Liquid Scintillation Counting. Methods and Results; Po Concentrations in UK Seafood; A Study of Colloids in the Near-Field Waters at the Low-Level Waste Repository Site at Drigg; Low Level Liquid Scintillation Counting in a Deep Underground Laboratory: Background Reduction Aspects; Complete Dissolution of Soil Samples by Fusion; LSC: From the Routine Counter to the Real Spectrometer; Simultaneous Determination of Long-Lived Radionuclides in Environmental Samples; Analysis of Am, Pu and Th in Large Volume Water Samples in the Presence of High Concentrations of Iron; In-Situ Radionuclide Retardation in Groundwater Conducting Systems - Overview of the Research Carried out at Nagra's Grimsel Test Site, Central Switzerland; Elution Behaviour of Technetium and Rehenium Through a Tc-Selective Chromatographic Resin Column; The Use of Fucus Vesiculosus to Monitor the Transport of 1291 in The English Channel; Determination of 237 Np by Neutron Activation Analysis and Alpha Sepctrometry; Man-Made Radionuclides in Age-Dated Sediment Cores from the Black Sea; Determination of Plutonium in the Air by Isotopic Dilution ICP-MS After TNOA Extraction Chromatographic Separation; Simple Method for C-14 Analysis in Organic Material and its Distribution in Forest and Cultivated Field; F-Labelling of Humic Substances; Chemicals and Radiological Characterisation of Santos Estuary Sediments; Thermochromatographic Studies on the Separation of Plutonium from Soil Samples; Partitioning of Plutonium Isotopes in Lake Bottom Sediments; Radioanalytical Method for the Determination of Sr In Soil Samples by Yttrium Solvent Extraction and Cerenkov Counting; Investigation of Inorganic Contaminants in Packaging Made From Recycled Paper and Board; Equilibrium Factor F and Effective Dose Equivalent with Solid State Nuclear Track Detectors; Biological Monitoring of Radioactivity and Metal Pollution in Edible Eggs of Liometopum apiculatum (Ants) From a Radioactive Waste Site in Central Mexico; Preparation of Environmental Samples for Radioanalytical Assay: An Overview; Comparative Investigations on Hydrophilicity and Mobility of Humic Substances Using Radiolabelling Techniques; Determination of Gross Alpha in Drinking Water and Nuclear Waste Water Using Actinide Resinâ⢠and LSC; Chromium Speciation in Acidic Solutions Using Radiochromtographic Methods; Influence of Geochemical Paramete
Download or read book Handbook of Radioactivity Analysis written by Michael F. L'Annunziata and published by Academic Press. This book was released on 2012-09-01 with total page 1419 pages. Available in PDF, EPUB and Kindle. Book excerpt: The updated and much expanded 3e of the Handbook of Radioactivity Analysis is an authoritative reference providing the principles, practical techniques, and procedures for the accurate measurement of radioactivity from the very low levels encountered in the environment to higher levels measured in radioisotope research, clinical laboratories, biological sciences, radionuclide standardization, nuclear medicine, nuclear power, and fuel cycle facilities and in the implementation of nuclear forensic analysis and nuclear safeguards. The book describes the basic principles of radiation detection and measurement and the preparation of samples from a wide variety of matrices, assists the investigator or technician in the selection and use of appropriate radiation detectors, and presents state-of-the-art methods of analysis. Fundamentals of radiation properties, radionuclide decay, the calculations involved, and methods of detection provide the basis for a thorough understanding of the analytical procedures. The Handbook of Radioactivity Analysis, 3e, is suitable as a teaching text for university and professional training courses. - The only comprehensive reference that describes the principles of detection and practical applications of every type of radioactivity detector currently used. The new 3e is broader in scope, with revised and expanded chapters, new authors, and seven new chapters on Alpha Spectrometry, Radionuclide Standardization, Radioactive Aerosol Measurements, Environmental Radioactivity Monitoring, Marine Radioactivity Analysis, Nuclear Forensic Analysis and Analytical Techniques in Nuclear Safeguards - Discusses in detail the principles, theory and practice applied to all types of radiation detection and measurement, making it useful for both teaching and research
Download or read book The Geochemistry of Stable Chlorine and Bromine Isotopes written by Hans Eggenkamp and published by Springer. This book was released on 2014-08-25 with total page 174 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book provides detailed information on the history, analysis and applications of chlorine and bromine isotope geochemistry. Chlorine and bromine are geochemically unique as they prefer to exist as single charged negative ions. For this reason isotope fractionation reflects mostly processes that are not related to changes in the redox state and this fractionation is generally modest. The book will describe the processes that are most easily detected using these isotopes. Also isotope variations, and processes that cause them, measured in oxidised species such as perchlorates and in organic molecules will be described in this book.
Download or read book Uranium series Geochemistry written by Bernard Bourdon and published by Walter de Gruyter GmbH & Co KG. This book was released on 2018-12-17 with total page 676 pages. Available in PDF, EPUB and Kindle. Book excerpt: Volume 52 of Reviews in Mineralogy and Geochemistry updates our knowledge of U-series geochemistry, offer an opportunity for non-specialists to understand its basic principles, and give us a view of the future of this active field of research. In this volume, for the first time, all the methods for determining the uranium and thorium decay chain nuclides in Earth materials are discussed. It was prepared in advance of a two-day short course (April 3-4, 2003) on U-series geochemistry, jointly sponsored by GS and MSA and presented in Paris, France prior to the joint EGS/AGU/EUG meeting in Nice.
Download or read book Inorganic Mass Spectrometry written by Sabine Becker and published by John Wiley & Sons. This book was released on 2008-02-28 with total page 514 pages. Available in PDF, EPUB and Kindle. Book excerpt: Providing an exhaustive review of this topic, Inorganic Mass Spectrometry: Principles and Applications provides details on all aspects of inorganic mass spectrometry, from a historical overview of the topic to the principles and functions of mass separation and ion detection systems. Offering a comprehensive treatment of inorganic mass spectrometry, topics covered include: Recent developments in instrumentation Developing analytical techniques for measurements of trace and ultratrace impurities in different materials This broad textbook in inorganic mass spectrometry, presents the most important mass spectrometric techniques used in all fields of analytical chemistry. By covering recent developments and advances in all fields of inorganic mass spectrometry, this text provides researchers and students with information to answer any questions on this topic as well as providing the basic fundamentals for understanding this potentially complex, but increasingly relevant subject.
Download or read book Modern Isotope Ratio Mass Spectrometry written by I. T. Platzner and published by John Wiley & Sons. This book was released on 1997-10-22 with total page 544 pages. Available in PDF, EPUB and Kindle. Book excerpt: I. T. Platzner Atomic Energy Commission, Israel Including contributions from instrument manufacturers! Geological aging, chemical reaction mechanism studies, determination of atomic weights and investigation of metabolic pathways-these are all examples of the truly diverse nature of isotope ratio mass spectrometry (IRMS). With applications in fields as far apart as analytical chemistry and astronomy, geochemistry and biomedical science, it is little wonder that this technique is becoming increasingly popular. In Modern Isotope Ratio Mass Spectrometry,the first comprehensive book written on the subject for twenty-five years, examples from all these areas, and many more,are given. All modern developments in this fascinating field are discussed with special attention paid to technical details and instrumentation. Features of the book include: * comprehensive element-by-element review including 94 elements * applications chapter which stresses multi-disciplinary nature of subject * instrumentation chapter with contributions from three leading industrialists on state-of-the-art instrumentation
Download or read book Advanced Mass Spectrometry for Food Safety and Quality written by and published by Elsevier. This book was released on 2015-05-08 with total page 733 pages. Available in PDF, EPUB and Kindle. Book excerpt: Advanced Mass Spectrometry for Food Safety and Quality provides information on recent advancements made in mass spectrometry-based techniques and their applications in food safety and quality, also covering the major challenges associated with implementing these technologies for more effective identification of unknown compounds, food profiling, or candidate biomarker discovery. Recent advances in mass spectrometry technologies have uncovered tremendous opportunities for a range of food-related applications. However, the distinctive characteristics of food, such as the wide range of the different components and their extreme complexity present enormous challenges. This text brings together the most recent data on the topic, providing an important resource towards greater food safety and quality. - Presents critical applications for a sustainable, affordable and safe food supply - Covers emerging problems in food safety and quality with many specific examples. - Encompasses the characteristics, advantages, and limitations of mass spectrometry, and the current strategies in method development and validation - Provides the most recent data on the important topic of food safety and quality
