Download or read book Novel Pulse Methods for Multidimensional NMR Imaging and Spectroscopy written by Michael D. Cockman and published by . This book was released on 1988 with total page 378 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Download or read book Pulse and Fourier Transform NMR written by Thomas C. Farrar and published by Elsevier. This book was released on 2012-12-02 with total page 132 pages. Available in PDF, EPUB and Kindle. Book excerpt: Pulse and Fourier Transform NMR: Introduction to Theory and Methods presents the different types of pulse experiments that are commonly used and provides the theoretical background necessary for understanding these techniques. This book evaluates the practical application of pulse methods and the necessary instrumentation. Organized into seven chapters, this book begins with an overview of the NMR fundamentals and the basic pulse methods. This text then summarizes the important features of pulse spectrometers. Other chapters consider the rationale, the advantages, and the limitations of Fourier transform NMR methods. This book discusses as well how the idea of the rotating frame can be utilized to understand certain experiments that extend the range of application of pulse methods. The final chapter deals with a few significant special uses of pulse techniques. This book is a valuable resource for chemists and readers who are familiar with high resolution NMR but with no background in pulse methods.

Download or read book Multidimensional NMR Methods for the Solution State written by Gareth A. Morris and published by John Wiley & Sons. This book was released on 2012-12-19 with total page 877 pages. Available in PDF, EPUB and Kindle. Book excerpt: The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the ultimate online resource for NMR and MRI. The literature of multidimensional NMR began with the publication of three papers in 1975, then nine in 1976 and fifteen in 1977, and now contains many tens of thousands of papers. Any attempt to survey the field must therefore necessarily be very selective, not to say partial. In assembling this handbook, the Editors have sought to provide both the new researcher and the established scientist with a solid foundation for the understanding of multidimensional NMR, a representative if inevitably limited survey of its applications, an authoritative account of classic techniques such as COSY, NOESY and TOSCY, and an account of the latest progress in the development of multidimensional techniques. This handbook is structured in four parts. The first opens with an historical introduction to, and a brief account of, the practicalities and applications of multidimensional NMR methods, followed by a definitive survey of their conceptual basis and a series of articles setting out the generic principles of methods for acquiring and processing multidimensional NMR data. In the second part, the main families of multidimensional techniques, arranged in approximate order of increasing complexity, are described in detail, from simple J-resolved spectroscopy through to the powerful heteronuclear 3D and 4D methods that now dominate the study of structural biology in solution. The third part offers and illustrative selection from the very wide range of applications of multidimensional NMR methods, including some of the most recent developments in protein NMR. Finally, the fourth part introduces the idea of multidimensional spectra containing non-frequency dimensions, in which properties such as diffusion and relaxation are correlated. About EMR Handbooks / eMagRes Handbooks The Encyclopedia of Magnetic Resonance (up to 2012) and eMagRes (from 2013 onward) publish a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks / eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of articles from eMagRes. In consultation with the eMagRes Editorial Board, the EMR Handbooks / eMagRes Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry. Have the content of this Handbook and the complete content of eMagRes at your fingertips! Visit: www.wileyonlinelibrary.com/ref/eMagRes View other eMagRes publications here

Download or read book Multidimensional NMR in Liquids written by Frank J. M. van de Ven and published by Wiley-VCH. This book was released on 1995 with total page 432 pages. Available in PDF, EPUB and Kindle. Book excerpt: Multidimensional NMR in Liquids offers a lucid treatment of basic NMR phenomena, building up to today's most sophisticated NMR experiments from first principles. Using easy-to-grasp product-operator formalism, diagrams, and practical examples, one-, two-, and N-dimensional NMR experiments are explained with minimal recourse to quantum mechanics.

Download or read book Nuclear Magnetic Resonance written by Daniel Canet and published by Wiley. This book was released on 1996-07-10 with total page 270 pages. Available in PDF, EPUB and Kindle. Book excerpt: Emphasizes the physical and mathematical features of liquid state NMR spectroscopy which underpin the numerous important applications of the technique. Details of some of these applications, such as structural determination from small organic molecules to large biomolecules, the study of molecular motions and NMR imaging then follow. Detailed examples and figures throughout the text enable the student to grasp conceptually challenging ideas, while the most advanced mathematical and quantum concepts are presented so that they can be skipped on a first reading without impeding a global understanding of the key concepts.

Download or read book Annual Reports on NMR Spectroscopy written by and published by Elsevier. This book was released on 2024-07-11 with total page 208 pages. Available in PDF, EPUB and Kindle. Book excerpt: Annual Reports on NMR Spectroscopy, Volume 111 presents the latest release in a series that has established itself as a premier resource for both specialists and non-specialists interested in new techniques and applications pertaining to NMR spectroscopy. Chapters in this new release include Electrophoretic NMR, Traceability and uncertainty in NMR measurements, Quantitative NMR Spectroscopy, Advances in Non-Uniform Sampling NMR, NMR spectroscopy of natural and synthetic fibers, Characterization of transition alkane complexes, and Recent applications of low field NMR to membrane science. Serves as the premier resource for learning new techniques and applications in NMR spectroscopy Provides a key reference for chemists and physicists using NMR spectroscopy to study the structure and dynamics of molecules Covers all aspects of molecular science, including MRI (Magnetic Resonance Imaging)

Download or read book Novel Methods for Modern NMR Spectroscopy Optimized Pulses and New Experiments written by Martin R. M. Koos and published by . This book was released on 2017 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:

Download or read book Signal Treatment and Signal Analysis in NMR written by D.N. Rutledge and published by Elsevier. This book was released on 1996-06-10 with total page 567 pages. Available in PDF, EPUB and Kindle. Book excerpt: Signal analysis and signal treatment are integral parts of all types of Nuclear Magnetic Resonance. In the last ten years, much has been achieved in the development of dimensional spectra. At the same time new NMR techniques such as NMR Imaging and multidimensional spectroscopy have appeared, requiring entirely new methods of signal analysis. Up until now, most NMR texts and reference books limited their presentation of signal processing to a short introduction to the principles of the Fourier Transform, signal convolution, apodisation and noise reduction. To understand the mathematics of the newer signal processing techniques, it was necessary to go back to the primary references in NMR, chemometrics and mathematics journals. The objective of this book is to fill this void by presenting, in a single volume, both the theory and applications of most of these new techniques to Time-Domain, Frequency-Domain and Space-Domain NMR signals. Details are provided on many of the algorithms used and a companion CD-ROM is also included which contains some of the computer programs, either as source code or in executable form. Although it is aimed primarily at NMR users in the medical, industrial and academic fields, it should also interest chemometricians and programmers working with other techniques.

Download or read book Experimental Pulse NMR written by Eiichi Fukushima and published by CRC Press. This book was released on 2018-03-08 with total page 290 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is about pulse nuclear magnetic resonance (NMR), with its techniques, the information to be obtained, and practical advice on performing experiments. The emphasis is on the motivation and physical ideas underlying NMR experiments and the actual techniques, including the hardware used. The level is generally suitable for those to whom pulse NMR is a new technique, be they students in chemistry or physics on the one hand and research workers in biology, geology, or agriculture, on the other. The book can be used for a senior or first year graduate course where it could supplement the standard NMR texts.

Download or read book Nuclear Magnetic Resonance Spectroscopy written by Joseph B. Lambert and published by John Wiley & Sons. This book was released on 2019-01-04 with total page 485 pages. Available in PDF, EPUB and Kindle. Book excerpt: Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.

Download or read book An Introduction to Pulse NMR Spectroscopy written by Thomas C. Farrar and published by . This book was released on 1989-09-01 with total page 211 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Download or read book Nuclear Magnetic Resonance Probes of Molecular Dynamics written by R. Tycko and published by Springer Science & Business Media. This book was released on 1994-11-30 with total page 574 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nuclear Magnetic Resonance Probes of Molecular Dynamics describes the theoretical basis and experimental techniques that make modern NMR spectroscopy a powerful and flexible tool for probing molecular dynamics in chemical, physical, and biochemical systems. Individual chapters, written by leaders in the development and application of NMR from around the world, treat systems that range from synthetic polymers, liquid crystals, and catalysts to proteins and oligonucleotides and techniques that include deuterium NMR, magic angle spinning, multidimensional spectroscopy, and magnetic resonance imaging. A combination of elementary and advanced material makes the book a useful introduction to the field for students at the graduate level as well as an important reference for practising NMR spectroscopists.

Download or read book Novel Sampling Approaches in Higher Dimensional NMR written by Martin Billeter and published by Springer Science & Business Media. This book was released on 2012-03-16 with total page 166 pages. Available in PDF, EPUB and Kindle. Book excerpt: Concepts in Projection-Reconstruction, by Ray Freeman and Ēriks Kupče.- Automated Projection Spectroscopy and Its Applications, by Sebastian Hiller and Gerhard Wider.- Data Sampling in Multidimensional NMR: Fundamentals and Strategies, by Mark W. Maciejewski, Mehdi Mobli, Adam D. Schuyler, Alan S. Stern and Jeffrey C. Hoch.- Generalized Fourier Transform for Non-Uniform Sampled Data, by Krzysztof Kazimierczuk, Maria Misiak, Jan Stanek, Anna Zawadzka-Kazimierczuk and Wiktor Koźmiński.- Applications of Non-Uniform Sampling and Processing, by Sven G. Hyberts, Haribabu Arthanari and Gerhard Wagner

Download or read book Multinuclear NMR written by J. Mason and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 642 pages. Available in PDF, EPUB and Kindle. Book excerpt: With the power and range of modern pulse spectrometers the compass of NMR spec troscopy is now very large for a single book-but we have undertaken this. Our book covers the Periodic Table as multinuclear spectrometers do, and introductory chapters are devoted to the essentials of the NMR experiment and its products. Primary products are chemical shifts (including anisotropies), spin-spin coupling constants, and relaxation times; the ultimate product is a knowledge of content and constitution, dynamic as well as static. Our province is chemical and biochemical rather than physical or technical; only passing reference is made to metallic solids or unstable species, or to practical NMR spectroscopy. Our aim is depth as well as breadth, to explain the fundamental processes, whether of nuclear magnetic shielding, spin-spin coupling, relaxation, or the multiple pulse sequences that have allowed the development of high-resolution studies of solids, multidimensional NMR spectroscopy, techniques for sensitivity enhancement, and so on. This book therefore combines the functions of advanced textbook and reference book. For reasonably comprehensive coverage in a single volume we have sum marized the information in tables and charts, and included all leading references.

Download or read book Novel Methodology Applications In High Resolution NMR NMR Imaging written by Christy George and published by LAP Lambert Academic Publishing. This book was released on 2013 with total page 300 pages. Available in PDF, EPUB and Kindle. Book excerpt: Novel methodology developments and applications of a variety of spectroscopic and spatially resolved NMR experiments are presented here. NMR has poor sensitivity, especially for rare spins. We have developed novel relaxation optimized double quantum filtered transition selective experiments to improve the sensitivity of rare spin correlation spectroscopy: Low Abundance Single transition correlation SpectroscopY (LASSY) in direct detection mode and 1H Indirect detected Carbon Low Abundance Single transition correlation Spectroscopy (HICLASS) in the indirect detection mode. These approaches typically halve the measurement time to produce a given sensitivity, in comparison to INADEQUATE CR and ADEQUATE respectively. They may be applied to 13C, 29Si, Sn isotopes, 183W, 77Se, etc. Secondly, the time evolution of multiple quantum coherences under spin lock has been studied in spin-1/2 A2X2 systems, and is shown to result in 'amplified' homonuclear scalar couplings. Further, the utility of spatially resolved NMR, ie, MRI and MRS is demonstrated for electrochemical applications such as membrane permeability studies. Finally, flow field imaging of an H2-O2 fuel cell under load is presented

Download or read book Applications of Pulsed Field Gradient Techniques and Slice Selective Methods in NMR Spectroscopy written by Kaitlyn Doolittle and published by . This book was released on 2023 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: Slice selection NMR spectroscopy is a method that enables the chemical analysis of specific, selected regions of an NMR sample along the z-axis. This type of NMR spectroscopy has applications in metabolomics, kinetics, extractions analyses, and more. The focus of this work is the development of a novel slice selection experiment, called the one-shot double-slice experiment. This experiment enables the simultaneous analysis of two different regions within an NMR tube, with the ability to differentiate between the selected regions, due to the signals from each region being of opposite phase in the resulting NMR spectrum. Slice selection NMR is possible through the combination of pulsed field gradients and shaped pulses. In order to develop this methodology and novel experiment, it was first necessary to develop a deep understanding of those two fundamental components. Pulsed field gradients were investigated through diffusion NMR spectroscopy and one-dimensional NMR imaging. The diffusion experiments were conducted to determine the self-diffusion coefficients of surfactant at various concentrations, in order to further define the system beyond the critical micelle concentration (at which point surface tension no longer can provide insight as to changes in the system). The one-dimensional gradient imaging experiments were employed to determine the location of the receiver coil with respect to the interface of biphasic NMR samples, in order to optimize biphasic sample preparation. Biphasic samples of model compounds were then used to test out classic slice selection NMR experiments, and to test out the novel one-shot double-slice one-dimensional experiment and the two-dimensional TOCSY version that were developed through this work. Once the model compound biphasic sample experiments were proven successful, the experiments were expanded to more complex biphasic samples that are more representative of real-life samples. The samples used to test these experiments were in-tube extractions of tea leaves and of hot and cold brewed coffees. The result of this research is a novel experiment that provides information about two different regions (or phases, in the case of biphasic samples) simultaneously in a single experiment. This experiment was proven to be robust and easy to implement, and it presents new opportunities for the field of slice selection NMR spectroscopy.

Download or read book Encyclopedia of Spectroscopy and Spectrometry written by and published by Academic Press. This book was released on 2016-09-22 with total page 3716 pages. Available in PDF, EPUB and Kindle. Book excerpt: This third edition of the Encyclopedia of Spectroscopy and Spectrometry, Three Volume Set provides authoritative and comprehensive coverage of all aspects of spectroscopy and closely related subjects that use the same fundamental principles, including mass spectrometry, imaging techniques and applications. It includes the history, theoretical background, details of instrumentation and technology, and current applications of the key areas of spectroscopy. The new edition will include over 80 new articles across the field. These will complement those from the previous edition, which have been brought up-to-date to reflect the latest trends in the field. Coverage in the third edition includes: Atomic spectroscopy Electronic spectroscopy Fundamentals in spectroscopy High-Energy spectroscopy Magnetic resonance Mass spectrometry Spatially-resolved spectroscopic analysis Vibrational, rotational and Raman spectroscopies The new edition is aimed at professional scientists seeking to familiarize themselves with particular topics quickly and easily. This major reference work continues to be clear and accessible and focus on the fundamental principles, techniques and applications of spectroscopy and spectrometry. Incorporates more than 150 color figures, 5,000 references, and 300 articles for a thorough examination of the field Highlights new research and promotes innovation in applied areas ranging from food science and forensics to biomedicine and health Presents a one-stop resource for quick access to answers and an in-depth examination of topics in the spectroscopy and spectrometry arenas