Download or read book Room Temperature Organic Synthesis written by Goutam Brahmachari and published by Elsevier. This book was released on 2015-03-19 with total page 388 pages. Available in PDF, EPUB and Kindle. Book excerpt: Filling a gap in the scientific literature, Room Temperature Organic Synthesis is unique in its authoritative, thorough, and applied coverage of a wide variety of "green" organic synthetic methodologies. The book describes practical, feasible protocols for room temperature reactions to produce carbon-carbon and carbon-heteroatom bond formations including aliphatic, aromatic, alicyclic, heterocycles, and more. Consistently organized for easy access, each selected reaction is discussed in a very compact and structured manner including: reaction type, reaction condition, reaction strategy, catalyst, keywords, general reaction scheme, mechanism (in selected cases), representative entries, experimental procedure, characterization data of representative entries, and references. This book will be a valuable resource for synthetic organic, natural products, medicinal, and biochemists as well as those working in the pharmaceutical and agrochemical industry. Includes more than 300 protocols for a green approach to organic synthesis Provides specific detail about experimental conditions Increases efficiency in the laboratory by eliminating time-consuming literature searches
Download or read book Mechanochemical Organic Synthesis written by Davor Margetic and published by Elsevier. This book was released on 2016-04-23 with total page 386 pages. Available in PDF, EPUB and Kindle. Book excerpt: Mechanochemical Organic Synthesis is a comprehensive reference that not only synthesizes the current literature but also offers practical protocols that industrial and academic scientists can immediately put to use in their daily work. Increasing interest in green chemistry has led to the development of numerous environmentally-friendly methodologies for the synthesis of organic molecules of interest. Amongst the green methodologies drawing attention, mechanochemistry is emerging as a promising method to circumvent the use of toxic solvents and reagents as well as to increase energy efficiency. The development of synthetic strategies that require less, or the minimal, amount of energy to carry out a specific reaction with optimum productivity is of vital importance for large-scale industrial production. Experimental procedures at room temperature are the mildest reaction conditions (essentially required for many temperature-sensitive organic substrates as a key step in multi-step sequence reactions) and are the core of mechanochemical organic synthesis. This green synthetic method is now emerging in a very progressive manner and until now, there is no book that reviews the recent developments in this area. Features cutting-edge research in the field of mechanochemical organic synthesis for more sustainable reactions Integrates advances in green chemistry research into industrial applications and process development Focuses on designing techniques in organic synthesis directed toward mild reaction conditions Includes global coverage of mechanochemical synthetic protocols for the generation of organic compounds
Download or read book Organic Synthesis in Water written by P.A. Grieco and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 321 pages. Available in PDF, EPUB and Kindle. Book excerpt: The use of water as a medium for promoting organic reactions has been rather neglected in the development of organic synthesis, despite the fact that it is the solvent in which almost all biochemical processes take place. Chemists have only recently started to appreciate the enormous potential water has to offer in the development of new synthetic reactions and strategies, where it can offer benefits in both unique chemistry and reduced environmental impact. In this new book, the editor, well known for his contribution to the development of water as a useful medium in synthetic organic chemistry, has assembled an international team of authors, themselves at the forefront of research into the use of the unique properties of water carrying out organic transformations, to provide a timely and concise overview of current research. By focusing on the practical use of water in synthetic organic chemistry, and with the concern for the use of solvents in organic chemistry, professional chemists, particularly those involved in industrial research and development, will find this book an essential guide to the current state of the art, and a useful starting point in their own research. Academic chemists, including postgraduate and advanced undergraduate students, will find this book an invaluable guide to this exciting and important area of chemistry.
Download or read book Modern Organic Synthesis in the Laboratory written by Jie Jack Li and published by Oxford University Press. This book was released on 2007-09-10 with total page 224 pages. Available in PDF, EPUB and Kindle. Book excerpt: Searching for reaction in organic synthesis has been made much easier in the current age of computer databases. However, the dilemma now is which procedure one selects among the ocean of choices. Especially for novices in the laboratory, it becomes a daunting task to decide what reaction conditions to experiment with first in order to have the best chance of success. This collection intends to serve as an "older and wiser lab-mate" one could have by compiling many of the most commonly used experimental procedures in organic synthesis. With chapters that cover such topics as functional group manipulations, oxidation, reduction, and carbon-carbon bond formation, Modern Organic Synthesis in the Laboratory will be useful for both graduate students and professors in organic chemistry and medicinal chemists in the pharmaceutical and agrochemical industries.
Download or read book Solvent free Organic Synthesis written by Koichi Tanaka and published by John Wiley & Sons. This book was released on 2006-03-06 with total page 442 pages. Available in PDF, EPUB and Kindle. Book excerpt: The demand for increasingly clean and efficient chemical syntheses is continuously becoming more urgent from both an economic and an environmental standpoint. So-called green technologies are looking for alternatives, yet they focus on large quantities of hazardous even toxic solvents. One could even say that the best solvent is no solvent. It is against this background that chemical synthesis without the use of solvents has increasingly developed into a powerful methodology. Once the chemical reactivity is increased, the amount of initial substances needed is reduced; in particular it removes the need for the complex recycling and disposal of solvents. In this book, the third in our open "Green Chemistry" series, Koichi Tanaka describes the latest developments in this exciting field. Packed with advice on applications, this will be equally useful to practitioners in research as well as process chemists in industry, such that it is sure to become an invaluable reference source.
Download or read book Tellurium in Organic Synthesis written by Nicola Petragnani and published by Elsevier. This book was released on 2010-07-07 with total page 398 pages. Available in PDF, EPUB and Kindle. Book excerpt: The increasing number of publications that use tellurium clearly demonstrates the important role of tellurium compounds as unique and powerful tools in a broad range of organic chemical manipulations, often characterized by their selective behavior. Tellurium in Organic Synthesis provides an overview of the principal aspects of organic tellurium chemistry. Many chapters have been enriched and updated in this second edition. New chapters include overviews of toxicology and pharmacology and a review on the preparation and reactivity of several tellurium heterocycles. The first part of the book focuses on the preparation of selected inorganic tellurium compounds and on the main classes of organotellurium compounds. The second part, and main interest of the book, details the use of these inorganic and organic compounds as reagents to perform specific organic manipulations and synthesis. Reactions covered include reduction, formation and reaction of anionic species, deprotection, tellurium cyclizations, formation of alkenes, use of vinyllic tellurides, free radical chemistry, transmetallations, and removal of tellurium. Overview of inorganic and organic tellurium chemistry Synthetic applications of tellurium compounds All topics accompanied by detailed experimental procedures
Download or read book Catalyst free Organic Synthesis written by Goutam Brahmachari and published by Royal Society of Chemistry. This book was released on 2017-11-06 with total page 392 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Organic Synthesis Using Samarium Diiodide written by David J. Procter and published by Royal Society of Chemistry. This book was released on 2010 with total page 221 pages. Available in PDF, EPUB and Kindle. Book excerpt: Samarium diiodide is one of the most important reducing agents available to synthetic organic chemists. The lanthanide(II) reagent acts by single-electron transfer to organic substrates leading to the formation of both radical and/or anionic intermediates. The power of the reagent arises from its versatility - samarium diiodide can be used in processes ranging from functional group conversions to elaborate carbon-carbon bond-forming cyclization sequences that result in a dramatic increase in molecular complexity. In addition, reactions involving samarium diiodide often show high stereoselectivity as samarium ions can coordinate to Lewis basic sites on substrates and can direct the stereochemical course of reactions. The ability to fine-tune the reactivity of the reagent by the use of additives and co-solvents is an additional, attractive feature. Although samarium diiodide is used extensively by organic chemists, there is still a widely held view that the reagent can be difficult to prepare and use. In addition, samarium diiodide can mediate such a wide variety of organic chemistry that potential new users are often overawed by the extensive primary literature on the reagent. The objective of this book is to provide a concise, practical guide to the reagent. Rather than being a comprehensive review of the chemistry of samarium diiodide, this user-friendly book adopts an "an all you need to know" approach to the topic. The international authors are well-known for their work with the reagent and their expertise covers current developments in new reactivity and selectivity, applications in target synthesis, co-solvent and additive effects, coordination chemistry and mechanism. The book includes the best methods for preparing and handling the reagent, how solvents, co-solvents and additives alter reactivity, the basic mechanisms of reactions, common transformations using the reagent, and emerging areas in samarium diiodide chemistry. The authors have distilled the extensive primary literature to allow the reader to quickly grasp an understanding of the reagent and its utility. The illustrative practical procedures help the reader to prepare and use the reagent in the laboratory while references from the recent literature allow readers to pursue their interest in the popular reagent. The book also contains many illustrations and chemical schemes.
Download or read book Solvent free Organic Synthesis written by Koichi Tanaka and published by John Wiley & Sons. This book was released on 2009-03-02 with total page 476 pages. Available in PDF, EPUB and Kindle. Book excerpt: In this second edition of a best-selling handbook all the chapters have been completely revised and updated, while four completely new chapters have been added. In order to meet the needs of the practitioner, emphasis is placed on describing precisely the technology and know-how involved. Adopting a didactic and comprehensible approach, the book guides the reader through theory and applications, thus ensuring its warm welcome among the scientific community. An excellent, essential and exhaustive overview.
Download or read book Advanced Organic Synthesis written by Dmitry V. Liskin and published by CRC Press. This book was released on 2015-11-04 with total page 131 pages. Available in PDF, EPUB and Kindle. Book excerpt: Laboratory experience equips students with techniques that are necessary for professional practice. Advanced Organic Synthesis: A Laboratory Manual focuses on a mechanistic background of key reactions in organic chemistry, gives insight into well-established trends, and introduces new developments in the field.The book features experiments performe
Download or read book High Pressure Organic Synthesis written by Davor Margetic and published by Walter de Gruyter GmbH & Co KG. This book was released on 2019-07-08 with total page 326 pages. Available in PDF, EPUB and Kindle. Book excerpt: High pressure chemistry is a widely used methodology in organic synthesis which helps to increase the rate and to improve the efficiency of chemical processes. The current publication outlines the impact of pressure on many types of chemical reactions important from synthetic point of view and gives practical considerations how to plan and perform synthetic experiments under high pressure in the lab.
Download or read book Sustainable Catalysis written by Rafael Luque and published by John Wiley & Sons. This book was released on 2018-05-07 with total page 292 pages. Available in PDF, EPUB and Kindle. Book excerpt: Highlighting sustainable catalytic processes in synthetic organic chemistry and industry, this useful guide places special emphasis on catalytic reactions carried out at room temperature. It describes the fundamentals, summarizes key advances, and covers applications in industrial processes in the field of energy generation from renewables, food science, and pollution control. Throughout, the latest research from various disciplines is combined, such as homogeneous and heterogeneous catalysis, biocatalysis, and photocatalysis. The book concludes with a chapter on future trends and energy challenges for the latter half of the 21st century. With its multidisciplinary approach this is an essential reference for academic and industrial researchers in catalysis science aiming to design more sustainable and energy-efficient processes.
Download or read book Distinctive Techniques for Organic Synthesis written by Tse-Lok Ho and published by World Scientific. This book was released on 1998-06-23 with total page 400 pages. Available in PDF, EPUB and Kindle. Book excerpt: This important book is intended to familiarize the practitioner of synthetic chemistry with somewhat extraordinary techniques which should prove very helpful to his or her work. It covers some reactions or techniques for organic synthesis which are not found in most introductory texts. They include reactions under high pressure, mediated by ultrasonic, flash vacuum pyrolysis, photochemical processes, phase transfer reactions, electrochemical reactions, and reactions on solid supports. The emphasis of the book is on applications. Examples are often drawn from significant contributions, such as natural product syntheses. Contents:Phase Transfer ReactionsReactions with Solid-Supported Reagents and CatalystsSonochemistryHigh Pressure ReactionsFlash Vacuum Pyrolysis and Some Other Thermal ProcessesElectroorganic TransformationsOrganic Photochemistry Readership: Organic chemists. keywords:
Download or read book Organic Synthesis at High Pressures written by Kiyoshi Matsumoto and published by Wiley-Interscience. This book was released on 1991-04-12 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presented here is a state-of-the-art examination of organic syntheses at high pressures designed to help synthetic organic chemists decide whether high pressure technology, with its advantages and limitations, might or might not be useful in solving their current problems. Following the introduction, chapters cover the basic principles, mechanisms, apparatus and operation of using high pressure technology. Further explores specific reactions and how they relate to various chemical compounds under high pressure.
Download or read book Versatile Precursors in Organic Synthesis written by Okram Mukherjee Singh and published by Cambridge Scholars Publishing. This book was released on 2022-09-23 with total page 387 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book elaborates on the synthesis of versatile precursors and their applications in organic synthesis through a systematic approach. It shows that understanding the chemical properties of different types of versatile building blocks is essential for the successful execution of organic synthesis. The text also discusses how a particular type of precursor is used in the preparation of different types of simple and complex organic compounds, depending on reaction conditions and other substrates.
Download or read book Microwave assisted Organic Synthesis written by D. Bogdal and published by Elsevier. This book was released on 2006-01-04 with total page 215 pages. Available in PDF, EPUB and Kindle. Book excerpt: Microwave-assisted Organic Synthesis: One Hundred Reaction Procedures provides readers with a broad overview of microwave assisted Organic Synthesis, enabling students and researchers alike to produce more efficient and high yield syntheses while saving time and resources. The work addresses key problems faced by chemistry laboratories in academia and in industry, that of an ever increasing need for procedures which are low-waste, energy efficient, high yield, occur over a short reaction period, and use environmentally friendly solvents. All these factors play an important role in the development of Green Chemistry methods, and in this, Microwave-assisted Organic Synthesis: One Hundred Reaction Procedures is an excellent resource for any library. Provides a broad overview of microwave enhanced chemistry Extensive references to the source of each procedure, including equipment used, full operating procedure, and associated hazards Includes exercises and worked problems which can support more independent study
Download or read book Photochemical Key Steps in Organic Synthesis written by Jochen Mattay and published by John Wiley & Sons. This book was released on 2008-07-11 with total page 361 pages. Available in PDF, EPUB and Kindle. Book excerpt: Basic laboratory technique in organic chemistry plays a vital part in the education of chemistry students. This textbook contains a collection of multistep experiments that all feature one or two photochemical key steps. More than 40 researchers active in the field of organic photochemistry have contributed their favorite experiments for this unusual and modern textbook. In addition, a general section discusses reaction control, the interpretation of UV spectra, quantum yields and chemical yields, and gives information on solvents, lamps, filters, and vessels. The experiments chosen fulfil the following criteria: * starting materials are cheap and readily available * the necessary photochemical equipment is available in (most) institutes * products prepared are useful for further syntheses * the light reaction is efficient. 'Photochemical Key Steps' is a source book of new ideas for supervisors of lab courses and gives students the opportunity to learn about modern techniques in the laboratory and about the important role photochemistry plays in organic synthesis.
