Download or read book High Resolution NMR in Solids Selective Averaging written by Ulrich Haeberlen and published by Elsevier. This book was released on 2012-12-02 with total page 205 pages. Available in PDF, EPUB and Kindle. Book excerpt: High Resolution NMR in Solids: Selective Averaging presents the principles and applications of the four approaches to high resolution NMR in solids — magic-angle sample spinning, multiple-pulse, proton-enhanced nuclear induction, and indirect detection methods. Divided into six chapters, this book initially describes the tensorial properties of nuclear spin interactions in both ordinary and spin spaces. It then deals with the manifestations of nuclear magnetic shielding in NMR spectra of both single-crystal and powder samples, and then discusses the techniques for analyzing spectra and rotation patterns in terms of shielding tensors. A wide range of NMR phenomena that are result of intentional or natural, selective or unselective averaging processes and the average Hamiltonian theory that yields the inclusion of correction are covered. This book also provides a detailed discussion on multiple-pulse sequences intended for high resolution NMR in solids. The concluding chapter examines the applications of multiple-pulse techniques, with particular emphasis on measurements of 19F and 1H shielding tensors. Discussions on rotations of angular momentum operators; time ordering and the Magnus expansion; off-resonance averaging of the second-order dipolar Hamiltonian; and phase transients are covered in the supplemental texts.
Download or read book High resolution NMR in solids written by and published by . This book was released on 1976 with total page 190 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book High resolution NMR in solids written by and published by . This book was released on with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Annual Reports on NMR Spectroscopy written by Graham A. Webb and published by Academic Press. This book was released on 2008-11-20 with total page 225 pages. Available in PDF, EPUB and Kindle. Book excerpt: The great importance of NMR in many areas of scientific research is once again highlighted in this volume of Annual Reports on NMR Spectroscopy. Provides updates on the latest developments in NMR spectroscopy Includes comprehensive review articles Highlights the increasing importance of NMR spectroscopy as a technique for structural determination
Download or read book High Resolution NMR written by Edwin D. Becker and published by Elsevier. This book was released on 2012-12-02 with total page 369 pages. Available in PDF, EPUB and Kindle. Book excerpt: High Resolution NMR: Theory and Chemical Applications discusses the principles and theory of nuclear magnetic resonance and how this concept is used in the chemical sciences. This book is written at an intermediate level, with mathematics used to augment verbal descriptions of the phenomena. This text pays attention to developing and interrelating four approaches – the steady state energy levels, the rotating vector picture, the density matrix, and the product operator formalism. The style of this book is based on the assumption that the reader has an acquaintance with the general principles of quantum mechanics, but no extensive background in quantum theory or proficiency in mathematics is required. This book begins with a description of the basic physics, together with a brief account of the historical development of the field. It looks at the study of NMR in liquids, including high resolution NMR in the solid state and the principles of NMR imaging and localized spectroscopy. This book is intended to assist chemistry graduate students, advanced undergraduate students, or researchers to understand NMR at a fundamental level. This text also provides illustrations of the applications of NMR to the determination of the structure of small organic molecules and macromolecules, including proteins.
Download or read book Phosphorus NMR in Biology written by C. Burt and published by CRC Press. This book was released on 2018-01-18 with total page 244 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR is a technique that can spoil you. It is true that it is not as sensitive as some of the spectroscopic methods, but the quality of the information and the incredible ease of sample preparation make it one of the tools that have opened new vistas in biological research. This volume is intended to show how those vistas can range from the molecule to the microbe to man himself. Further, it is what prompts the rather broad title.
Download or read book Modern Techniques in High Resolution FT NMR written by Narayanan Chandrakumar and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 396 pages. Available in PDF, EPUB and Kindle. Book excerpt: The magnetism of nuclear spin systems has proved an amazingly fertile ground for the creativity of researchers. This happy circumstance results from the triple benediction that nature appears to have bestowed on nuclear spins: they are sporting spies-being infinitely manipulable (one is even tempted to say malleable), not unduly coy in revealing their secrets, and having a whole treasure house of secrets to reveal in the first place. researcher with Since spin dynamics are now orchestrated by the NMR ever more subtle scores, it is important to be able to tune into the pro ceedings with precision, if one is to make sense of it at all. Fortunately, it is not terribly difficult to do so, since in many ways spin dynamics are the theoretician's dream come true: they are often finite dimensional and quite tractable with basic quantum mechanics, frequently allowing near exact treatments and readily testable predictions. This book was conceived two years ago, with the objective of providing a simple, consistent introduction to the description of the spin dynamics that one encounters in modern NMR experiments. We believed it was a good time to attempt this, since it was possible by then to give sufficiently general descriptions of powelful classes of new NMR experiments. The choice of experiments we discuss in detail is necessarily subjective, al though we hope to have given a flavor of most of the important classes of pulse sequences, including some surface coil imaging applications.
Download or read book Characterization of Solid Polymers written by S.J. Spells and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 380 pages. Available in PDF, EPUB and Kindle. Book excerpt: The last decade or so has seen a dramatic increase in the amount of detailed structural information available from a range of experimental techniques. Exciting new techniques such as atomic force microscopy have become widely available, while the potential of established methods like X-ray diffraction and electron microscopy has been greatly enhanced by powerful new sources and analytical methods. Progress in computing has also had a widespread impact: in areas such as neutron scattering, large data sets can now be manipulated more readily. The software supplied with commercial instruments generally provides more sophisti cated analytical facilities, while time-resolved X-ray studies rely on rapid data handling capabilities. The polymer scientist is faced with an expanding array of experimental tools for addressing both fundamental science and industrial problems. This work reviews some recent developments in structural techniques, with the aim of presenting the current 'state of the art' in a selection of areas.
Download or read book Spectroscopic Properties of Inorganic and Organometallic Compounds written by E A V Ebsworth and published by Royal Society of Chemistry. This book was released on 2007-10-31 with total page 506 pages. Available in PDF, EPUB and Kindle. Book excerpt: Spectroscopic Properties of Inorganic and Organometallic Compounds provides a unique source of information on an important area of chemistry. Divided into sections mainly according to the particular spectroscopic technique used, coverage in each volume includes: NMR (with reference to stereochemistry, dynamic systems, paramagnetic complexes, solid state NMR and Groups 13-18); nuclear quadrupole resonance spectroscopy; vibrational spectroscopy of main group and transition element compounds and coordinated ligands; and electron diffraction. Reflecting the growing volume of published work in this field, researchers will find this Specialist Periodical Report an invaluable source of information on current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading experts in their specialist fields, this series is designed to help the chemistry community keep current with the latest developments in their field. Each volume in the series is published either annually or biennially and is a superb reference point for researchers. www.rsc.org/spr
Download or read book Solid State NMR of Polymers written by T. Asakura and published by Elsevier. This book was released on 1998-08-03 with total page 1017 pages. Available in PDF, EPUB and Kindle. Book excerpt: In polymer science and technology, the advanced development of various new polymer materials with excellent properties and functions is desirable. For this purpose it is necesary to determine the exact relationship between physical properties and molecular structure-dynamics with powerful techniques. One such technique is solid state NMR. Recently, high resolution NMR studies of solids have been realized by using advanced pulse and mechanical techniques, which has resulted in a variety of structural and dynamical information on polymer systems. Solid state NMR has provided characteristic information which cannot be obtained by other spectroscopic methods. This book is divided into two parts. The first part covers the principles of NMR, important NMR parameters such as chemical shifts, relaxation times, dipolar interactions, quadrupolar interactions, pulse techniques and new NMR methods. In the second part, applications of NMR to a variety of polymer systems in the solid state are described. Features of this book: • Contains an up-to-date and comprehensive account of solid state NMR of polymers by leading researchers in the field • Provides a compilation of solid state NMR of polymers, which makes it an ideal reference book for both NMR researchers and general polymer scientists. This book will be of interest to the NMR community, and will be invaluable for both the beginner and the expert.
Download or read book Nuclear Magnetic Resonance in Agriculture written by Philip E. Pfeffer and published by CRC Press. This book was released on 1989-04-30 with total page 454 pages. Available in PDF, EPUB and Kindle. Book excerpt: This informative publication presents the broad application of nuclear magnetic resonance to many of today's problem areas in agriculture. Solid-state NMR methodology is covered, with its applications to the study of intact agricultural matrices such as plant cell walls, photosynthetic chloroplast membranes, forages, wood cellulose, and soils. In vivo solution NMR methodology and its applications to the study of different functioning plant tissues and their biochemical responses to various pathological, physiological, and toxicological stresses are illustrated with examples using 31P, 13C, 23Na, and 15N resonance methods. An introductory chapter presents a review of the in vivo literature and some basic principles and requirements for carrying out such experiments. A special section focuses on state-of-the-art 13C and 1H high-resolution multidimensional methods and their application to the study of agricultural toxins; biologically active components, including their structures and biosyntheses, and dynamic measurements of relaxation phenomena associated with cross relaxation in water bound to food proteins.
Download or read book Object Oriented Magnetic Resonance written by Michael Mehring and published by Elsevier. This book was released on 2012-12-02 with total page 582 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents, for the first time, a unified treatment of the quantum mechanisms of magnetic resonance, including both nuclear magnetic resonance (NMR) and electron spin resonance (ESR). Magnetic resonance is perhaps the most advanced type of spectroscopy and it is applied in biology, chemistry, physics, material science, and medicine. If applied in conjunction with spectroscopy, the imaging version of magnetic resonance has no counterpart in any type of experimental technique. The authors present explanations and applications from fundamental to advanced levels. The authors present explanations and applications from fundamental to advanced levels This groundbreaking volume is accompanied by software which simulates magnetic resonance phenomena
Download or read book NMR Spectroscopy of Biological Solids written by A. Ramamoorthy and published by CRC Press. This book was released on 2005-09-22 with total page 368 pages. Available in PDF, EPUB and Kindle. Book excerpt: Over the past decade, a myriad of techniques have shown that solid-state nuclear magnetic resonance (NMR) can be used in a broad spectrum of applications with exceptionally impressive results. Solid-state NMR results can yield high-resolution details on the structure and function of many important biological solids, including viruses, fibril-formin
Download or read book Solid State NMR I Methods written by B. Blümich and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 286 pages. Available in PDF, EPUB and Kindle. Book excerpt: 1. A.-R. Grimmer, Berlin, FRG; B. Bl}mich, Aachen, FRG: Introduction to Solid-State NMR 2. F. Laupretre, Paris, France: High-Resolution 13C NMRInvestigations of Local Dynamics in Bulk Polymers at Temperatures Below andAbove the Glass-Transition Temperature 3. D. Raftery, Philadelphia, PA;B.F. Chmelka, Santa Barbara, CA: Xenon NMR Spectroscopy 4. G. Fleischer, Leipzig, FRG; F. Fujara, Mainz, FRG: NMR as a Generalized Incoherent Scattering Experiment 5. P. Bl}mler, B. Bl}mich, Mainz, FRG: NMR Imaging of Solids.
Download or read book Principles of Magnetic Resonance written by Charles P. Slichter and published by Springer Science & Business Media. This book was released on 2013-06-29 with total page 407 pages. Available in PDF, EPUB and Kindle. Book excerpt: It is a source of great pleasure to help launch the new Springer Series in Solid-State Sciences. Some years aga I wrote my book, Principles of Magnetic Resonance. I have been eager to publish a new book concerned with spin temperature, double resonance, and spin-flip line narrowing, topics basic to important trends in present-day magnetic resonance which were not treated in my earlier book. Invitations to lecture in Osaka, Japan, in Leuven, Belgium, and Lausanne, Switzerland, had provided occasion to prepare first drafts of the new topics and to get student feedback. My plans were changed, however, when I learned that Principles of M agnetic Resonance was no longer available. Dr. Lotsch, Physics Editor of Springer-Verlag, and I decided it made sense to combine the new book with a modified old one, thereby continuing to make available a complete text in basic magnetic resonance written with a philosophy of presenting a thorough treatment of a small number of concepts which are key to large areas of magnetic res on an ce. In addition to adding three new chapters, I have added new material to the original chapters, have added two new appendices-one on the use of Bloch equations to describe rate processes, the other on the effect of diffusion on spin echoes-and have augmented the collection of homework problems.
Download or read book High Resolution NMR Techniques in Organic Chemistry written by Timothy D.W. Claridge and published by Newnes. This book was released on 2009 with total page 400 pages. Available in PDF, EPUB and Kindle. Book excerpt: "Nuclear Magnetic Resonance (NMR) Spectroscopy remains the foremost analytical technique for the structure elucidation of organic molecules and an indispensable tool for the synthetic, medicinal and natural product chemist. New techniques continue to emerge and the application of NMR methods continues to expand. High-Resolution NMR Techniques in Organic Chemistry is designed for use in academic and industrial NMR facilities, as a text for graduate-level NMR courses, and as an accessible reference for the chemist's or spectroscopist's desk."--BOOK JACKET.
Download or read book Magnetic Resonance in Colloid and Interface Science written by J. Fraissard and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 709 pages. Available in PDF, EPUB and Kindle. Book excerpt: In 1976, on the occasion of the Centennial of the Ameri can Chemical Society, H. A. RESrnG and C. G. WADE organized an international symposium on magnetic resonance in collo1d and in terface science which brought together a large number of scien tists from the United States and from abroad. The aim of this symposium was to include all experimental inorganic, organic and biochemical systems in which molecules are bound to interfaces and to show the contribution of various techniques based on ma gnetic resonance to the knowledge of these systems. This ambi tious program resulted into a very interesting gathering that initiated a more interdisciplinary approach to the problem of interfaces. Because of the success of this symposium it was sug gested that a similar meeting should be organized in Europe within the next three years. Professor J. FRAISSARD accepted this task but, conside ring the rapid developments in the theory and in the applica tions of the magnetic resonance spectroscopies, the organ1z1ng committee decided to arrange the meeting to be held in MENTON (France) in two parts, the first being a School and the second the Symposium proper. The former was' intended to review and to teach theoretical aspects as well as to discuss the experimental results derived from these advanced methods; the Symposium was to be for the discussion of the latest results at the highest level.
