Download or read book Nuclear Magnetic Resonance Spin Dynamics in Solids written by and published by . This book was released on 1974 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Spin Dynamics written by Malcolm H. Levitt and published by John Wiley & Sons. This book was released on 2013-05-20 with total page 824 pages. Available in PDF, EPUB and Kindle. Book excerpt: Spin Dynamics: Basics of Nuclear Magnetic Resonance, Second Edition is a comprehensive and modern introduction which focuses on those essential principles and concepts needed for a thorough understanding of the subject, rather than the practical aspects. The quantum theory of nuclear magnets is presented within a strong physical framework, supported by figures. The book assumes only a basic knowledge of complex numbers and matrices, and provides the reader with numerous worked examples and exercises to encourage understanding. With the explicit aim of carefully developing the subject from the beginning, the text starts with coverage of quarks and nucleons and progresses through to a detailed explanation of several important NMR experiments, including NMR imaging, COSY, NOESY and TROSY. Completely revised and updated, the Second Edition features new material on the properties and distributions of isotopes, chemical shift anisotropy and quadrupolar interactions, Pake patterns, spin echoes, slice selection in NMR imaging, and a complete new chapter on the NMR spectroscopy of quadrupolar nuclei. New appendices have been included on Euler angles, and coherence selection by field gradients. As in the first edition, all material is heavily supported by graphics, much of which is new to this edition. Written for undergraduates and postgraduate students taking a first course in NMR spectroscopy and for those needing an up-to-date account of the subject, this multi-disciplinary book will appeal to chemical, physical, material, life, medical, earth and environmental scientists. The detailed physical insights will also make the book of interest for experienced spectroscopists and NMR researchers. • An accessible and carefully written introduction, designed to help students to fully understand this complex and dynamic subject • Takes a multi-disciplinary approach, focusing on basic principles and concepts rather than the more practical aspects • Presents a strong pedagogical approach throughout, with emphasis placed on individual spins to aid understanding • Includes numerous worked examples, problems, further reading and additional notes Praise from the reviews of the First Edition: "This is an excellent book... that many teachers of NMR spectroscopy will cherish... It deserves to be a ‘classic’ among NMR spectroscopy texts." NMR IN BIOMEDICINE "I strongly recommend this book to everyone...it is probably the best modern comprehensive description of the subject." ANGEWANDTE CHEMIE, INTERNATIONAL EDITION
Download or read book Pulsed Nuclear Magnetic Resonance and Spin Dynamics in Solids written by J. W. Hennel and published by . This book was released on 1973 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Pulsed Nuclear Magnetic Resonance and Spin Dynamics in Solids written by Jacek W. Hennel and published by . This book was released on 1973 with total page 278 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Transient Techniques in NMR of Solids written by Bernard C. Gerstein and published by . This book was released on 1985 with total page 320 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume is an ideal starting point for the graduate student seeking a basic introduction to the theory and uses of solid-state nuclear magnetic resonance (NMR) spectroscopy. Accessible to students with only a survey-level physics background, the material assumes little prior knowledge of the basic theory of electromagnetism. All the major areas are covered, including an introduction to concepts of time-dependent quantum mechanics as they apply to NMR spectroscopy of the solid state. Each chapter includes problems designed to enhance the reader's understanding of the material. Instructive and practical, this volume provides the basic knowledge needed to access the general literature and the more advanced monographs on this subject. In addition to assisting entrance into the field, Transient Techniques in NMR of Solids will be a useful guide for professionals already working in related areas of chemistry. FROM THE PREFACE: Nuclear magnetic resonance (NMR) is truly a remarkable phenomenon. Remarkable can imply different things to different people. From the point of view of a physicist, spin dynamics is an elegant example of the use of time-dependent quantum mechanics, and NMR absorption of energy is a prototype for spectroscopic transitions. From the point of view of the practicing chemist and materials scientist, NMR spectroscopy is an invaluable tool for the identification of chemical species and structures. Had NMR spectroscopic techniques commercially available in the early 1960s been the only result of investigations of this phenomenon, it would have had a major impact on the course of chemical analysis. The study of liquids and solutions for chemical shifts and couplings of protons had produced a rapid means of identifying chemical species nondestructively. The study of dynamical properties also could be addressed by study of temperature dependence of the spectra or of the saturation of the resonance by high-power irradiation. Even at that time, however, studies of the spin dynamics had already begun to indicate that there were many interesting facets of the NMR phenomenon left to exploit. For example, the Fourier-transform relationship of the free-induction decay and the absorption spectrum had been shown and the basis of the cross-polarization experiment was being investigated. A number of chemists had begun to study the spin*b1lattice relaxation times of species by pulse NMR techniques by utilizing methods that were not familiar at that time to the typical chemist but that are now commonly employed in NMR analysis. The principal characteristic of the NMR technique that makes it so useful for chemical analysis of liquids and solutions is the high resolution that allows one to observe very small interactions such as the chemical shift and the spin*b1spin coupling. These weak interactions are quite sensitive to the local environment of the spin and therefore may be used as a diagnostic for the environment. The connectivity of chemical structure is often mimicked closely in the NMR connectivity of the spectrum, and quantitative informaton is relatively easy to obtain. Nuclear magnetic resonance spectra of solids exhibit such resolution only in special cases. The primary (although not the exclusive) reason for the lack of resolution in the spectrum of a typical solid is the presence of the dipole*b1dipole interaction, which dominates the NMR spectroscopy of solids that have been of interest to chemists. One solution (no pun intended) to the problem of obtaining chemical-shift information about such solids is to dissolve them and to study them in solution. However, if the solid is insoluble or otherwise intractable or if the analysis involves questions about the properties of the substance in the solid state, then there arises a need for techniques to study the weaker interactions in the presence of the dipole*b1dipole interaction or other overwhelming interactions. This volume describes the means dev
Download or read book Spin Dynamics written by Malcolm H. Levitt and published by Wiley. This book was released on 2008-07-31 with total page 744 pages. Available in PDF, EPUB and Kindle. Book excerpt: Spin Dynamics: Basics of Nuclear Magnetic Resonance, Second Edition is a comprehensive and modern introduction which focuses on those essential principles and concepts needed for a thorough understanding of the subject, rather than the practical aspects. The quantum theory of nuclear magnets is presented within a strong physical framework, supported by figures. The book assumes only a basic knowledge of complex numbers and matrices, and provides the reader with numerous worked examples and exercises to encourage understanding. With the explicit aim of carefully developing the subject from the beginning, the text starts with coverage of quarks and nucleons and progresses through to a detailed explanation of several important NMR experiments, including NMR imaging, COSY, NOESY and TROSY. Completely revised and updated, the Second Edition features new material on the properties and distributions of isotopes, chemical shift anisotropy and quadrupolar interactions, Pake patterns, spin echoes, slice selection in NMR imaging, and a complete new chapter on the NMR spectroscopy of quadrupolar nuclei. New appendices have been included on Euler angles, and coherence selection by field gradients. As in the first edition, all material is heavily supported by graphics, much of which is new to this edition. Written for undergraduates and postgraduate students taking a first course in NMR spectroscopy and for those needing an up-to-date account of the subject, this multi-disciplinary book will appeal to chemical, physical, material, life, medical, earth and environmental scientists. The detailed physical insights will also make the book of interest for experienced spectroscopists and NMR researchers. • An accessible and carefully written introduction, designed to help students to fully understand this complex and dynamic subject • Takes a multi-disciplinary approach, focusing on basic principles and concepts rather than the more practical aspects • Presents a strong pedagogical approach throughout, with emphasis placed on individual spins to aid understanding • Includes numerous worked examples, problems, further reading and additional notes Praise from the reviews of the First Edition: "This is an excellent book... that many teachers of NMR spectroscopy will cherish... It deserves to be a ‘classic’ among NMR spectroscopy texts." NMR IN BIOMEDICINE "I strongly recommend this book to everyone…it is probably the best modern comprehensive description of the subject." ANGEWANDTE CHEMIE, INTERNATIONAL EDITION
Download or read book Molecular and Spin Dynamics in Solid State Nuclear Magnetic Resonance Spectroscopy written by Douglas Charles Maus and published by . This book was released on 1996 with total page 304 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Nuclear Magnetic Resonance in Solids written by Lieven Gerven and published by Springer Science & Business Media. This book was released on 2013-03-09 with total page 433 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Spin Temperature and Nuclear Magnetic Resonance in Solids written by Maurice Goldman and published by . This book was released on 1970 with total page 268 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Pulsed Nuclear Magnetic Resonance and Spin Dynamics in Solids Proceedings of the First Specialized Colloque Krakow 28th August 1st September 1973 Ed by J W Hennel written by Jacek W. Hennel and published by . This book was released on 1973 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Spin Dynamics of Pulsed Nuclear Magnetic Double Resonance in Solids written by Michael Edward Stoll and published by . This book was released on 1977 with total page 187 pages. Available in PDF, EPUB and Kindle. Book excerpt: In the first part of this thesis, experiments utilizing an NMR phase interferometric concept are presented. The spinor character of two-level systems is explicitly demonstrated by using this concept. Following this is the presentation of an experiment which uses this same idea to measure relaxation times of off-diagonal density matrix elements corresponding to magnetic-dipole-forbidden transitions in a 13C-1H, AX spin system. The theoretical background for these experiments and the spin dynamics of the interferometry are discussed also. The second part of this thesis deals with NMR dipolar modulated chemical shift spectroscopy, with which internuclear bond lengths and bond angles with respect to the chemical shift principal axis frame are determined from polycrystalline samples. Experiments using benzene and calcium formate verify the validity of the technique in heteronuclear (13C-1H) systems. Similar experiments on powdered trichloroacetic acid confirm the validity in homonuclear (1H-1H) systems. The theory and spin dynamics are explored in detail, and the effects of a number of multiple pulse sequences are discussed. The last part deals with an experiment measuring the 13C chemical shift tensor in K2Pt(CN)4Br0.3 · 3H2O, a one-dimensional conductor. The 13C spectra are strongly affected by 14N quadrupolar interactions via the 13C -14N dipolar interaction. Single crystal rotation spectra are shown. An appendix discussing the design, construction, and performance of a single-coil double resonance NMR sample probe is included.
Download or read book Solid State NMR Spectroscopy written by Melinda J. Duer and published by John Wiley & Sons. This book was released on 2008-04-15 with total page 592 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is for those familiar with solution-state NMR who are encountering solid-state NMR for the first time. It presents the current understanding and applications of solid-state NMR with a rigorous but readable approach, making it easy for someone who merely wishes to gain an overall impression of the subject without details. This dual requirement is met through careful construction of the material within each chapter. The book is divided into two parts: "Fundamentals" and "Further Applications." The section on Fundamentals contains relatively long chapters that deal with the basic theory and practice of solid-state NMR. The essential differences and extra scope of solid-state NMR over solution-state is dealt with in an introductory chapter. The basic techniques that all chapters rely on are collected into a second chapter to avoid unnecessary repetition later. Remaining chapters in the "Fundamentals" part deal with the major areas of solid-state NMR which all solid-state NMR spectroscopists should know about. Each begins with an overview of the topic that puts the chapter in context. The basic principles upon which the techniques in the chapter rely are explained in a separate section. Each of these chapters exemplifies the principles and techniques with the applications most commonly found in current practice. The "Further Applications" section contains a series of shorter chapters which describe the NMR techniques used in other, more specific areas. The basic principles upon which these techniques rely will be expounded only if not already in the Fundamentals part.
Download or read book Dynamic Nuclear Polarization and Electron Spin Resonance in Paramagnetic Solids at High Field written by Souheil James Inati and published by . This book was released on 1999 with total page 161 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Advances in Magnetic Resonance written by Warren S. Warren and published by Academic Press. This book was released on 2012-12-02 with total page 309 pages. Available in PDF, EPUB and Kindle. Book excerpt: Advances in Magnetic Resonance: The Waugh Symposium, Volume 14 is a collection of manuscripts presented at the 1989 symposium on “High Resolution NMR in Solids , held at the Massachusetts Institute of Technology. The contributors provide 20- to 30-page articles consistent with AMR’s traditional emphasis on quantitative analysis of NMR techniques. Organized into 13 chapters, this book discusses the principles triple-quantum filtered two-dimensional exchange spectroscopy and its application in the measurement of cross correlation between pairs of dipole-dipole interactions. It then describes alternative ways of using fictitious spin in pulsed nuclear quadrupole resonance or NMR. General topics on the application of optical spectroscopy; the saturation of spin-spin energy by slow continuous bulk rotation; the frequency-switched Lee-Goldburg pulse cycle; and high-resolution proton NMR in solid systems are also explored. A chapter examines an entirely different view of spin dynamics in the presence of radio-frequency fields. This book also deals with the theoretical background and application of solid-state and zero-field NMR spectroscopies to structure determination. Lastly, the utilization of the Floquet formalism in the design of broadband propagators in two-level systems and the two classes of novel NMR phenomena related to the symmetrization postulate are discussed. Analytical and quantum chemists, physicists, biochemists, and materials science researchers will find this book invaluable.
Download or read book NMR of Quadrupolar Nuclei in Solid Materials written by Roderick E. Wasylishen and published by John Wiley & Sons. This book was released on 2012-12-19 with total page 564 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR OF QUADRUPOLAR NUCLEI IN SOLID MATERIALS Over the past 20 years technical developments in superconducting magnet technology and instrumentation have increased the potential of NMR spectroscopy so that it is now possible to study a wide range of solid materials. In addition, one can probe the nuclear environments of many other additional atoms that possess the property of spin. In particular, it is possible to carry out NMR experiments on isotopes that have nuclear spin greater that 1⁄2 (i.e. quadrupolar nuclei). Since more that two-thirds of all NMR active isotopes are quadrupolar nuclei, applications of NMR spectroscopy with quadrupolar nuclei are increasing rapidly. The purpose of this handbook is to provide under a single cover the fundamental principles, techniques and applications of quadrupolar NMR as it pertains to solid materials. Each chapter has been prepared by an expert who has made significant contributions to out understanding and appreciation of the importance of NMR studies of quadrupolar nuclei in solids. The text is divided into three sections: The first provides the reader with the background necessary to appreciate the challenges in acquiring and interpreting NMR spectra of quadrupolar neclei in solids. The second presents cutting-edge techniques and methodology for employing these techniques to investigate quadrupolar nuclei in solids. The final section explores applications of solid-state NMR studies of solids ranging from investigations of dynamics, characterizations of biological samples, organic and inorganic materials, porous materials, glasses, catalysts, semiconductors and high-temperature superconductors. About EMR Handbooks The Encyclopedia of Magnetic Resonance (EMR) publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence-of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of Encyclopedia articles. In consultation with the EMR Editorial Board, the EMR Handbooks are coherently planned in advance by specially-selected Editors, and new articles, are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry. Have the content of this handbook and the complete content of the Encyclopedia of Magnetic Resonance at your fingertips! Visit: www.wileyonlinelibrary.com/ref/emr
Download or read book Solid State NMR written by Klaus Müller and published by John Wiley & Sons. This book was released on 2021-06-23 with total page 560 pages. Available in PDF, EPUB and Kindle. Book excerpt: Solid State NMR A thorough and comprehensive textbook covering the theoretical background, experimental approaches, and major applications of solid-state NMR spectroscopy Nuclear Magnetic Resonance (NMR) spectroscopy is a powerful non-destructive technique capable of providing information about the molecular structure and dynamics of molecules. Alongside solution-state NMR, a well-established technique to study chemical structures and investigate physico-chemical properties of molecules in solutions, solid-state NMR (SSNMR) offers many exciting possibilities for the analysis of solid and soft materials across scientific fields. SSNMR shows unique capabilities for a detailed investigation of structural and dynamic properties of materials over wide space and time ranges. For this reason, and thanks to significant advances in the past several years, the application of SSNMR to materials is rapidly increasing in disciplines such as chemistry, physics, and materials and life sciences. Solid State NMR: Principles, Methods, and Applications offers a systematic introduction to the theory, methodological concepts, and major experimental methods of SSMR spectroscopy. Exploring the unique potential of SSNMR for the structural and dynamic characterization of soft and either amorphous or crystalline solid materials, this comprehensive textbook provides foundational knowledge and recent developments of SSNMR, covering physical and theoretical background, experimental methods, and applications to pharmaceuticals, polymers, inorganic and hybrid materials, liquid crystals, and model membranes. Written by two expert authors to ensure a clear and consistent presentation of the subject, this textbook: Includes a brief introduction to the historical aspects and broad theoretical background of solid-state NMR spectroscopy Provides helpful illustrations to explain the various SSNMR concepts and methods Features accessible descriptive text with self-consistent use of quantum mechanics Covers the experimental aspects of SSNMR spectroscopy and in particular a description of many useful pulse sequences Contains references to relevant literature Solid State NMR: Principles, Methods, and Applications is the ideal textbook for university courses on SSNMR, advanced spectroscopies, and a valuable single-volume reference for spectroscopists, chemists, and researchers in the field of materials.
Download or read book Nuclear Magnetic Resonance in Solid Polymers written by Vincent J. McBrierty and published by Cambridge University Press. This book was released on 1993-10-14 with total page 375 pages. Available in PDF, EPUB and Kindle. Book excerpt: Authoritative and comprehensive account of the principles and practice of NMR spectroscopy of solids as applied to polymeric materials to determine their structure and dynamics at a molecular level.
