Download or read book Measuring delta H Using DSC TGA and DTA written by Roland S. Hoffman and published by . This book was released on 1990 with total page 192 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Differential Scanning Calorimetry written by Günther Höhne and published by Springer Science & Business Media. This book was released on 2013-03-09 with total page 304 pages. Available in PDF, EPUB and Kindle. Book excerpt: In this fully updated and revised second edition the authors provide the newcomer and the experienced practitioner with a balanced and comprehensive insight into all important DSC methods, including a sound presentation of the theoretical basis of DSC and TMDSC measurements. Emphasis is layed on instrumentation, the underlying measurement principles, metrologically correct calibrations, factors influencing the measurement process, and on the exact interpretation of the results. The information given enables the research scientist, the analyst and experienced laboratory staff to apply DSC methods successfully and to measure respective properties correctly.
Download or read book Principles and Applications of Thermal Analysis written by Paul Gabbott and published by John Wiley & Sons. This book was released on 2008-04-30 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal Analysis techniques are used in a wide range of disciplines, from pharmacy and foods to polymer science, materials and glasses; in fact any field where changes in sample behaviour are observed under controlled heating or controlled cooling conditions. The wide range of measurements possible provide fundamental information on the material properties of the system under test, so thermal analysis has found increasing use both in basic characterisation of materials and in a wide range of applications in research, development and quality control in industry and academia. Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides the reader with sound practical instruction on how to use the techniques and gives an up to date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including the new approach of Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then developing the discussion to encompass industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues and relating the measurements to the physical behaviour of the materials under test, the book will also serve as an important reference for experienced analysts.
Download or read book Handbook of Thermal Analysis and Calorimetry written by and published by Elsevier. This book was released on 2018-03-12 with total page 862 pages. Available in PDF, EPUB and Kindle. Book excerpt: Handbook of Thermal Analysis and Calorimetry: Recent Advances, Techniques and Applications, Volume Six, Second Edition, presents the latest in a series that has been well received by the thermal analysis and calorimetry community. This volume covers recent advances in techniques and applications that complement the earlier volumes. There has been tremendous progress in the field in recent years, and this book puts together the most high-impact topics selected for their popularity by new editors Sergey Vyazovkin, Nobuyoshi Koga and Christoph Schick—all editors of Thermochimica Acta. Among the important new techniques covered are biomass conversion; sustainable polymers; polymer nanocompsoties; nonmetallic glasses; phase change materials; propellants and explosives; applications to pharmaceuticals; processes in ceramics, metals, and alloys; ionic liquids; fast-scanning calorimetry, and more. Features 19 all-new chapters to bring readers up to date on the current status of the field Provides a broad overview of recent progress in the most popular techniques and applications Includes chapters authored by a recognized leader in each field and compiled by a new team of editors, each with at least 20 years of experience in the field of thermal analysis and calorimetry Enables applications across a wide range of modern materials, including polymers, metals, alloys, ceramics, energetics and pharmaceutics Overviews the current status of the field and summarizes recent progress in the most popular techniques and applications
Download or read book Thermal Analysis of Pharmaceuticals written by Duncan Q.M. Craig and published by CRC Press. This book was released on 2006-12-21 with total page 416 pages. Available in PDF, EPUB and Kindle. Book excerpt: As a result of the Process Analytical Technologies (PAT) initiative launched by the U.S. Food and Drug Administration (FDA), analytical development is receiving more attention within the pharmaceutical industry. Illustrating the importance of analytical methodologies, Thermal Analysis of Pharmaceuticals presents reliable and versatile charac
Download or read book Solid State Properties of Pharmaceutical Materials written by Stephen R. Byrn and published by John Wiley & Sons. This book was released on 2017-07-12 with total page 432 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presents a detailed discussion of important solid-state properties, methods, and applications of solid-state analysis Illustrates the various phases or forms that solids can assume and discussesvarious issues related to the relative stability of solid forms and tendencies to undergo transformation Covers key methods of solid state analysis including X-ray powder diffraction, thermal analysis, microscopy, spectroscopy, and solid state NMR Reviews critical physical attributes of pharmaceutical materials, mainly related to drug substances, including particle size/surface area, hygroscopicity, mechanical properties, solubility, and physical and chemical stability Showcases the application of solid state material science in rational selection of drug solid forms, analysis of various solid forms within drug substance and the drug product, and pharmaceutical product development Introduces appropriate manufacturing and control procedures using Quality by Design, and other strategies that lead to safe and effective products with a minimum of resources and time
Download or read book Thermal Analysis in Practice written by Matthias Wagner and published by Carl Hanser Verlag GmbH Co KG. This book was released on 2017-12-11 with total page 353 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal analysis comprises a group of techniques used to determine the physical or chemical properties of a substance as it is heated, cooled, or held at constant temperature. It is particularly important for polymer characterization, but also has major application in analysis of pharmaceuticals and foodstuffs. This comprehensive handbook presents practical and theoretical aspects of the key techniques of DSC, TGA, TMA, DMA, and related methods. It also includes separate chapters on the glass transition, polymers, polymorphism, purity determination, and method development. The large number of practical examples included should inspire readers toward new ideas for applications in their own fields of work. The chapters are independent of one another and can be read individually in any desired order. Based on years of experience in thermal analysis of users, application specialists, consultants, and course instructors, this book provides practical help to newcomers, inexperienced users, and anyone else interested in the practical aspects of thermal analysis.
Download or read book Handbook of Differential Scanning Calorimetry written by Joseph D Menczel and published by Butterworth-Heinemann. This book was released on 2023-02-22 with total page 876 pages. Available in PDF, EPUB and Kindle. Book excerpt: Differential scanning calorimetry (DSC) is the most important thermal analysis technique used today and the most common thermal analysis instrument found in chemical characterization laboratories. DSC has become an everyday tool in characterization laboratories, but many researchers using this technique have a limited understanding of the true breadth of its capabilities. Up to now, there has been no book that would describe the application of DSC in all the various areas of materials chemistry. The Handbook of Differential Scanning Calorimetry has been written to fill that void. This book is designed to summarize the knowledge of differential scanning calorimetry so that materials researchers and application chemists are given both a better understanding of techniques , as well as a review of the full scope of its capabilities. It also discusses how to properly interpret the DSC thermograms data obtained. Included in this work is the most up-to-date information written by some of the leaders in the field. It is written not only to help users get the most out of their equipment, After reading this book, people in all chemical and biological areas will have a broad overview of this measuring technique, and will be able to utilize this analytical technique more efficiently. Provides a detail description of the theory behind differential scanning while simultaneously providing a wider breadth of understanding of the actual DSC technique Includes a review of the basics of heat flux and power compensation DSC’s, as well as separate chapters on inorganic and organic materials Reviews the most common commercial DSC instruments on the market and their uses, including TA Instruments, Perkin-Elmer, Hitachi, Mettler Toledo, Netzsch, and Setaram
Download or read book Glass Transition and Phase Transitions in Food and Biological Materials written by Jasim Ahmed and published by John Wiley & Sons. This book was released on 2017-02-03 with total page 494 pages. Available in PDF, EPUB and Kindle. Book excerpt: Glass and State Transitions in Food and Biological Materials describes how glass transition has been applied to food micro-structure, food processing, product development, storage studies, packaging development and other areas. This book has been structured so that readers can initially grasp the basic principles and instrumentation, before moving through the various applications. In summary, the book will provide the “missing link” between food science and material science/polymer engineering. This will allow food scientists to better understand the concept and applications of thermal properties.
Download or read book Protein Stability and Folding written by Wolfgang Pfeil and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 662 pages. Available in PDF, EPUB and Kindle. Book excerpt: Protein folding remains one of the most exclusive problems of modern biochemistry. Structure analysis has given access to the wealth of the molecular architecture of pro teins. As architecture needs static calculations, protein structure is always related to thermodynamic factors that govern folding and stability of a particular folded protein over the non-organized polypeptide chain. During the past decades a huge amount of thermodynamic data related to protein folding and stability has been accumulated. The data are certainly of importance in dechiffring the protein folding problem. At the same time, the data can guide the con struction of modified and newly synthesized proteins with properties optimized for particular application. The intention of this book is a generation of a data collection which makes the vast amount of present data accessible for multidisciplinary research where chemistry, phy sics, biology, and medicine are involved and also pharmaceutical and food research and technology. It took several years to compile all the data and the author wishes to thank everyone who provided data, ideas or even unpublished results. The author is, in particular, indebted to Prof. Wadso (Lund, Sweden) and IUPAC's Steering Committee on Bio physical Chemistry. Furthermore, support by the Deutsche Forschungsgemeinschafi (INK 16 AI-I) is acknowledged.
Download or read book Encyclopedia of Biophysics written by Gordon Roberts and published by Springer. This book was released on 2012-10-08 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: The Encyclopedia of Biophysics is envisioned both as an easily accessible source of information and as an introductory guide to the scientific literature. It includes entries describing both Techniques and Systems. In the Techniques entries, each of the wide range of methods which fall under the heading of Biophysics are explained in detail, together with the value and the limitations of the information each provides. Techniques covered range from diffraction (X-ray, electron and neutron) through a wide range of spectroscopic methods (X-ray, optical, EPR, NMR) to imaging (from electron microscopy to live cell imaging and MRI), as well as computational and simulation approaches. In the Systems entries, biophysical approaches to specific biological systems or problems – from protein and nucleic acid structure to membranes, ion channels and receptors – are described. These sections, which place emphasis on the integration of the different techniques, therefore provide an inroad into Biophysics from a biological more than from a technique-oriented physical/chemical perspective. Thus the Encyclopedia is intended to provide a resource both for biophysicists interested in methods beyond those used in their immediate sub-discipline and for those readers who are approaching biophysics from either a physical or biological background.
Download or read book Encyclopedia of Geochemistry written by C.P. Marshall and published by Springer Science & Business Media. This book was released on 1999-07-31 with total page 677 pages. Available in PDF, EPUB and Kindle. Book excerpt: This is a complete and authoritative reference text on an evolving field. Over 200 international scientists have written over 340 separate topics on different aspects of geochemistry including organics, trace elements, isotopes, high and low temperature geochemistry, and ore deposits, to name just a few.
Download or read book Principles of Thermal Analysis and Calorimetry written by Simon Gaisford and published by Royal Society of Chemistry. This book was released on 2019-03-15 with total page 280 pages. Available in PDF, EPUB and Kindle. Book excerpt: The use of thermal and calorimetric methods has shown rapid growth over the past few decades, in an increasingly wide range of applications. The original text was published in 2001; since then there have been significant advances in various analytical techniques and their applications. This second edition supplies an up to date, concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis. Written by experts in their field, brief accounts of the basic theory are reinforced with detailed technical advances and contemporary developments. Where appropriate, applications are used to highlight particular operating principles or methods of interpretation. As an important source of information for many levels of readership in a variety of areas, this book will be an aid for students and lecturers through to industrial and laboratory staff and consultants.
Download or read book Thermal Safety of Chemical Processes written by Francis Stoessel and published by John Wiley & Sons. This book was released on 2021-05-24 with total page 581 pages. Available in PDF, EPUB and Kindle. Book excerpt: Vollständig überarbeitete,aktualisierte 2. Auflage mit fünf neuen Kapiteln und den aktuellen IUPAC-Normen. Beschäftigt sich mit thermischen Risiken in der chemischen Prozessindustrie. Jedes Kapitel beginnt mit einer Fallstudie und den aus Zwischenfällen gewonnen Erkenntnissen.
Download or read book Introduction to Thermal Analysis written by M.E. Brown and published by Springer Science & Business Media. This book was released on 2006-01-10 with total page 268 pages. Available in PDF, EPUB and Kindle. Book excerpt: to Thermal Analysis Techniques and Applications Edited by Michael E. Brown Chemistry Department, Rhodes University, Grahamstown, South Africa KLUWER ACADEMIC PUBLISHERS NEW YORK, BOSTON, DORDRECHT, LONDON, MOSCOW eBook ISBN: 0-306-48404-8 Print ISBN: 1-4020-0472-9 ©2004 Kluwer Academic Publishers New York, Boston, Dordrecht, London, Moscow Print ©2001 Kluwer Academic Publishers Dordrecht All rights reserved No part of this eBook may be reproduced or transmitted in any form or by any means, electronic, mechanical, recording, or otherwise, without written consent from the Publisher Created in the United States of America Visit Kluwer Online at: http://kluweronline. com and Kluwer's eBookstore at: http://ebooks. kluweronline. com CONTENTS Preface to the First Edition, Chapman & Hall, London, 1988 ix About the First Edition of this Book x Preface to the Second Edition xi 1. INTRODUCTION 1. 1 Definition and History 1 1. 2 Thermal Analysis Instruments 4 References 11 2. THERMAL EVENTS 2. 1 Introduction 13 2. 2 The Solid State 13 2. 3 Reactions of Solids 14 2. 4 Decomposition of Solids 15 2. 5 Reaction with the Surrounding Atmosphere 16 2. 6 Solid-Solid Interactions 16 References 17 3. THERMOGRAVIMETRY (TG) Introduction 3. 1 19 3. 2 The Balance 19 3. 3 Heating the Sample 21 3. 4 The Atmosphere 24 3. 5 The Sample 26 3. 6 Temperature Measurement 26 3. 7 Temperature Control 28 Sample Controlled Thermal Analysis (SCTA) 29 3. 8 3. 9 Calibration 36 3. 10 Presentation of TG Data 37 3.
Download or read book Thermal Analysis and Calorimetry written by Aline Auroux and published by Walter de Gruyter GmbH & Co KG. This book was released on 2023-07-04 with total page 521 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book summarizes the application of thermal analysis tools in different research areas. Areas covered include characterization of catalytic materials, plastics and polymers, analysis of salts, minerals and oxides. The reader is provided with an overview of experimental strategy, methodology, usage of complementary thermoanalytical methods and the type of information which could be drawn depending on the research field.
Download or read book Kinetics of Phase Transitions written by Sanjay Puri and published by CRC Press. This book was released on 2009-03-24 with total page 356 pages. Available in PDF, EPUB and Kindle. Book excerpt: Providing a comprehensive introduction with the necessary background material to make it accessible for a wide scientific audience, Kinetics of Phase Transitions discusses developments in domain-growth kinetics. This book combines pedagogical chapters from leading experts in this area and focuses on incorporating various experimentally releva
