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Book Development of New Probes Based on Carbon Nanocones for Near field Microscopies

Download or read book Development of New Probes Based on Carbon Nanocones for Near field Microscopies written by Germercy Paredes Guerrero and published by . This book was released on 2020 with total page 258 pages. Available in PDF, EPUB and Kindle. Book excerpt: Near-field microscopy allows studying the topography and the physical properties (electrical, mechanical, etc.) of a material surface at nanoscale. For such a purpose, the sample surface is scanned by a probe (or tip) which geometric characteristics (such as the apex radius and the aspect ratio) and the physical properties (mechanical, electrical, etc.) must be suitable to ensure a sufficient resolution and a reliable representation of the surface. However, the current probes have significant limitations regarding the resolution, the possible imaging artifacts, as well as their ability to be used in different modes (conductive and non-conductive). These limitations are caused mainly by the type of material used (for example silicon or silicon nitride, for standard probes, or carbon nanotubes), as well as by the manufacturing processes used to structure the geometry of the probes. In this work, we study the potential of carbon nanocones (graphenic carbonaceous morphology with conical shape with high aspect ratio and nanosized apex) for different modes of near-field microscopy. These nanocones exhibit excellent mechanical (strong C-C bond) and electrical properties. They have already been successfully tested and patented as electron emitters for the cold-field-emission guns which equip the most performing transmission electron microscopes. These various characteristics of the nanocones (aspect ratio, nanosized apex, conductivity, mechanical stability, strong atomic cohesion) and others (hydrophobicity, chemical inertia, multiscale micro-nano morphology ...), make that they could also constitute a promising solution for designing probes potentially superior to existing probes, either standard or more specific such as those in carbon nanotubes, for various types of near-field microscopy, in particular in terms of spatial resolution and durability. In the first part, this thesis is dedicated to the synthesis of individual carbon nanocones using an original synthesis method called ToF-CVD (Time of Flight Chemical Vapor Deposition). The work reveals complex formation mechanisms involving the heterogeneous phase nucleation mechanisms specific of the CVD deposition of pyrolytic carbon on the one hand, and well-known wetting mechanisms such the Plateau-Rayleigh instability on the other hand. The mounting of the nanocones on dedicated supports as probes for near-field microscopies is then carried out, followed by characterization studies (SEM, TEM, RAMAN spectroscopy) to assess their starting characteristics from the geometry and structure point of view, and their evolution under the operating conditions required for both the probe fabrication and for the different near-field microscopy modes studied. In a second part, the potentiality of carbon nanocones as probes for non-conductive modes such as topographic mode (atomic force microscopy - AFM) and "Peak Force Quantitative Nano Mechanical" (PF-QNM) mode, as well as for conductive modes such as scanning tunneling microscopy (STM), conductive atomic force microscopy (c-AFM), and Kelvin force microscopy (KFM) is evaluated. This evaluation is made on the basis of (i) performances; (ii) durability; (iii) versatility. The final goal is to compare the performance of the carbon nanocone probes with other commercial probes. Carbon nanocones reveal to truly be multimode probes with few existing counterparts nowadays. Improvements are needed and possible, for which directions are proposed

Book Handbook of Nanoscopy  2 Volume Set

Download or read book Handbook of Nanoscopy 2 Volume Set written by Gustaaf van Tendeloo and published by John Wiley & Sons. This book was released on 2012-05-21 with total page 1484 pages. Available in PDF, EPUB and Kindle. Book excerpt: This completely revised successor to the Handbook of Microscopy supplies in-depth coverage of all imaging technologies from the optical to the electron and scanning techniques. Adopting a twofold approach, the book firstly presents the various technologies as such, before going on to cover the materials class by class, analyzing how the different imaging methods can be successfully applied. It covers the latest developments in techniques, such as in-situ TEM, 3D imaging in TEM and SEM, as well as a broad range of material types, including metals, alloys, ceramics, polymers, semiconductors, minerals, quasicrystals, amorphous solids, among others. The volumes are divided between methods and applications, making this both a reliable reference and handbook for chemists, physicists, biologists, materials scientists and engineers, as well as graduate students and their lecturers.

Book Carbon Nanotubes

    Book Details:
  • Author : M. Endo
  • Publisher : Elsevier
  • Release : 2013-10-22
  • ISBN : 008054553X
  • Pages : 200 pages

Download or read book Carbon Nanotubes written by M. Endo and published by Elsevier. This book was released on 2013-10-22 with total page 200 pages. Available in PDF, EPUB and Kindle. Book excerpt: Carbon nanotubes have been studied extensively in relation to fullerenes, and together with fullerenes have opened a new science and technology field on nano scale materials. A whole range of issues from the preparation, structure, properties and observation of quantum effects in carbon nanotubes in comparison with 0-D fullerenes are discussed. In addition, complementary reviews on carbon nanoparticles such as carbon nano-capsules, onion-like graphite particles and metal-coated fullerenes are covered. This book aims to cover recent research and development in this area, and so provide a convenient reference tool for all researchers in this field. It is also hoped that this book can serve to stimulate future work on carbon nanotubes.

Book Advanced Transmission Electron Microscopy

Download or read book Advanced Transmission Electron Microscopy written by Francis Leonard Deepak and published by Springer. This book was released on 2015-06-05 with total page 281 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book highlights the current understanding of materials in the context of new and continuously emerging techniques in the field of electron microscopy. The authors present applications of electron microscopic techniques in characterizing various well-known & new nanomaterials. The applications described include both inorganic nanomaterials as well as organic nanomaterials.

Book Nanotechnology  Concepts  Methodologies  Tools  and Applications

Download or read book Nanotechnology Concepts Methodologies Tools and Applications written by Management Association, Information Resources and published by IGI Global. This book was released on 2014-02-28 with total page 1654 pages. Available in PDF, EPUB and Kindle. Book excerpt: Over the past few decades, devices and technologies have been significantly miniaturized from one generation to the next, providing far more potential in a much smaller package. The smallest of these recently developed tools are miniscule enough to be invisible to the naked eye. Nanotechnology: Concepts, Methodologies, Tools, and Applications describes some of the latest advances in microscopic technologies in fields as diverse as biochemistry, materials science, medicine, and electronics. Through its investigation of theories, applications, and new developments in the nanotechnology field, this impressive reference source will serve as a valuable tool for researchers, engineers, academics, and students alike.

Book Raman Spectroscopy in Graphene Related Systems

Download or read book Raman Spectroscopy in Graphene Related Systems written by Ado Jorio and published by John Wiley & Sons. This book was released on 2011-08-24 with total page 319 pages. Available in PDF, EPUB and Kindle. Book excerpt: Raman spectroscopy is the inelastic scattering of light by matter. Being highly sensitive to the physical and chemical properties of materials, as well as to environmental effects that change these properties, Raman spectroscopy is now evolving into one of the most important tools for nanoscience and nanotechnology. In contrast to usual microscopyrelated techniques, the advantages of using light for nanoscience relate to both experimental and fundamental aspects.

Book Nanofibers

    Book Details:
  • Author : Ashok Kumar
  • Publisher : BoD – Books on Demand
  • Release : 2010-02-01
  • ISBN : 9537619869
  • Pages : 454 pages

Download or read book Nanofibers written by Ashok Kumar and published by BoD – Books on Demand. This book was released on 2010-02-01 with total page 454 pages. Available in PDF, EPUB and Kindle. Book excerpt: “There’s Plenty of Room at the Bottom” ⎯ this was the title of the lecture Prof. Richard Feynman delivered at California Institute of Technology on December 29, 1959 at the American Physical Society meeting. He considered the possibility to manipulate matter on an atomic scale. Indeed, the design and controllable synthesis of nanomaterials have attracted much attention because of their distinctive geometries and novel physical and chemical properties. For the last two decades nano-scaled materials in the form of nanofibers, nanoparticles, nanotubes, nanoclays, nanorods, nanodisks, nanoribbons, nanowhiskers etc. have been investigated with increased interest due to their enormous advantages, such as large surface area and active surface sites. Among all nanostructures, nanofibers have attracted tremendous interest in nanotechnology and biomedical engineering owing to the ease of controllable production processes, low pore size and superior mechanical properties for a range of applications in diverse areas such as catalysis, sensors, medicine, pharmacy, drug delivery, tissue engineering, filtration, textile, adhesive, aerospace, capacitors, transistors, battery separators, energy storage, fuel cells, information technology, photonic structures and flat panel displays, just to mention a few. Nanofibers are continuous filaments of generally less than about 1000 nm diameters. Nanofibers of a variety of cellulose and non-cellulose based materials can be produced by a variety of techniques such as phase separation, self assembly, drawing, melt fibrillation, template synthesis, electro-spinning, and solution spinning. They reduce the handling problems mostly associated with the nanoparticles. Nanoparticles can agglomerate and form clusters, whereas nanofibers form a mesh that stays intact even after regeneration. The present book is a result of contributions of experts from international scientific community working in different areas and types of nanofibers. The book thoroughly covers latest topics on different varieties of nanofibers. It provides an up-to-date insightful coverage to the synthesis, characterization, functional properties and potential device applications of nanofibers in specialized areas. We hope that this book will prove to be timely and thought provoking and will serve as a valuable reference for researchers working in different areas of nanofibers. Special thanks goes to the authors for their valuable contributions.

Book Graphene Surfaces

    Book Details:
  • Author : Karim Kakaei
  • Publisher : Academic Press
  • Release : 2018-10-09
  • ISBN : 0128145242
  • Pages : 456 pages

Download or read book Graphene Surfaces written by Karim Kakaei and published by Academic Press. This book was released on 2018-10-09 with total page 456 pages. Available in PDF, EPUB and Kindle. Book excerpt: Graphene Surfaces: Particles and Catalysts focuses on the surface chemistry and modification of graphene and its derivatives from a theoretical and electrochemical point-of-view. It provides a comprehensive overview of their electronic structure, synthesis, properties and general applications in catalysis science, including their relevance in alcohols and their derivatives oxidation, oxygen reduction, hydrogen evolution, energy storage, corrosion protection and supercapacitors. The book also covers emerging research on graphene chemistry and its impact. Chemical engineers, materials scientists, electrochemists and engineers will find information that will answer their most pressing questions on the surface aspects of graphene and its effect on catalysis. Serves as a time-saving reference for researchers, graduated students and chemical engineers Equips the reader with catalysis knowledge for practical applications Discusses the physical and electrochemical properties of graphene Provides the most important applications of graphene in electrochemical systems Highlights both experimental and theoretical aspects of graphene

Book Carbon Nanotubes

Download or read book Carbon Nanotubes written by Michael J. O’Connell and published by CRC Press. This book was released on 2018-10-03 with total page 339 pages. Available in PDF, EPUB and Kindle. Book excerpt: Since their discovery more than a decade ago, carbon nanotubes (CNTs) have held scientists and engineers in captive fascination, seated on the verge of enormous breakthroughs in areas such as medicine, electronics, and materials science, to name but a few. Taking a broad look at CNTs and the tools used to study them, Carbon Nanotubes: Properties and Applications comprises the efforts of leading nanotube researchers led by Michael O’Connell, protégé of the late father of nanotechnology, Richard Smalley. Each chapter is a self-contained treatise on various aspects of CNT synthesis, characterization, modification, and applications. The book opens with a general introduction to the basic characteristics and the history of CNTs, followed by discussions on synthesis methods and the growth of “peapod” structures. Coverage then moves to electronic properties and band structures of single-wall nanotubes (SWNTs), magnetic properties, Raman spectroscopy of electronic and chemical behavior, and electromechanical properties and applications in NEMS (nanoelectromechanical systems). Turning to applications, the final sections of the book explore mechanical properties of SWNTs spun into fibers, sidewall functionalization in composites, and using SWNTs as tips for scanning probe microscopes. Taking a fresh look at this burgeoning field, Carbon Nanotubes: Properties and Applications points the way toward making CNTs commercially viable.

Book Carbon Alloys

    Book Details:
  • Author : E. Yasuda
  • Publisher : Elsevier
  • Release : 2003-03-05
  • ISBN : 0080528538
  • Pages : 584 pages

Download or read book Carbon Alloys written by E. Yasuda and published by Elsevier. This book was released on 2003-03-05 with total page 584 pages. Available in PDF, EPUB and Kindle. Book excerpt: In recent years the Japanese have funded a comprehensive study of carbon materials which incorporate other elements including boron, nitrogen and fluorine, hence the title of the project "Carbon Alloys". Coined in 1992, the phrase "Carbon Alloys" can be applied to those materials mainly composed of carbon materials in multi-component systems. The carbon atoms of each component have a physical and/or chemical interactive relationship with other atoms or compounds. The carbon atoms of the components may have different hybrid bonding orbitals to create quite different carbon components. Eiichi Yasuda and his team consider the definition of Carbon Alloys, present the results of the Carbon Alloys projects, describe typical Carbon Alloys and their uses, discuss recent techniques for their characterization, and finally, illustrate potential applications and future developments for Carbon Alloy science. The book contains over thirty chapters on these studies from as many researchers. The most modern of techniques, particularly in the area of spectroscopy, were used as diagnostic tools, and many of these are applicable to pure carbons also. Porosity in carbons received considerable attention.

Book Carbon Nanotubes

    Book Details:
  • Author : M. Meyyappan
  • Publisher : CRC Press
  • Release : 2004-07-28
  • ISBN : 0203494938
  • Pages : 306 pages

Download or read book Carbon Nanotubes written by M. Meyyappan and published by CRC Press. This book was released on 2004-07-28 with total page 306 pages. Available in PDF, EPUB and Kindle. Book excerpt: Carbon nanotubes, with their extraordinary mechanical and unique electronic properties, have garnered much attention in the past five years. With a broad range of potential applications including nanoelectronics, composites, chemical sensors, biosensors, microscopy, nanoelectromechanical systems, and many more, the scientific community is more moti

Book Electrochemical Methods

    Book Details:
  • Author : Allen J. Bard
  • Publisher : Wiley Global Education
  • Release : 2012-04-13
  • ISBN : 1118312805
  • Pages : 862 pages

Download or read book Electrochemical Methods written by Allen J. Bard and published by Wiley Global Education. This book was released on 2012-04-13 with total page 862 pages. Available in PDF, EPUB and Kindle. Book excerpt: Das führende Werk auf seinem Gebiet - jetzt durchgängig auf den neuesten Stand gebracht! Die theoretischen Grundlagen der Elektrochemie, erweitert um die aktuellsten Erkenntnisse in der Theorie des Elektronentransfers, werden hier ebenso besprochen wie alle wichtigen Anwendungen, darunter modernste Verfahren (Ultramikroelektroden, modifizierte Elektroden, LCEC, Impedanzspektrometrie, neue Varianten der Pulsvoltammetrie und andere). In erster Linie als Lehrbuch gedacht, läßt sich das Werk aber auch hervorragend zum Selbststudium und zur Auffrischung des Wissensstandes verwenden. Lediglich elementare Grundkenntnisse der physikalischen Chemie werden vorausgesetzt.

Book Guide Through the Nanocarbon Jungle

Download or read book Guide Through the Nanocarbon Jungle written by David Tománek and published by Iop Concise Physics. This book was released on 2014-02 with total page 106 pages. Available in PDF, EPUB and Kindle. Book excerpt: Buckyball, onion, nanobud, peapod - what are these buzzwords about? was a question posed to me many times over the last decade or two. This concise glossary is designed to provide the first answer to these and similar questions, and be a guide through th

Book Nanotechnology Applications to Telecommunications and Networking

Download or read book Nanotechnology Applications to Telecommunications and Networking written by Daniel Minoli and published by John Wiley & Sons. This book was released on 2005-11-07 with total page 509 pages. Available in PDF, EPUB and Kindle. Book excerpt: Be a part of the nanotechnology revolution in telecommunications This book provides a unique and thought-provoking perspective on how nanotechnology is poised to revolutionize the telecommunications, computing, and networking industries. The author discusses emerging technologies as well as technologies under development that will lay the foundation for such innovations as: * Nanomaterials with novel optical, electrical, and magnetic properties * Faster and smaller non-silicon-based chipsets, memory, and processors * New-science computers based on Quantum Computing * Advanced microscopy and manufacturing systems * Faster and smaller telecom switches, including optical switches * Higher-speed transmission phenomena based on plasmonics and other quantum-level phenomena * Nanoscale MEMS: micro-electro-mechanical systems The author of this cutting-edge publication has played a role in the development of actual nanotechnology-based communication systems. In this book, he examines a broad range of the science of nanotechnology and how this field will affect every facet of the telecommunications and computing industries, in both the near and far term, including: * Basic concepts of nanotechnology and its applications * Essential physics and chemistry underlying nanotechnology science * Nanotubes, nanomaterials, and nanomaterial processing * Promising applications in nanophotonics, including nanocrystals and nanocrystal fibers * Nanoelectronics, including metal nanoclusters, semiconducting nanoclusters, nanocrystals, nanowires, and quantum dots This book is written for telecommunications professionals, researchers, and students who need to discover and exploit emerging revenue-generating opportunities to develop the next generation of nanoscale telecommunications and network systems. Non-scientists will find the treatment completely accessible. A detailed glossary clarifies unfamiliar terms and concepts. Appendices are provided for readers who want to delve further into the hard-core science, including nanoinstrumentation and quantum computing. Nanotechnology is the next industrial revolution, and the telecommunications industry will be radically transformed by it in a few years. This is the publication that readers need to understand how that transformation will happen, the science behind it, and how they can be a part of it.

Book Nano Optics for Enhancing Light Matter Interactions on a Molecular Scale

Download or read book Nano Optics for Enhancing Light Matter Interactions on a Molecular Scale written by Baldassare Di Bartolo and published by Springer. This book was released on 2012-12-04 with total page 470 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume presents a considerable number of interrelated contributions dealing with the new scientific ability to shape and control matter and electromagnetic fields on a sub-wavelength scale. The topics range from the fundamental ones, such as photonic metamateriials, plasmonics and sub-wavelength resolution to the more applicative, such as detection of single molecules, tomography on a micro-chip, fluorescence spectroscopy of biological systems, coherent control of biomolecules, biosensing of single proteins, terahertz spectroscopy of nanoparticles, rare earth ion-doped nanoparticles, random lasing, and nanocoax array architecture. The various subjects bridge over the disciplines of physics, biology and chemistry, making this volume of interest to people working in these fields. The emphasis is on the principles behind each technique and on examining the full potential of each technique. The contributions that appear in this volume were presented at a NATO Advanced Study Institute that was held in Erice, Italy, 3-18 July, 2011. The pedagogical aspect of the Institute is reflected in the topics presented in this volume.

Book Kelvin Probe Force Microscopy

Download or read book Kelvin Probe Force Microscopy written by Sascha Sadewasser and published by Springer Science & Business Media. This book was released on 2011-10-22 with total page 334 pages. Available in PDF, EPUB and Kindle. Book excerpt: Over the nearly 20 years of Kelvin probe force microscopy, an increasing interest in the technique and its applications has developed. This book gives a concise introduction into the method and describes various experimental techniques. Surface potential studies on semiconductor materials, nanostructures and devices are described, as well as application to molecular and organic materials. The current state of surface potential at the atomic scale is also considered. This book presents an excellent introduction for the newcomer to this field, as much as a valuable resource for the expert.

Book Surface Enhanced Vibrational Spectroscopy

Download or read book Surface Enhanced Vibrational Spectroscopy written by Ricardo Aroca and published by John Wiley & Sons. This book was released on 2006-05-01 with total page 260 pages. Available in PDF, EPUB and Kindle. Book excerpt: Surface Enhanced Vibrational Spectroscopy (SEVS) has reached maturity as an analytical technique, but until now there has been no single work that describes the theory and experiments of SEVS. This book combines the two important techniques of surface-enhanced Raman scattering (SERS) and surface-enhanced infrared (SEIR) into one text that serves as the definitive resource on SEVS. Discusses both the theory and the applications of SEVS and provides an up-to-date study of the state of the art Offers interpretations of SEVS spectra for practicing analysts Discusses interpretation of SEVS spectra, which can often be very different to the non-enhanced spectrum - aids the practicing analyst