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Book Practical High Performance Liquid Chromatography

Download or read book Practical High Performance Liquid Chromatography written by Veronika R. Meyer and published by John Wiley & Sons. This book was released on 2013-03-25 with total page 342 pages. Available in PDF, EPUB and Kindle. Book excerpt: Jump into the HPLC adventure! Three decades on from publication of the 1st German edition of Veronika Meyer's book on HPLC, this classic text remains one of the few titles available on general HPLC aimed at practitioners. New sections on the following topics have been included in this fifth edition: Comparison of HPLC with capillary electrophoresis How to obtain peak capacity van Deemter curves and other coherences Hydrophilic interaction chromatography Method transfer Comprehensive two-dimensional HPLC Fast separations at 1000 bar HPLC with superheated water In addition, two chapters on the instrument test and troubleshooting in the appendix have been updated and expanded by Bruno E. Lendi, and many details have been improved and numerous references added. A completely new chapter is presented on quality assurance covering: Is it worth the effort? Verification with a second method Method validation Standard operating procedures Measurement uncertainty Qualifications, instrument test, and system suitability test The quest for quality Reviews of earlier editions "That this text is written by an expert in both the practice and teaching of HPLC is evident from the first paragraph....not only an enjoyable, fascinating and easy read, but a truly excellent text that has and will serve many teachers, students and practitioners very well." —The Analyst “...provides essential information on HPLC for LC practitioners in academia, industry, government, and research laboratories...a valuable introduction." - American Journal of Therapeutics

Book High Performance Liquid Chromatography

Download or read book High Performance Liquid Chromatography written by Omar Al Sayed Omar and published by Walter de Gruyter GmbH & Co KG. This book was released on 2022-02-21 with total page 322 pages. Available in PDF, EPUB and Kindle. Book excerpt: The book provides an indispensable guide on how to use HPLC in pharmaceutical analysis and drug control. Following a hands-on approach, the authors give practical advices how to prepare stationary and mobile phases, choose a suitable detector and set up an HPLC analysis. The publication gives insight into the key pharmaceutical applications of HPLC and the latest requirements of the major regulatory agencies.

Book A Practical Guide to HPLC Detection

Download or read book A Practical Guide to HPLC Detection written by Donald Parriott and published by Academic Press. This book was released on 2012-12-02 with total page 304 pages. Available in PDF, EPUB and Kindle. Book excerpt: This guide for the practicing chromatographer who wants a ready source of information on HPLC detection explores and compares existing detection systems and detectors, outlines the common problems associated with a given detector, and offers proven approaches to avoiding such problems. - Addresses the practical aspects of HPLC detection, including: basic theory, when a particular type of detector can be used, how detectors from various manufacturers differ, common problems of detectors and ways to avoid them - Presents an overview of today's most common techniques - Discusses the advantages and disadvantages of HPLC, dispelling common misconceptions

Book Selective Sample Handling and Detection in High Performance Liquid Chromatography

Download or read book Selective Sample Handling and Detection in High Performance Liquid Chromatography written by K. Zech and published by Elsevier. This book was released on 1989-10-30 with total page 407 pages. Available in PDF, EPUB and Kindle. Book excerpt: This is the second of a two-volume project which treats the handling, separation and detection of complex samples as an integrated, interconnected process. On the basis of this philosophy the editors have selected those contributions which demonstrate that optimal sample preparation leads to a simplification of detection or reduced demands on the separation process. Throughout the book emphasis is on chemical principles with minimum discussion of the equipment required - an approach which reflects the editors' view that the limiting factor in the analysis of complex samples is an incomplete knowledge of the underlying chemistry rather than the hardware available. This lack of knowledge becomes more evident as the demands for lower detection limits grow, as solving complex matrix problems requires a greater understanding of the chemical interaction between the substance to be analysed and the stationary phase. Thus, apart from one chapter dealing with chemically modified silicas, the main theme of the book is developed in three chapters on sample preparation and three on detection.The opening chapter outlines concentration and chromatography on chemically modified silicas with complexing properties, and gives examples of the use of these phases with organic and inorganic compounds. Chapter II, the first of the three contributions dealing with sample preparation, addresses such questions as whether the prepared sample is representative of the material to be analysed; how to avoid contamination; which separation procedure should be used to avoid tedious sample preparation. Chapter III describes the processing of whole blood for drug analysis. The determination of cyclosporine and its metabolites (an especially difficult case) demonstrates how comprehensive the optimisation of sample preparation must be to successfully perform the analysis. Several other examples are also given. Chapter IV deals with radio-column liquid chromatography and introduces the other theme of the book, i.e. selective detection methods. The widespread use of radioisotopes requires a high degree of purification during the manufacture of the compounds, as well as highly accurate detection methods in biological and biochemical studies.Chapter V continues the theme of selective detection with an overview of post-column reaction detection. The use of immobilised enzymes in post-column reactors or `pumpless' reactor systems for on-line reagent generation after the chromatographic separation step is discussed in detail. Various examples of the separation of biological compounds show how the production of electrochemical reagents and photochemical reaction detection have increased the selectivity of the detection, leading to more economical analytical systems. Selective detection employing luminescence detection techniques is outlined in Chapter VI. The use of immobilised fluorophores or the coupling to photochemical reactions leads to highly selective detection systems which can greatly simplify the sample handling. The final chapter reviews the use of continuous separation techniques in flow injection analysis thus revealing the need for a strong interdisciplinary dependence between sample handling and separation in this area.Written by experienced practitioners, this book will be extremely useful to investigators in many areas of application. Each chapter includes sufficient references to the literature to serve as a valuable starting point for more detailed investigation. The strong emphasis on sample handling makes the book unique in many ways and it will be welcomed by environmental scientists as well as those active in the clinical, pharmaceutical and bioanalytical fields.

Book High Performance Liquid Chromatography in Phytochemical Analysis

Download or read book High Performance Liquid Chromatography in Phytochemical Analysis written by Monika Waksmundzka-Hajnos and published by CRC Press. This book was released on 2010-11-08 with total page 998 pages. Available in PDF, EPUB and Kindle. Book excerpt: The powerful, efficient technique of high performance liquid chromatography (HPLC) is essential to the standardization of plant-based drugs, identification of plant material, and creation of new herbal medicines. Filling the void in this critical area, High Performance Liquid Chromatography in Phytochemical Analysis is the first book to give a comp

Book High Performance Liquid Chromatography

Download or read book High Performance Liquid Chromatography written by Win Fung Ho and published by Royal Society of Chemistry. This book was released on 2003 with total page 52 pages. Available in PDF, EPUB and Kindle. Book excerpt: "This book covers the basic practical aspects of high performance liquid chromatography (HPLC) and is aimed at the inexperienced analyst who may have no or very little knowledge of this technique. It includes basic tips, identifies key skills, arouses awareness and gives guidance on good practice of the basic aspects of HPLC." - page 1.

Book Applications of High Performance Liquid Chromatography

Download or read book Applications of High Performance Liquid Chromatography written by S. Pryde and published by Springer Science & Business Media. This book was released on 1979-01-31 with total page 288 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book High Performance Liquid Chromatography

Download or read book High Performance Liquid Chromatography written by Heinz Engelhardt and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 263 pages. Available in PDF, EPUB and Kindle. Book excerpt: Modern liquid column chromatography (LC) has developed rapidly since 1969 to become a standard method of separation. If the statisticians are to be believed, the recent growth of LC has been the most specta cular development in analytical chemistry and has not yet abated be cause its vast potential for application remains to be fully exploit ed. Significant factors contributing to this continued rise are the simplicity and low cost of the required basic equipment and the rela tive ease of acquiring and interpreting the data. Unfortunately, in LC, as so often in the field of analytical chemistry, the available commercial instruments are frequently far more complicated - and consequently far more expensive - than is nec essary for routine application. Therein also lies the risk of propa gating a "black box" philosophy that would be particularly detrimen tal to chromatography. Moreover, it appears to have been forgotten, as was done previously with gas chromatography, that inadequate sep aration by a column can be remedied only with great difficulty, if at all, by electronic means. Also, whether the capillary columns recent ly advocated with great enthusiasm for LC will fulfill the expecta tions of their proponents is highly questionable unless someone comes up with some new and revolutionary ideas.

Book Sample Introduction in Atomic Spectroscopy

Download or read book Sample Introduction in Atomic Spectroscopy written by J. Sneddon and published by Elsevier. This book was released on 2012-12-02 with total page 396 pages. Available in PDF, EPUB and Kindle. Book excerpt: A comprehensive and detailed description of the most widely used sample introduction techniques in atomic spectroscopy is presented in this volume. Comprising twelve separate chapters, the book describes the theory in detail, and gives an account of techniques and selected applications of sample introduction systems. The first chapter is a general overview on sample introduction. The remaining eleven chapters are each devoted to a specific sample introduction and deal with the basic principles, describe the system, advantages, disadvantages and selected applications. Systems described are: pneumatic nebulization, electrothermal vaporization, laser ablation, impaction/electrostatic precipitation, slurry atomization, ultrasonic and thermospray nebulization, hydride generation, chromatographic, spark and arc, low-pressure discharges, flow injection analysis and direct solid introduction. Each chapter is suitable for a separate discussion. Being a unique textbook in this field, Sample Introduction in Atomic Spectroscopy should prove invaluable for courses at graduate level.

Book Publications of the National Institute of Standards and Technology     Catalog

Download or read book Publications of the National Institute of Standards and Technology Catalog written by National Institute of Standards and Technology (U.S.) and published by . This book was released on 1980 with total page 648 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book HPLC

    Book Details:
  • Author : Toshihiko T Hanai
  • Publisher : Royal Society of Chemistry
  • Release : 2007-10-31
  • ISBN : 1847551076
  • Pages : 146 pages

Download or read book HPLC written by Toshihiko T Hanai and published by Royal Society of Chemistry. This book was released on 2007-10-31 with total page 146 pages. Available in PDF, EPUB and Kindle. Book excerpt: How can these compounds be separated? Why was that method used? These are the two basic questions often asked by students of chromatography. HPLC: A Practical Guide provides the answers, enabling the reader to grasp the concepts of the technique using simple, representative chromatograms. Divided into six chapters, this practical guide covers basic concepts of HPLC; instrumentation; stationary phase materials; eluents; column efficiency; and the influence of physical chemistry on separations. Focusing on the basic considerations such as selection of stationary phase and eluent, rather than specific applications, sections on troubleshooting are also included. Uniquely, the descriptions of chromatographic separations are based on solubility using molecular properties, and solubility parameters are used to analyse the selections of chromatographic mode and column. Presenting the chemistry of liquid chromatography for undergraduate students, this valuable practical guide will also be useful for laboratory staff in industry and academia.

Book NBS Special Publication

Download or read book NBS Special Publication written by and published by . This book was released on 1968 with total page 668 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Practical Aspects of Modern High Performance Liquid Chromatography

Download or read book Practical Aspects of Modern High Performance Liquid Chromatography written by Imre Molnar and published by Walter de Gruyter. This book was released on 2011-06-01 with total page 465 pages. Available in PDF, EPUB and Kindle. Book excerpt: Cover title: Practical aspects of modern HPLC.

Book Trace Element Speciation Analytical Methods and Problems

Download or read book Trace Element Speciation Analytical Methods and Problems written by Graeme E. Batley and published by CRC Press. This book was released on 1989-06-30 with total page 392 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book discusses in detail the application of physical separation procedures together with modern instrumental analysis techniques such as HPLC, gas chromatography, and anodic strip-ping voltammetry. Particular emphasis is given to environmental samples where the greatest concern for the effects of speciation on trace element transport, toxicity, and bioavailability have been ex-pressed. Special chapters are also devoted to methods of sam-pling and storage, and to the mathematical modeling of chemical speciation. Although designed for the practical analytical chemist, this publication is essential reading for researchers in or entering the field of chemical speciation.

Book Analytical Separation Science  5 Volume Set

Download or read book Analytical Separation Science 5 Volume Set written by Jared Anderson and published by John Wiley & Sons. This book was released on 2016-02-29 with total page 2148 pages. Available in PDF, EPUB and Kindle. Book excerpt: Endlich ein Forschungsleitfaden für Wissenschaftler des Fachgebiets, die neue Methoden entwickeln oder einsetzen. Dieses Handbuch umfasst fünf thematische Bände und bietet damit einen umfassenden Überblick über das Fachgebiet. Erläutert werden Grundlagen, die Methodenentwicklung und hochkarätige Anwendungen für alle wichtigen Analyseverfahren, darunter chromatische Verfahren, Techniken in den Bereichen Elektromigration und Membranen. Dieses Referenzwerk umfasst ein breites Spektrum und legt den Schwerpunkt auf Entwicklungen für die Zukunft. Damit ist es ein Muss für Forscher und eine wertvolle Wissensquelle für Studenten im Hauptstudium und Studienabsolventen.

Book Publications

Download or read book Publications written by United States. National Bureau of Standards and published by . This book was released on 1980 with total page 668 pages. Available in PDF, EPUB and Kindle. Book excerpt: