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Book Standard Test Method for Total Mercury in Crude Oil Using Combustion and Direct Cold Vapor Atomic Absorption Method with Zeeman Background Correction

Download or read book Standard Test Method for Total Mercury in Crude Oil Using Combustion and Direct Cold Vapor Atomic Absorption Method with Zeeman Background Correction written by and published by . This book was released on with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Handbook of Petroleum Product Analysis

Download or read book Handbook of Petroleum Product Analysis written by James G. Speight and published by John Wiley & Sons. This book was released on 2015-02-02 with total page 368 pages. Available in PDF, EPUB and Kindle. Book excerpt: Introduces the reader to the production of the products in a refinery • Introduces the reader to the types of test methods applied to petroleum products, including the need for specifications • Provides detailed explanations for accurately analyzing and characterizing modern petroleum products • Rewritten to include new and evolving test methods • Updates on the evolving test methods and new test methods as well as the various environmental regulations are presented

Book Determination of Total Mercury in Crude Oil by Combustion Cold Vapor Atomic Absorption Spectrometry  CVAAS

Download or read book Determination of Total Mercury in Crude Oil by Combustion Cold Vapor Atomic Absorption Spectrometry CVAAS written by BS. Fox and published by . This book was released on 2005 with total page 11 pages. Available in PDF, EPUB and Kindle. Book excerpt: Unlike many heavy metals, mercury is a long-range air and water pollutant whose load on the environment is increasing. According to published reports, a major source of atmospheric mercury is the burning of coal for electrical power generation. However, certain crude oils may contain up to several hundred ng/g of total mercury. Accurate analysis of total mercury in crude oil is the first step in determining the value of a crude oil and one's ability to process the material within the refinery, while generating finished products. This paper details the use of Combustion Cold Vapor Atomic Absorption Spectrometry (CVAAS) technology for the analysis of crude samples and distillation cuts. The instrument described in the report is one of several instrument methods currently being evaluated by groups in industry and government. The use of a boat-inlet sample introduction system allows crude oil and other types of material to be analyzed without acid digestion. The strengths and weaknesses of the combustion-CVAAS technique, along with a year's worth of operating experience, will be presented from the user's perspective.

Book Measurement of Total Mercury in Air

Download or read book Measurement of Total Mercury in Air written by Association canadienne de normalisation and published by . This book was released on 1987 with total page 29 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Measurement of Total Mercury in Air   Cold Vapour Atomic Absorption Spectrophotometric Method

Download or read book Measurement of Total Mercury in Air Cold Vapour Atomic Absorption Spectrophotometric Method written by Canadian Standards Association and published by Rexdale, Ont. : The Association. This book was released on 1987 with total page 29 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Mercury  Ultra Trace Analysis

Download or read book Mercury Ultra Trace Analysis written by Dr. Paul Gouda and published by iUniverse. This book was released on 2013-06-19 with total page 145 pages. Available in PDF, EPUB and Kindle. Book excerpt: Dr. Paul H. Ramses Gouda, is a globally renowned chemist who authored several science books and papers. He has been credited with the foundation of several analytical laboratory procedures utilizing Atomic Absorption and Inductively Coupled Plasma for ultra trace analysis of As, Se, Sb &Hg. These Methods were officially adopted by EPL and by other agencies, and as routinely practiced in the scientific arena they were named after him. The author, who first attended medical school before specializing in analytical chemistry and pharmacological research, has acquired two doctorates. His contributions to the scientific community include a recent paper on the unique concept of the duplication and manipulation of neurological compounds to trigger a natural and optimum physiological response. Tour the authors books at and his book-signing sessions at www.goudabooks.com and his science project, scheduled symposiums & seminars at www.optimumgreen.com This book offers a complete coverage of mercury analysis methodology. An analytical laboratory reference, a chemist manual, and a university textbook. A must for every library.

Book Determination of Mercury in Water by Cold Vapor Atomic Absorption Spectrometry

Download or read book Determination of Mercury in Water by Cold Vapor Atomic Absorption Spectrometry written by United States. Environmental Protection Agency. Office of Research and Development and published by . This book was released on 1991 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Determination of Mercury in Tissues by Cold Vapor Atomic Absorption Spectrometry

Download or read book Determination of Mercury in Tissues by Cold Vapor Atomic Absorption Spectrometry written by United States. Environmental Protection Agency. Office of Research and Development and published by . This book was released on 1991 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Comparison of Adsorbed Mercury Screening Method With Cold Vapor Atomic Absorption Spectrophotometry for Determination of Mercury in Soil

Download or read book Comparison of Adsorbed Mercury Screening Method With Cold Vapor Atomic Absorption Spectrophotometry for Determination of Mercury in Soil written by and published by . This book was released on 2000 with total page 20 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Method 1631

Download or read book Method 1631 written by and published by . This book was released on 1995 with total page 44 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Determination of Low level Mercury by Cold Vapor Generation and Atomic Absorption Spectroscopy

Download or read book Determination of Low level Mercury by Cold Vapor Generation and Atomic Absorption Spectroscopy written by and published by . This book was released on 1977 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: A procedure for determining mercury in liquid samples by cold vapor flameless atomic absorption spectroscopy was developed. The optimum parameter values were determined and mercury standard storage conditions investigated. The effect and tolerance levels of twenty-seven ions, including those ions common to Tank Farm Operations and the Synthetic Wastes, were measured. Standard deviation for the procedure is less than 1%. The procedure can be used to determine mercury at the part per billion level in any liquid sample, a thousand-fold increase in sensitivity over current flame techniques.

Book Evaluation of SW 846 Cold Vapor Mercury Methods 7470 and 7471

Download or read book Evaluation of SW 846 Cold Vapor Mercury Methods 7470 and 7471 written by WF. Beckert and published by . This book was released on 1990 with total page 12 pages. Available in PDF, EPUB and Kindle. Book excerpt: The protocols for Methods 7470 and 7471 in the SW-846 methods manual are designed for the cold-vapor atomic absorption spectrometric (CV-AAS) determination of total mercury in aqueous (extracts, wastewater, ground water, etc.) and solid (soils, sediments, sludges, etc.) materials, respectively. Aqueous samples are digested with a combination of nitric and sulfuric acid plus permanganate and persulfate solutions at elevated temperature; solid samples are heated either on a steam bath with aqua regia and permanganate, or in an autoclave with sulfuric acid, nitric acid and permanganate. The mercuric ions in the digests are then reduced with hydroxylamine, and the elemental mercury is aerated into the AAS cell, either in a closed (recirculating) or an open system, where the absorption at 253.7 nm is determined.

Book Standard Test Method for Total Mercury in Water

Download or read book Standard Test Method for Total Mercury in Water written by and published by . This book was released on 2007 with total page 7 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Interlaboratory Study of the Cold Vapor Technique for Total Mercury in Water

Download or read book Interlaboratory Study of the Cold Vapor Technique for Total Mercury in Water written by HA. Clements and published by . This book was released on 1975 with total page 15 pages. Available in PDF, EPUB and Kindle. Book excerpt: The American Society for Testing and Materials (ASTM) and the U.S. Environmental Protection Agency (EPA) conducted a joint study of the cold vapor technique for total mercury in water, before formal acceptance of the method by each organization. The method employs an acid-permanganate-persulfate oxidation step with heat.

Book Mercury determination in gasoline by cold vapor and aas with direct reduction in microemulsion

Download or read book Mercury determination in gasoline by cold vapor and aas with direct reduction in microemulsion written by and published by . This book was released on 2003 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Foi estudada a determinação de mercúrio em gasolina pela técnica do vapor frio, com redução em meio orgânico e de solução de três componentes (microemulsão). Foram utilizadas várias metodologias empregando a técnica degeração de vapor frio e detecção em espectrômetro de absorção atômica, a saber: determinação direta em gasolina; determinação direta em gasolina estabilizada na forma de microemulsão, com e sem pré-concentração em rede de ouro; edeterminação direta em gasolina estabilizada na forma de microemulsão utilizando uma armadilha para vapores de gasolina antes da pré-concentração em rede de ouro. Analisando os resultados, foi verificado que a determinação de mercúrio em gasolina estabilizada na forma de microemulsão fornece medidas mais repetitivas do que em gasolina in natura; além disso, foi observada anecessidade de utilizar pré-concentração em rede de ouro, devido aos baixos níveis de mercúrio em gasolina; entretanto, foi detectado que os vapores de gasolina envenenam o ouro. Dentre as armadilhas estudadas para evitar o envenenamento do ouro, foi escolhida a armadilha com solução de K2Cr2O7/H2SO4, na qual, os vapores rovenientes do frasco de reação foram borbulhados eo Hg0, oxidado; posteriormente, a solução foi reduzida com SnCl2/ H2SO4 e os vapores enviados para a rede de ouro. Assim, os resultados indicaram que o método para determinação de mercúrio total em gasolina, no qual o mercúrio é reduzido diretamente da gasolina como microemulsão, utilizando armadilha de K2Cr2O7/H2SO4 antes da pré-concentração em ouro, com detecção por CV-AAS, érecomendado. Após uma otimização multivariada, curvas analíticas apresentaram coeficientes de correlação de até 0,9999 com uma massa característica correspondente de 2ng de mercúrio. O limite de detecção obtido por este métodofoi de 0,10 ng/mL (0,14 ng/g).