Download or read book Spectroscopic Tools for the Analysis of Electrochemical Systems written by James McBreen and published by The Electrochemical Society. This book was released on 2002 with total page 208 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Electrochemical Impedance Spectroscopy written by Mark E. Orazem and published by John Wiley & Sons. This book was released on 2011-10-13 with total page 510 pages. Available in PDF, EPUB and Kindle. Book excerpt: Using electrochemical impedance spectroscopy in a broad range of applications This book provides the background and training suitable for application of impedance spectroscopy to varied applications, such as corrosion, biomedical devices, semiconductors and solid-state devices, sensors, batteries, fuel cells, electrochemical capacitors, dielectric measurements, coatings, electrochromic materials, analytical chemistry, and imaging. The emphasis is on generally applicable fundamentals rather than on detailed treatment of applications. With numerous illustrative examples showing how these principles are applied to common impedance problems, Electrochemical Impedance Spectroscopy is ideal either for course study or for independent self-study, covering: Essential background, including complex variables, differential equations, statistics, electrical circuits, electrochemistry, and instrumentation Experimental techniques, including methods used to measure impedance and other transfer functions Process models, demonstrating how deterministic models of impedance response can be developed from physical and kinetic descriptions Interpretation strategies, describing methods of interpretating of impedance data, ranging from graphical methods to complex nonlinear regression Error structure, providing a conceptual understanding of stochastic, bias, and fitting errors in frequency-domain measurements An overview that provides a philosophy for electrochemical impedance spectroscopy that integrates experimental observation, model development, and error analysis This is an excellent textbook for graduate students in electrochemistry, materials science, and chemical engineering. It's also a great self-study guide and reference for scientists and engineers who work with electrochemistry, corrosion, and electrochemical technology, including those in the biomedical field, and for users and vendors of impedance-measuring instrumentation.
Download or read book Tip enhanced Raman Spectroscopy on Electrochemical Systems written by Thomas Touzalin and published by . This book was released on 2018 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: The in situ investigation of electrochemical interfaces structures at the nanoscale is a key element in the understanding of charge and electron transfer mechanisms e.g. in the fields of energy storage or electrocatalysis. This thesis introduces the implementation of tip-enhanced Raman spectroscopy (TERS) in liquid and in electrochemical conditions enabling the nanoscale analysis of electrified solid/liquid interfaces through the strong and local electric field enhancement at gold or silver scanning tunneling microscopy (STM) probes. The ability of TERS to image inhomogeneities in the coverage density of a self-assembled monolayer (SAM) through a layer of organic solvent on gold was demonstrated. A TERS-inspired analytical tool was also developed, based on a TERS tip used simultaneously as a single-hot spot surface-enhanced Raman spectroscopy (SERS) platform and as a microelectrode (EC tip SERS). The reduction of an electroactive SAM could then be monitored by electrochemical and in situ SERS measurements. In situ electrochemical STM-TERS was also evidenced through the imaging of local variations of the electric field enhancement on peculiar sites of a gold electrode with a lateral resolution lower than 8 nm. Finally TERS also demonstrated to be efficient in investigating the structure of organic layers grafted either by electrochemical reduction or spontaneously. This work is therefore a major advance for the analysis of functionalized surfaces.
Download or read book Nonaqueous Electrochemistry written by Doron Aurbach and published by CRC Press. This book was released on 1999-07-27 with total page 980 pages. Available in PDF, EPUB and Kindle. Book excerpt: An examination of applications of electrochemical techniques to many organic and inorganic compounds that are either unstable or insoluble in water. It focuses on the continuing drive toward miniaturization in electronics met by designs for high-energy density batteries (based on nonaqueous systems). It addresses applications to nonaqueous batteries, supercapacitators, highly sensitive reagents, and electroorganic and electroinorganic synthesis.
Download or read book Developments in Electrochemistry written by Derek Pletcher and published by John Wiley & Sons. This book was released on 2014-08-11 with total page 392 pages. Available in PDF, EPUB and Kindle. Book excerpt: Martin Fleischmann was truly one of the ‘fathers’ of modern electrochemistry having made major contributions to diverse topics within electrochemical science and technology. These include the theory and practice of voltammetry and in situ spectroscopic techniques, instrumentation, electrochemical phase formation, corrosion, electrochemical engineering, electrosynthesis and cold fusion. While intended to honour the memory of Martin Fleischmann, Developments in Electrochemistry is neither a biography nor a history of his contributions. Rather, the book is a series of critical reviews of topics in electrochemical science associated with Martin Fleischmann but remaining important today. The authors are all scientists with outstanding international reputations who have made their own contribution to their topic; most have also worked with Martin Fleischmann and benefitted from his guidance. Each of the 19 chapters within this volume begin with an outline of Martin Fleischmann’s contribution to the topic, followed by examples of research, established applications and prospects for future developments. The book is of interest to both students and experienced workers in universities and industry who are active in developing electrochemical science.
Download or read book Fast Electrochemical Impedance Spectroscopy written by Pavle Boškoski and published by Springer. This book was released on 2017-05-07 with total page 90 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book offers a review of electrochemical impedance spectroscopy (EIS) and its application in online condition monitoring of electrochemical devices, focusing on the practicalities of performing fast and accurate EIS. The first part of the book addresses the theoretical aspects of the fast EIS technique, including stochastic excitation signals, time-frequency signal processing, and statistical analysis of impedance measurements. The second part presents an application of the fast EIS technique for condition monitoring and evaluates the performance of the proposed fast EIS methodology in three different types of electrochemical devices: a Li-ion battery, a Li-S cell, and a polymer electrolyte membrane (PEM) fuel cell. Uniquely, in addition to theoretical aspects the book provides practical guidelines for implementation, commissioning, and exploitation of EIS for condition monitoring of electrochemical devices, making it a valuable resource for practicing engineers as well as researchers.
Download or read book Impedance Spectroscopy written by Evgenij Barsoukov and published by John Wiley & Sons. This book was released on 2005-03-18 with total page 615 pages. Available in PDF, EPUB and Kindle. Book excerpt: A skillful balance of theoretical considerations and practical know-how Backed by a team of expert contributors, the Second Edition of this highly acclaimed publication brings a solid understanding of impedance spectroscopy to students, researchers, and engineers in physical chemistry, electrochemistry, and physics. Starting with general principles, the book moves on to explain in detail practical applications for the characterization of materials in electrochemistry, semiconductors, solid electrolytes, corrosion, solid-state devices, and electrochemical power sources. The book covers all of the topics needed to help readers identify whether impedance spectroscopy may be an appropriate method for their particular research problem. The book helps readers quickly grasp how to apply their new knowledge of impedance spectroscopy methods to their own research problems through the use of unique features such as: * Step-by-step instructions for setting up experiments and then analyzing the results * Theoretical considerations for dealing with modeling, equivalent circuits, and equations in the complex domain * Best measurement methods for particular systems and alerts to potential sources of errors * Equations for the most widely used impedance models * Figures depicting impedance spectra of typical materials and devices * Extensive references to the scientific literature for more information on particular topics and current research This Second Edition incorporates the results of the last two decades of research on the theories and applications of impedance spectroscopy. Most notably, it includes new chapters on batteries, supercapacitors, fuel cells, and photochromic materials. A new chapter on commercially available measurement systems reflects the emergence of impedance spectroscopy as a mainstream research tool. With its balanced focus on both theory and practical problem solving, Impedance Spectroscopy: Theory, Experiment, and Applications, Second Edition serves as an excellent graduate-level textbook as well as a hands-on guide and reference for researchers and engineers.
Download or read book Electrochemical Impedance written by John R. Scully and published by ASTM International. This book was released on 1993 with total page 477 pages. Available in PDF, EPUB and Kindle. Book excerpt: The collection of twenty-seven papers published has been grouped into six major categories : corrosion process characterization and modeling, applications of Kramers-Kronig transformations for evaluating the validity of data, corrosion and its inhibition by either corrosion products of specially added inhibitors, corrosion of aluminum and aluminum alloys, corrosion of steel in soils and concrete, and evaluation of coatings on metal substrates.
Download or read book Springer Handbook of Electrochemical Energy written by Cornelia Breitkopf and published by Springer. This book was released on 2016-12-05 with total page 1019 pages. Available in PDF, EPUB and Kindle. Book excerpt: This comprehensive handbook covers all fundamentals of electrochemistry for contemporary applications. It provides a rich presentation of related topics of electrochemistry with a clear focus on energy technologies. It covers all aspects of electrochemistry starting with theoretical concepts and basic laws of thermodynamics, non-equilibrium thermodynamics and multiscale modeling. It further gathers the basic experimental methods such as potentiometry, reference electrodes, ion-sensitive electrodes, voltammetry and amperometry. The contents cover subjects related to mass transport, the electric double layer, ohmic losses and experimentation affecting electrochemical reactions. These aspects of electrochemistry are especially examined in view of specific energy technologies including batteries, polymer electrolyte and biological fuel cells, electrochemical capacitors, electrochemical hydrogen production and photoelectrochemistry. Organized in six parts, the overall complexity of electrochemistry is presented and makes this handbook an authoritative reference and definitive source for advanced students, professionals and scientists particularly interested in industrial and energy applications.
Download or read book New Trends in Electrochemical Impedance Spectroscopy EIS and Electrochemical Noise Analysis ENA written by Florian Mansfeld and published by The Electrochemical Society. This book was released on 2001 with total page 282 pages. Available in PDF, EPUB and Kindle. Book excerpt: These 22 contributions concentrate primarily on newer applications of the staple EIS technique, and secondarily, on the more recent use of ENA in corrosion research. Papers treat experimental aspects of EIS and data analysis; EIS for investigating the protective properties and degradation of polymer coatings; and EIS in combination with other techniques to study specific corrosion phenomena, e.g., the corrosive rates of steel in soil environments. Mansfeld (U. of Southern California), et al., describe the use of both techniques to monitor the corrosion behavior of active and passive systems exposed to chloride media. The volume includes facts about the Electrochemical Society. Annotation copyrighted by Book News Inc., Portland, OR.
Download or read book Electrochemical Impedance Spectroscopy written by Marwa El-Azazy and published by BoD – Books on Demand. This book was released on 2020-12-16 with total page 169 pages. Available in PDF, EPUB and Kindle. Book excerpt: Electrochemical Impedance Spectroscopy is a compendium of contributions from experts in the field of electrochemical impedance spectroscopy (EIS). This compilation of investigations and reviews addresses the groundbreaking applications of EIS in different fields. An array of exploitations are revealed throughout this book such as the use of EIS in monitoring and controlling of corrosion, in medicine where accurate information on fluid distribution is needed as well as environmental applications in food, water, and drug analyses. Competency of EIS as an approach compared to the traditional electrochemical techniques is assessed in almost every application. This book, therefore, is a valuable reference for students, researchers, and anyone interested in electrochemical impedance spectroscopy.
Download or read book Springer Handbook of Inorganic Photochemistry written by Detlef Bahnemann and published by Springer Nature. This book was released on 2022-06-25 with total page 1914 pages. Available in PDF, EPUB and Kindle. Book excerpt: The handbook comprehensively covers the field of inorganic photochemistry from the fundamentals to the main applications. The first section of the book describes the historical development of inorganic photochemistry, along with the fundamentals related to this multidisciplinary scientific field. The main experimental techniques employed in state-of-art studies are described in detail in the second section followed by a third section including theoretical investigations in the field. In the next three sections, the photophysical and photochemical properties of coordination compounds, supramolecular systems and inorganic semiconductors are summarized by experts on these materials. Finally, the application of photoactive inorganic compounds in key sectors of our society is highlighted. The sections cover applications in bioimaging and sensing, drug delivery and cancer therapy, solar energy conversion to electricity and fuels, organic synthesis, environmental remediation and optoelectronics among others. The chapters provide a concise overview of the main achievements in the recent years and highlight the challenges for future research. This handbook offers a unique compilation for practitioners of inorganic photochemistry in both industry and academia.
Download or read book An Introduction to Electrochemical Impedance Spectroscopy written by Ramanathan Srinivasan and published by CRC Press. This book was released on 2021-05-03 with total page 263 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book covers the fundamental aspects and the application of electrochemical impedance spectroscopy (EIS), with emphasis on a step-by-step procedure for mechanistic analysis of data. It enables the reader to learn the EIS technique, correctly acquire data from a system of interest, and effectively interpret the same. Detailed illustrations of how to validate the impedance spectra, use equivalent circuit analysis, and identify the reaction mechanism from the impedance spectra are given, supported by derivations and examples. MATLAB® programs for generating EIS data under various conditions are provided along with free online video lectures to enable easier learning. Features: Covers experimental details and nuances, data validation method, and two types of analysis – using circuit analogy and mechanistic analysis Details observations such as inductive loops and negative resistances Includes a dedicated chapter on an emerging technique (Nonlinear EIS), including code in the supplementary material illustrating simulations Discusses diffusion, constant phase element, porous electrodes, and films Contains exercise problems, MATLAB codes, PPT slide, and illustrative examples This book is aimed at senior undergraduates and advanced graduates in chemical engineering, analytical chemistry, electrochemistry, and spectroscopy.
Download or read book Electrochemical Systems written by John Newman and published by John Wiley & Sons. This book was released on 2021-01-07 with total page 608 pages. Available in PDF, EPUB and Kindle. Book excerpt: Provides a comprehensive understanding of a wide range of systems and topics in electrochemistry This book offers complete coverage of electrochemical theories as they pertain to the understanding of electrochemical systems. It describes the foundations of thermodynamics, chemical kinetics, and transport phenomena—including the electrical potential and charged species. It also shows how to apply electrochemical principles to systems analysis and mathematical modeling. Using these tools, the reader will be able to model mathematically any system of interest and realize quantitative descriptions of the processes involved. This brand new edition of Electrochemical Systems updates all chapters while adding content on lithium battery electrolyte characterization and polymer electrolytes. It also includes a new chapter on impedance spectroscopy. Presented in 4 sections, the book covers: Thermodynamics of Electrochemical Cells, Electrode Kinetics and Other Interfacial Phenomena, Transport Processes in Electrolytic Solutions, and Current Distribution and Mass Transfer in Electrochemical Systems. It also features three appendixes containing information on: Partial Molar Volumes, Vectors and Tensors, and Numerical Solution of Coupled, Ordinary Differential Equations. Details fundamental knowledge with a thorough methodology Thoroughly updated throughout with new material on topics including lithium battery electrolyte characterization, impedance analysis, and polymer electrolytes Includes a discussion of equilibration of a charged polymer material and an electrolytic solution (the Donnan equilibrium) A peerless classic on electrochemical engineering Electrochemical Systems, Fourth Edition is an excellent resource for students, scientists, and researchers involved in electrochemical engineering.
Download or read book In situ Spectroscopic Studies of Adsorption at the Electrode and Electrocatalysis written by Shi-Gang Sun and published by Elsevier. This book was released on 2011-08-11 with total page 559 pages. Available in PDF, EPUB and Kindle. Book excerpt: In-Situ Spectroscopic Studies of Adsorption at the Electrode and Electrocatalysis is a new reference on in-situ spectroscopic techniques/applications, fundamentals of electrocatalysis at molecule level, and progresses within electrochemical surface science. Presenting both essential background knowledge at graduate level and original research within the fields of spectroscopy, electrochemistry, and surface science. Featuring 15 chapters by prominent worldwide scholars, based on their recent progress in different aspects of in-situ spectroscopy studies, this book will appeal to a wide audience of scientists. In summary this book is highly suitable for graduates learning basic concepts and advanced applications of in-situ spectroscopy, electrocatalysis and electrode adsorptions.* Written by the most active scientists in the fields of spectroscopy, electrochemistry and surface science* Essential background knowledge for graduate students* A modern reference of cutting-edge scientific research
Download or read book Scaling Up of Microbial Electrochemical Systems written by Dipak Ashok Jadhav and published by Elsevier. This book was released on 2022-01-28 with total page 514 pages. Available in PDF, EPUB and Kindle. Book excerpt: Scaling Up of Microbial Electrochemical Systems: From Reality to Scalability is the first book of its kind to focus on scaling up of microbial electrochemical systems (MES) and the unique challenges faced when moving towards practical applications using this technology. This book emphasizes an understanding of the current limitations of MES technology and suggests a way forward towards onsite applications of MES for practical use. It includes the basics of MES as well as success stories and case studies of MES in the direction of practical applications. This book will give a new direction to energy researchers, scientists and policymakers working on field applications of microbial electrochemical systems—microbial fuel cells, microbial electrolysis cells, microbial electrosynthesis cells, and more. - Promotes the advancement of microbial electrochemical systems, from lab scale to field applications - Illustrates the challenges of scaling up using successive case studies - Provides the basics of MES technology to help deepen understanding of the subject - Addresses lifecycle analysis of MES technology to allow comparison with other conventional methods
Download or read book An Electrochemical Impedance Spectroscopic Diagnostic Device for Characterization of Liquid liquid Systems and Phase Separation Detection in Emulsions written by Seyedehsan Shahidi and published by . This book was released on 2013 with total page 197 pages. Available in PDF, EPUB and Kindle. Book excerpt: Rapid characterization of complex fluids, especially sensing emulsion stability, is crucial for many industrial applications, ranging from pharmaceutical industry to petroleum production. Electrochemical impedance spectroscopy (EIS) is a powerful tool for electrical characterization of such systems. In this study, a "milli-fluidic" EIS test fixture which is inexpensive, easily fabricated, yet robust, is designed and fabricated using 3D printing technology, which allows reliable experiments, and can then be disposed of after each test. The developed cell is tested using solutions, liquid-liquid mixtures, and oil-water emulsions. Frequency response analysis and equivalent circuit modeling have been performed to find the effective electrical properties of the liquids, and relate them to their physical properties, such as stability. EIS is applied to reveal the electrical behavior of emulsions during phase separation. It is found that creaming can be sensed based on permittivity decay, and capacitance-based measurements can be utilized to detect phase separation in emulsions.
