Download or read book Revised Final Report for Tank 241 AN 101 Grab Samples 1AN 95 1 Through 1AN 95 7 Revision 1 written by and published by . This book was released on 2001 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Six supernate grab samples and one field blank were taken from tank 241-AN-101. This report documents analyses performed in support of the Safety Screening program: differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), density by specific gravity (Sp. G.), and total alpha activity (AT).

Download or read book Final Report for Tank 241 AP 101 Grab Samples 1AP 95 1 1AP 95 2 1AP 95 3 1AP 95 4 1AP 95 5 and 1AP 95 6 written by and published by . This book was released on 1996 with total page 711 pages. Available in PDF, EPUB and Kindle. Book excerpt: Six supernate grab samples (1AP-95-1 through 6) and one field blank (1AP-95-7) were taken from tank 241-AP-101, on Nov. 10 and 13, 1995. Analyses were performed in support of the Safety Screening and the Waste Compatibility Safety programs. All analytical results were within the action limits stated in the TSAP.

Download or read book Tank 241 AN 101 Grab Samples 1AN 98 1 1AN 98 2 and 1AN 98 3 Analytical Results for the Final Report written by and published by . This book was released on 2002 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: This document is the final report for tank 241-AN-101 grab samples. Three grab samples 1AN-98-1, 1AN-98-2 and 1AN-98-3 were taken from riser 16 of tank 241-AN-101 on April 8, 1998 and received by the 222-S Laboratory on April 9, 1998. Analyses were performed in accordance with the ''Compatability Grab Sampling and Analysis Plan'' (TSAP) and the ''Data Quality Objectives for Tank Farms Waste Compatability Program'' (DQO). The analytical results are presented in the data summary report. No notification limits were exceeded.

Download or read book Final Report for Tank 241 AN 102 Grab Samples 2AN 95 1 Through 2AN 95 6 and 102 AN 1 Through 102 AN 4 written by and published by . This book was released on 1996 with total page 862 pages. Available in PDF, EPUB and Kindle. Book excerpt: Ten grab samples (2AN-95-1, 2, 3, 4A, 5A; 102-AN-1, 2, 3(A), 3(B), and 4) and one field blank (2AN-95-6) were taken from tank 241-AN-102. In support of the safety screening program, total organic carbon and cyanide were performed as secondary analyses because the differential scanning calorimetry results exceeded the notification limit. These were compared to safety screening limits at a confidence level of 95%. Waste compatibility analyses were performed on the 3 supernate samples and the field blank from the latest sampling event. Results presented in the 45 day and in this report show that the waste in Tank 241-AN-1D2 has energetics greater than 480 J/g (dry) and total organic carbon> 3 wt%; however, with a moisture content> 17 wt%, the tank may be considered c̀̀onditionally ̀̀safe in accordance with the Data Quality Objective to Support Resolution of the Organic Complexant Safety Issue.

Download or read book Final Report for Tank 241 AY 101 Grab Samples 1AY 96 1 Through 1AY 96 10 and 1AY 96 FB written by and published by . This book was released on 1996 with total page 1223 pages. Available in PDF, EPUB and Kindle. Book excerpt: This report contains tables of the analytical results from grab samples from tank 241-AY-101. Activity levels of radionuclides are tabulated. This tanks has not been watch listed.

Download or read book Waste Compatibility and Final Report for Tank 241 A 101 Grab Samples 1A 96 1 1A 96 2 and 1A 96 3 written by and published by . This book was released on 2001 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: This document is the final report deliverable for tank 241-A- 101 grab samples. Three grab samples (IA-96-1, IA-96-2 and IA-96-3) were taken from riser 4 of tank 241-A-101. Samples were collected on April 3, 1996 and received by the 222-S Laboratory on April 4, 1996. Analyses were performed in accordance with the Compatibility Grab Sampling and Analysis Plan (TSAP) and the Data Quality Objectives for Tank Farms Waste Compatibility Program (DQO). The samples were subsampled and analyzed in accordance with the TSAP. Two of the three grab samples contained a significant amount of solids and special analyses were requested. None of the samples exceeded notification limits. No similarities in sample appearance were noted; this could be an explanation for the varying analytical results. Quality control issues are discussed in each analytical subheading. The raw data for all analyses are included in this report.

Download or read book Tank 241 AX 101 Grab Samples 1AX 97 1 Through 1AX 97 3 Analytical Results for the Final Report written by and published by . This book was released on 1997 with total page 459 pages. Available in PDF, EPUB and Kindle. Book excerpt: This document is the final report for tank 241-AX-101 grab samples. Four grab samples were collected from riser 5B on July 29, 1997. Analyses were performed on samples 1AX-97-1, 1AX-97-2 and 1AX-97-3 in accordance with the Compatibility Grab Sampling and Analysis Plan (TSAP) and the Data Quality Objectives for Tank Farms Waste Compatibility Program (DQO) (Rev. 1: Fowler, 1995; Rev. 2: Mulkey and Miller, 1997). The analytical results are presented in Table 1. No notification limits were exceeded. All four samples contained settled solids that appeared to be large salt crystals that precipitated upon cooling to ambient temperature. Less than 25 % settled solids were present in the first three samples, therefore only the supernate was sampled and analyzed. Sample 1AX-97-4 contained approximately 25.3 % settled solids. Compatibility analyses were not performed on this sample. Attachment 1 is provided as a cross-reference for relating the tank farm customer identification numbers with the 222-S Laboratory sample numbers and the portion of sample analyzed. Table 2 provides the appearance information. All four samples contained settled solids that appeared to be large salt crystal that precipitated upon cooling to ambient temperature. The settled solids in samples 1AX-97-1, 1AX-97-2 and 1AX-97-3 were less than 25% by volume. Therefore, for these three samples, two 15-mL subsamples were pipetted to the surface of the liquid and submitted to the laboratory for analysis. In addition, a portion of the liquid was taken from each of the these three samples to perform an acidified ammonia analysis. No analysis was performed on the settled solid portion of the samples. Sample 1AX-97-4 was reserved for the Process Chemistry group to perform boil down and dissolution testing in accordance with Letter of Instruction for Non-Routine Analysis of Single-Shell Tank 241-AX-101 Grab Samples (Field, 1997) (Correspondence 1). However, prior to the analysis, the sample was inadvertently archived and the solid portion was not represented in the archive.

Download or read book Final Report for Tank 241 BY 103 Auger Samples 95 AUG 012 and 95 AUG 013 Revision 1 written by and published by . This book was released on 1995 with total page 93 pages. Available in PDF, EPUB and Kindle. Book excerpt: This document summarizes the sampling activities for tank 241-BY-103.

Download or read book Final Report for Tank 241 B 112 Auger Samples 95 AUG 014 and 95 AUG 015 Revision 1 written by and published by . This book was released on 1995 with total page 110 pages. Available in PDF, EPUB and Kindle. Book excerpt: This document reports the sampling events for tank 241-B-112.

Download or read book 222 S Analytical Services Final Results for Tank 241 U 101 Grab Samples 1U 96 1 Through 1U 96 4 written by and published by . This book was released on 1996 with total page 185 pages. Available in PDF, EPUB and Kindle. Book excerpt: This document is the final, format IV, laboratory report for characterization of tank 241-U-101 (U-101) grab samples from risers 1 and 7. It transmits additional analytical data for specific gravity (Sp. G.), and all raw analytical data which were not provided in the 45-day report. The 45-day report is attached to this final report as Part II. Secondary analyses were not performed on any of the U-101 samples. This is because none of the primary analyte limits, which trigger the performance of secondary analyses, were exceeded. Grab samples were taken on May 29, 1996 and May 30, 1996 from risers 1 and 7, respectively, and were received at the 222-S Laboratory on the same days that they were collected. Analyses were performed in accordance with the Tank Sampling and Analysis Plan (TSAP) for this tank and the Safety Screening Data Quality Objective (DQO). The samples were analyzed for differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), total alpha activity (AT), visual appearance, bulk density, and specific gravity. A sample data summary table, includes sample analytical data accompanied by quality control data (for example, duplicate, spike, blank and standard results and detection limits and counting efforts). The table includes data for DSC, TGA, AT, bulk density, volume percent solids and Sp. G. analyses. Data regarding the visual appearance of samples, volume percent solids and density of the solids are provided in tabular form of the 45-day report (attached as Part II). The table of the 45-day report also associates the original customer sample number with corresponding laboratory sample numbers. The TSAP specified notification limits for only DSC and total alpha. Notification limits were not exceeded for DSC or total alpha analyses for any of the samples, consequently immediate notifications were not necessary and were not made.

Download or read book Tank 214 AW 105 Grab Samples Analytical Results for the Finalreport written by and published by . This book was released on 2001 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: This document is the final report for tank 241-AW-105 grab samples. Twenty grabs samples were collected from risers 10A and 15A on August 20 and 21, 1996, of which eight were designated for the K Basin sludge compatibility and mixing studies. This document presents the analytical results for the remaining twelve samples. Analyses were performed in accordance with the Compatibility Grab Sampling and Analysis Plan (TSAP) and the Data Quality Objectives for Tank Farms Waste Compatibility Program (DO). The results for the previous sampling of this tank were reported in WHC-SD-WM-DP-149, Rev. 0, 60-Day Waste Compatibility Safety Issue and Final Results for Tank 241-A W-105, Grab Samples 5A W-95-1, 5A W-95-2 and 5A W-95-3. Three supernate samples exceeded the TOC notification limit (30,000 microg C/g dry weight). Appropriate notifications were made. No immediate notifications were required for any other analyte. The TSAP requested analyses for polychlorinated biphenyls (PCB) for all liquids and centrifuged solid subsamples. The PCB analysis of the liquid samples has been delayed and will be presented in a revision to this document.

Download or read book Tank 241 AP 107 Grab Samples 7AP 97 1 7AP 97 2 and 7AP 97 3 Analytical Results for the Final Report written by and published by . This book was released on 2005 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: This document is the final report for tank 241-AP-107 grab samples. Three grab samples were collected from riser 1 on September 11, 1997. Analyses were performed on samples 7AP-97-1, 7AP-97-2 and 7AP-97-3 in accordance with the Compatibility Grab Sampling and Analysis Plan (TSAP) (Sasaki, 1997) and the Data Quality Objectives for Tank Farms Waste Compatibility Program (DQO) (Rev. 1: Fowler, 1995; Rev. 2: Mulkey and Nuier, 1997). The analytical results are presented in the data summary report (Table 1). A notification was made to East Tank Farms Operations concerning low hydroxide in the tank and a hydroxide (caustic) demand analysis was requested. The request for sample analysis (RSA) (Attachment 2) received for AP-107 indicated that the samples were polychlorinated biphenyl (PCB) suspects. Therefore, prior to performing the requested analyses, aliquots were made to perform PCB analysis in accordance with the 222-S Laboratory administrative procedure, LAP-101-100. The results of this analysis indicated that no PCBs were present at 50 ppm and analysis proceeded as non-PCB samples. The results and raw data for the PCB analysis will be included in a revision to this document. The sample breakdown diagrams (Attachment 1) are provided as a cross-reference for relating the tank farm customer identification numbers with the 222-S Laboratory sample numbers and the portion of sample analyzed.

Download or read book Tank 241 AP 106 Grab Samples 6AP 96 1 Through 6AP 96 3 Analytical Results for the Final Report written by and published by . This book was released on 1996 with total page 282 pages. Available in PDF, EPUB and Kindle. Book excerpt: This document is the final report for tank 241-AP-106 grab samples. This document presents the analytical results for three samples (6AP-96-1, 6AP-96-2 and 6AP-96-3) taken from riser 1 @ 150° of tank 241-AP-1 06 on September 12, 1996. Analyses were performed in accordance with the Compatibility Grab Sampling and Analysis Plan (TSAP) (Sasaki, 1996) and the Data Quality Objectives for Tank Farms Waste Compatibility Program (DQO) (Fowler, 1995).

Download or read book Revised Final Report for Tank 241 C 203 Auger Samples 95 AUG 20 and 95 AUG 21 Revision 1 written by and published by . This book was released on 1995 with total page 131 pages. Available in PDF, EPUB and Kindle. Book excerpt: Two auger samples from tank 241-C-203 (C-203) were received at the 222-S Laboratories and underwent safety screening analyses, consisting of differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), and total alpha activity. No notification limits were exceeded for the analyses. Two samples were submitted for a density determination at the request of Characterization Plant Engineering. SCOPE This document is the revised final report for the tank C-203 auger samples collected on April 5, 1995 (samples 95-AUG-20 and 95-AUG-021).

Download or read book Tank 241 ER 311 Grab Samples ER311 98 1 ER311 98 2 ER311 98 3 Analytical Results for the Final Report written by and published by . This book was released on 2002 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: This document is the final report for catch tank 241-ER-311 grab samples. Three grab samples ER311-98-1, ER311-98-2 and ER311-98-3 were taken from East riser of tank 241-ER-311 on August 4, 1998 and received by the 222-S Laboratory on August 4, 1998. Analyses were performed in accordance with the Compatibility Grab Sampling and Analysis Plan (TSAP) (Sasaki, 1998)and the Data Quality Objectives for Tank Farms Waste Compatibility Program (DQO) (Mulkey and Miller, 1997). The analytical results are presented in the data summary report (Table 1). No notification limits were exceeded.

Download or read book Final Report for Tank 241 B 101 Push Mode Cores 90 and 91 Revision 1 written by and published by . This book was released on 2001 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: This is the final report for tank 241-@101, cores 90 and 91. Samples from these cores were analyzed for safety screening purposes in accordance with the Tank 241-B-101 Tank Characterization Plan (TCP) (Reference 1). This final report contains the results for three sets of TGA and gravimetric analyses performed after the 90-day report was issued. Two of these TGA/gravimetric percent water sets of analyses were done because low original TGA results were obtained for the lower half segment of core 90, segment 2 and the facie of core 91, segment 2; the third set of analyses were performed because the TGA and gravimetric percent water results for the upper half segment of core 90, segment 2 differed by approximately a factor of three and further investigation was warranted.

Download or read book Tank 241 S 302 Grab Samples 302S 97 1 302S 97 2 and 302S 97 3 Analytical Results for the Final Report written by and published by . This book was released on 1998 with total page 332 pages. Available in PDF, EPUB and Kindle. Book excerpt: This document is the final report for tank 241-S-302 grab samples. Three grab samples were collected on January 30, 1998. Analyses were performed on samples 302-S-97-1, 302-S-97-2 and 302-S-97-3 in accordance with the Compatibility Grab Sampling and Analysis Plan (TSAP) (Sasaki, 1997) and the Data Quality Objectives (DQO) for Tank Farms Waste Compatibility Program (Mulkey, 1997). The analytical results are presented in Table 1. No notification limits were exceeded. The sample breakdown diagrams (Attachment 1) are provided as a cross-reference for relating the tank farm customer identification numbers with the 222-S Laboratory sample numbers and the portion of sample analyzed. Table 2 provides the appearance information. Visual observation indicated that the sample was a clear, light-yellow liquid with less than one percent solids. No organic layer was observed. The 125 mL sample was submitted to the laboratory for analysis of inorganic analytes and radionuclides.