Download or read book X ray Photoemission Electron Microscopy a Tool for the Investigation of Complex Magnetic Structures written by and published by . This book was released on 2001 with total page 5 pages. Available in PDF, EPUB and Kindle. Book excerpt: X-ray Photoemission Electron Microscopy unites the chemical specificity and magnetic sensitivity of soft x-ray absorption techniques with the high spatial resolution of electron microscopy. The discussed instrument possesses a spatial resolution of better than 50 nm and is located at a bending magnet beamline at the Advanced Light Source, providing linearly and circularly polarized radiation between 250 and 1300 eV. We will present examples which demonstrate the power of this technique applied to problems in the field of thin film magnetism. The chemical and elemental specificity is of particular importance for the study of magnetic exchange coupling because it allows separating the signal of the different layers and interfaces in complex multi-layered structures.

Download or read book Topology in Magnetism written by Jiadong Zang and published by Springer. This book was released on 2018-09-24 with total page 426 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents both experimental and theoretical aspects of topology in magnetism. It first discusses how the topology in real space is relevant for a variety of magnetic spin structures, including domain walls, vortices, skyrmions, and dynamic excitations, and then focuses on the phenomena that are driven by distinct topology in reciprocal momentum space, such as anomalous and spin Hall effects, topological insulators, and Weyl semimetals. Lastly, it examines how topology influences dynamic phenomena and excitations (such as spin waves, magnons, localized dynamic solitons, and Majorana fermions). The book also shows how these developments promise to lead the transformative revolution of information technology.

Download or read book Nanomagnetism written by and published by Elsevier. This book was released on 2006-03-27 with total page 349 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nanoscience is of central importance in the physical and biological sciences and is now pervasive in technology. However nanomagnetism has a special role to play as magnetic properties depend uniquely on both dimensionality and lengthscales. Nanomagnetism is already central to data storage, sensor and device technologies but is increasingly being used in the life sciences and medicine. This volume aims to introduce scientists, computer scientists, engineers and technologists from diverse fields to this fascinating and technologically important new branch of nanoscience. The volume should appeal to both the interested general reader but also to the researcher wishing to obtain an overview of this fast moving field. The contributions come from acknowledged leaders in the field who each give authoritative accounts of key fundamental aspects of nanomagnetism to which they have themselves made a major contribution. After a brief introduction by the editors, Wu first surveys the fundamental properties of magnetic nanostructures. The interlayer exchange interactions within magnetic multilayer structures is next discussed by Stiles. Camley then discusses the static, dynamic and thermal properties of magnetic multilayers and nanostructures, followed by an account of the phenomenon of exchange anisotropy by Berkowitz and Kodama. This latter phenomenon is widely in current read head devices for example. The transport properties of nanostructures also are spectacular, and again underpin computer technology, as we see from the discussion of giant magnetoresistance (GMR) and tunnelling magnetoresistance (TMR) presented by Fert and his colleagues. Beyond GMR and TMR we look to the field of spintronics where new electronic devices are envisioned and for which quantumcomputing may depend as discussed in the chapter by Flatte and Jonker.The volume concludes with discussion of the recently discovered phenomenon of current induced switching of magnetization by Edwards and Mathon.* Subject is in the forefront of nanoscience* All Section authors are leading figures in this key field* Presentations are accessible to non specialists, with focus on underlying fundamentals

Download or read book Advanced Analytical Methods in Tribology written by Martin Dienwiebel and published by Springer. This book was released on 2018-10-04 with total page 332 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book presents the basics and methods of nanoscale analytical techniques for tribology field. It gives guidance to the application of mechanical, microstructural, chemical characterization methods and topography analysis of materials. It provides an overview of the of state-of-the-art for researchers and practitioners in the field of tribology. It shows different examples to the application of mechanical, microstructural, chemical characterization methods and topography analysis of materials. Friction and Wear phenomena are governed by complexe processes at the interface of sliding surfaces. For a detailed understanding of these phenomena many surface sensitive techniques have become available in recent years. The applied methods are atom probe tomography, in situ TEM, SERS, NEXAFS, in situ XPS, nanoindentation and in situ Raman spectroscopy. A survey of new related numerical calculations completes this book. This concerns ab-initio coupling, numerical calculations for mechanical aspects and density functional theory (DFT) to study chemical reactivity.

Download or read book Environmental Mineralogy II written by D.J. Vaughan and published by The Mineralogical Society of Great Britain and Ireland. This book was released on 2013-02-06 with total page 507 pages. Available in PDF, EPUB and Kindle. Book excerpt: In a sense, all mineralogy is environmental mineralogy. However, the term environmental has come to be employed (particularly in combination with terms such as science, issue or problem) to refer to those systems at or near the surface of the Earth where the geosphere comes into contact with the hydrosphere, atmosphere and biosphere. This is, of course, the environment upon which the human race depends for survival and, hence, is now sometimes referred to as the critical zone. Those systems containing minerals that constitute the most important or key environments are considered here: soils, modern sediments, atmospheric aerosols, and the interior or exterior parts of certain micro- and macro-organisms. Particularly important are the roles that minerals play in processes that act over time to control or influence the environment at various scales of observation. Both pure systems and those contaminated as a result of human activity are considered. The objectives for this volume are to help to define the subject of environmental mineralogy, and to provide an initial source of information both for mineralogists and other scientists who wish to understand or work in this field. It was hoped that it might also provide a text for use by those teaching courses in the subject at advanced undergraduate or graduate student level.

Download or read book Applications of Synchrotron Radiation in Low Temperature Geochemistry and Environmental Science written by Paul A. Fenter and published by Walter de Gruyter GmbH & Co KG. This book was released on 2018-12-17 with total page 604 pages. Available in PDF, EPUB and Kindle. Book excerpt: Volume 49 of Reviews in Mineralogy and Geochemistry reviews the state of the art of synchrotron radiation applications in low temperature geochemistry and environmental science, and offer speculations on future developments. The reader of this volume will acquire an appreciation of the theory and applications of synchrotron radiation in low temperature geochemistry and environmental science, as well as the significant advances that have been made in this area in the past two decades. It gives a fairly comprehensive overview of synchrotron radiation applications in low temperature geochemistry and environmental science, describes the ways that synchrotron radiation is generated, including a history of synchrotrons and a discussion of aspects of synchrotron radiation that are important to the experimentalist, describes specific synchrotron methods that are most useful for single-crystal surface and mineral-fluid interface studies as well as methods that can be used more generally for investigating complex polyphase fine-grained or amorphous materials, including soils, rocks, and organic matter.

Download or read book Concise Encyclopedia of Magnetic and Superconducting Materials written by K.H.J. Buschow and published by Elsevier. This book was released on 2005-12-28 with total page 1361 pages. Available in PDF, EPUB and Kindle. Book excerpt: Magnetic and superconducting materials pervade every avenue of the technological world – from microelectronics and mass-data storage to medicine and heavy engineering. Both areas have experienced a recent revitalisation of interest due to the discovery of new materials, and the re-evaluation of a wide range of basic mechanisms and phenomena.This Concise Encyclopedia draws its material from the award-winning Encyclopedia of Materials and Engineering, and includes updates and revisions not available in the original set -- making it the ideal reference companion for materials scientists and engineers with an interest in magnetic and superconducting materials. - Contains in excess of 130 articles, taken from the award-winning Encyclopedia of Materials: Science and Technology, including ScienceDirect updates not available in the original set - Each article discusses one aspect of magnetic and superconducting materials and includes photographs, line drawings and tables to aid the understanding of the topic at hand - Cross-referencing guides readers to articles covering subjects of related interest

Download or read book Scanning Electron Microscopy X Ray Microanalysis and Analytical Electron Microscopy written by Charles E. Lyman and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 415 pages. Available in PDF, EPUB and Kindle. Book excerpt: During the last four decades remarkable developments have taken place in instrumentation and techniques for characterizing the microstructure and microcomposition of materials. Some of the most important of these instruments involve the use of electron beams because of the wealth of information that can be obtained from the interaction of electron beams with matter. The principal instruments include the scanning electron microscope, electron probe x-ray microanalyzer, and the analytical transmission electron microscope. The training of students to use these instruments and to apply the new techniques that are possible with them is an important function, which. has been carried out by formal classes in universities and colleges and by special summer courses such as the ones offered for the past 19 years at Lehigh University. Laboratory work, which should be an integral part of such courses, is often hindered by the lack of a suitable laboratory workbook. While laboratory workbooks for transmission electron microscopy have-been in existence for many years, the broad range of topics that must be dealt with in scanning electron microscopy and microanalysis has made it difficult for instructors to devise meaningful experiments. The present workbook provides a series of fundamental experiments to aid in "hands-on" learning of the use of the instrumentation and the techniques. It is written by a group of eminently qualified scientists and educators. The importance of hands-on learning cannot be overemphasized.

Download or read book Realization of a new Magnetic Scanning X ray Microscope and Investigation of Landau Structures under Pulsed Field Excitation written by Markus Weigand and published by Cuvillier Verlag. This book was released on 2015-05-05 with total page 320 pages. Available in PDF, EPUB and Kindle. Book excerpt: Magnetic nanostructures in thin films and their behavior have seen a drastic increase in scientific interest in the last decades. Similarly, X-ray microscopy has moved into the spotlight since the turn of the century. This thesis combines both topics with the investigation of magnetic vortex structures under pulsed field excitation using both micromagnetic simulations and time resolved magnetic X-ray microscopy. This allowed the observation of vortex core polarization switches with

Download or read book Advanced Scanning Electron Microscopy and X Ray Microanalysis written by Patrick Echlin and published by Springer Science & Business Media. This book was released on 2013-06-29 with total page 463 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book has its origins in the intensive short courses on scanning elec tron microscopy and x-ray microanalysis which have been taught annually at Lehigh University since 1972. In order to provide a textbook containing the materials presented in the original course, the lecturers collaborated to write the book Practical Scanning Electron Microscopy (PSEM), which was published by Plenum Press in 1975. The course con tinued to evolve and expand in the ensuing years, until the volume of material to be covered necessitated the development of separate intro ductory and advanced courses. In 1981 the lecturers undertook the project of rewriting the original textbook, producing the volume Scan ning Electron Microscopy and X-Ray Microanalysis (SEMXM). This vol ume contained substantial expansions of the treatment of such basic material as electron optics, image formation, energy-dispersive x-ray spectrometry, and qualitative and quantitative analysis. At the same time, a number of chapters, which had been included in the PSEM vol ume, including those on magnetic contrast and electron channeling con trast, had to be dropped for reasons of space. Moreover, these topics had naturally evolved into the basis of the advanced course. In addition, the evolution of the SEM and microanalysis fields had resulted in the devel opment of new topics, such as digital image processing, which by their nature became topics in the advanced course.

Download or read book Hard X Ray Photoelectron Spectroscopy of Deeply Buried Magnetic Layers written by Xeniya Kozina and published by LAP Lambert Academic Publishing. This book was released on 2013-01 with total page 148 pages. Available in PDF, EPUB and Kindle. Book excerpt: This work focuses on the investigation of multilayer structures, employed in spintronics devices, by a number of techniques based on hard x-ray photoelectron spectroscopy (HAXPES). The application of hard x-rays increases the inelastic mean free path of the emitted electrons what makes HAXPES a non-destructive bulk sensitive probe for solid state research, especially studies of buried layers. Magnetoelectronic properties such as exchange splitting in ferromagnetic materials as well as the macroscopic magnetic ordering can be studied by magnetic circular dichroism in photoemission (MCDAD). In the present work MCDAD was integrated into HAXPES to explore the magnetic phenomena in deeply buried layers of the complex multilayer structures. In turn, direct measurements of electron spins of ferromagnets always attracted much attention but up to date have been limited by the surface sensitivity of the developed techniques. The last part of the work presents the results of the successfully performed spin-resolved HAXPES experiment using a spin polarimeter of the SPLEED-type on a buried magnetic layer.

Download or read book Depth resolved Electronic Structure of Spintronic Nanostructures and Complex Materials with Soft and Hard X ray Photoemission written by Alexander Gray and published by . This book was released on 2011 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: In this dissertation we describe several new directions in the field of x-ray photoelectron spectroscopy, with a particular focus on the enhancement and control of the depth sensitivity and selectivity of the measurement. Enhancement of the depth sensitivity is achieved by going to higher photon energies with hard x-ray excitation and taking advantage of the resulting larger electron inelastic mean-free paths. This novel approach provides a more accurate picture of bulk electronic structure, when compared to the traditional soft x-ray photoelectron spectroscopy (XPS) which, for some systems, may be too strongly influenced by surface effects. We present three case-studies wherein such hard x-ray photoelectron spectroscopy (HAXPES) in the multi-keV regime is used to probe the bulk properties of complex thin-film materials, which would be otherwise impossible to investigate using conventional soft x-ray XPS. Namely, (1) we directly observe the opening of a semiconducting gap in epitaxial Cr[subscript 0.08]Al[subscript 0.20] alloy thin films and confirm this with theory, (2) we study the electronic and structural properties of near-Heusler Fe[subscript x]Si[subscript 1-x] alloy thin films of various composition and degrees of crystallinity, and (3) we observe the Mott metal-to-insulator transition in the ultra-thin epitaxial LaNiO3 films via core-level and valence-band spectroscopies. By performing the experiments at the photon energy of 5.95 keV, the bulk-sensitivity of the measurements, characterized by the inelastic mean-free path of the photoemitted electrons, is enhanced by a factor of 4-7 compared to the conventional soft x-ray photoelectron spectroscopy. The experimental results are compared to calculations performed using various first-principle theoretical approaches, such as the density-functional theory and the one-step theory of photoemission. Furthermore, we present the first results of hard x-ray angle-resolved photoemission measurements (HARPES), at excitation energies of 3.24 and 5.95 keV. Compared to traditional ARPES, carried out in the UPS regime (20-100 eV), our technique enables us to probe on average 10-40 times deeper into the bulk. Single-crystal W(110) is used to demonstrate viability of the technique, with clear dispersive bands seen at 5.95 keV. As a second proof of principle for HARPES, the technologically-relevant material GaAs(001) is used to illustrate the broad applicability of the technique. In order to demonstrate the compositional sensitivity of the new method, we also compare the measurements of pure GaAs to the measurements of the ferromagnetic semiconductor Ga[subscript 0.97]Mn[0.03]As. Clear differences due to Mn-derived states are observed in the bulk band structure measured with the excitation energy of 3.24 keV. All of these experimental HARPES results are compared to free-electron final-state model calculations and more precise fully-relativistic one-step photoemission theory including matrix element effects. As noted, increasing the inelastic mean-free path, or more properly the effective attenuation length [Lambda subscript EAL] of the photoemitted electrons by going to higher photon energies increases the bulk sensitivity of the measurement, and facilitates a wider range of probing depths which can be accessed via variable take-off angle (theta subscript TOA) experiments. However, this approach does not circumvent the fact that no matter how long the photoelectron escape depth is, the photoemission signal originating closer to the surface will prevail over the signal originating from below according to I(z)=I0exp[-z /[Lambda subscript EAL]sin[theta subscript TOA]]. This constraint can be modulated in a useful way, if one were allowed to tailor the intensity profile of the electromagnetic field of the incident x-ray radiation inside the sample. In a second aspect of this dissertation, this type of depth selectivity is achieved by setting-up an x-ray standing wave field in the sample by growing it on a synthetic periodic multilayer mirror substrate, which in first-order Bragg reflection acts as the standing-wave generator. The antinodes of the standing wave function as "epicenters" for photoemission, and can be moved in the direction perpendicular to the sample surface by either scanning the incidence angle [theta subscript inc], or the photon energy through the Bragg condition. Alternatively, provided that one of the underlying layers in the structure is grown in a shape of a wedge with varying thickness, the standing wave can be scanned vertically though the sample simply by moving the sample laterally under the x-ray measurement spot. We present the first study in which the chemical and electronic-structure profiles of a magnetic tunnel junction La[subscript 0.7]Sr[subscript 0.3]MnO3/SrTiO3 (LSMO/STO) have been quantitatively determined by a combination of soft and hard x-ray standing-wave excited photoemission. By comparing experiment to x-ray optical calculations, the detailed chemical profile of the constituent layers and their interfaces is quantitatively derived with Ångstrom precision. Combined with core-hole multiplet theory incorporating Jahn-Teller distortion, these results indicate a change in the Mn bonding state near the LSMO/STO interface. Our results thus further clarify the reduced performance of LSMO/STO magnetic tunnel junction compared to ideal theoretical expectations. Finally, we demonstrate the addition of depth resolution to the usual two-dimensional images in photoelectron emission microscopy (PEEM) as a further aspect of standing-wave photoemission. We show that standing-wave excited photoelectron microscopy can be used to produce element-specific and depth-selective images of patterned samples. In conjunction with x-ray optical theoretical modeling, quantitative information about the depth-dependent chemical composition of the sample can be extracted from the photoemission data. The good agreement between our experimental results and model calculations suggests that future studies with better spatial and spectral resolution will also yield more detailed information about the interfacial regions. This addition of quantitative depth selectivity to the conventional laterally-resolved soft x-ray photoelectron emission microscopy thus should considerably enhance the capabilities of the PEEM as a research, development and metrology tool for science and industry.

Download or read book Handbook of Magnetism and Advanced Magnetic Materials 5 Volume Set written by Helmut Kronmüller and published by Wiley-Interscience. This book was released on 2007-09-11 with total page 534 pages. Available in PDF, EPUB and Kindle. Book excerpt: From the first application of the oxide magnetite as a compass in China in ancient times, and from the early middle ages in Europe, magnetic materials have become an indispensable part of our daily life. Magnetic materials are used ubiquitously in the modern world, in fields as diverse as, for example, electrical energy transport, high-power electro-motors and generators, telecommunication systems, navigation equipment, aviation and space operations, micromechanical automation, medicine, magnetocaloric refrigeration, computer science, high density recording, non-destructive testing of materials, and in many household applications. Research in many of these areas continues apace. The progress made in recent years in computational sciences and advanced material preparation techniques has dramatically improved our knowledge of fundamental properties and increased our ability to produce materials with highly-tailored magnetic properties, even down to the nanoscale dimension. Containing approximately 120 chapters written and edited by acknowledged world leaders in the field, The Handbook of Magnetism and Advanced Magnetic Materials provides a state-of-the-art, comprehensive overview of our current understanding of the fundamental properties of magnetically ordered materials, and their use in a wide range of sophisticated applications. The Handbook is published in five themed volumes, as follows: Volume 1- Fundamentals and Theory Volume 2- Micromagnetism Volume 3- Novel Techniques for Characterizing and Preparing Samples Volume 4- Novel Materials Volume 5- Spintronics and Magnetoelectronics

Download or read book Scanning Electron Microscopy and X Ray Microanalysis written by Joseph I. Goldstein and published by Springer. This book was released on 2017-11-17 with total page 554 pages. Available in PDF, EPUB and Kindle. Book excerpt: This thoroughly revised and updated Fourth Edition of a time-honored text provides the reader with a comprehensive introduction to the field of scanning electron microscopy (SEM), energy dispersive X-ray spectrometry (EDS) for elemental microanalysis, electron backscatter diffraction analysis (EBSD) for micro-crystallography, and focused ion beams. Students and academic researchers will find the text to be an authoritative and scholarly resource, while SEM operators and a diversity of practitioners — engineers, technicians, physical and biological scientists, clinicians, and technical managers — will find that every chapter has been overhauled to meet the more practical needs of the technologist and working professional. In a break with the past, this Fourth Edition de-emphasizes the design and physical operating basis of the instrumentation, including the electron sources, lenses, detectors, etc. In the modern SEM, many of the low level instrument parameters are now controlled and optimized by the microscope’s software, and user access is restricted. Although the software control system provides efficient and reproducible microscopy and microanalysis, the user must understand the parameter space wherein choices are made to achieve effective and meaningful microscopy, microanalysis, and micro-crystallography. Therefore, special emphasis is placed on beam energy, beam current, electron detector characteristics and controls, and ancillary techniques such as energy dispersive x-ray spectrometry (EDS) and electron backscatter diffraction (EBSD). With 13 years between the publication of the third and fourth editions, new coverage reflects the many improvements in the instrument and analysis techniques. The SEM has evolved into a powerful and versatile characterization platform in which morphology, elemental composition, and crystal structure can be evaluated simultaneously. Extension of the SEM into a "dual beam" platform incorporating both electron and ion columns allows precision modification of the specimen by focused ion beam milling. New coverage in the Fourth Edition includes the increasing use of field emission guns and SEM instruments with high resolution capabilities, variable pressure SEM operation, theory, and measurement of x-rays with high throughput silicon drift detector (SDD-EDS) x-ray spectrometers. In addition to powerful vendor- supplied software to support data collection and processing, the microscopist can access advanced capabilities available in free, open source software platforms, including the National Institutes of Health (NIH) ImageJ-Fiji for image processing and the National Institute of Standards and Technology (NIST) DTSA II for quantitative EDS x-ray microanalysis and spectral simulation, both of which are extensively used in this work. However, the user has a responsibility to bring intellect, curiosity, and a proper skepticism to information on a computer screen and to the entire measurement process. This book helps you to achieve this goal. Realigns the text with the needs of a diverse audience from researchers and graduate students to SEM operators and technical managers Emphasizes practical, hands-on operation of the microscope, particularly user selection of the critical operating parameters to achieve meaningful results Provides step-by-step overviews of SEM, EDS, and EBSD and checklists of critical issues for SEM imaging, EDS x-ray microanalysis, and EBSD crystallographic measurements Makes extensive use of open source software: NIH ImageJ-FIJI for image processing and NIST DTSA II for quantitative EDS x-ray microanalysis and EDS spectral simulation. Includes case studies to illustrate practical problem solving Covers Helium ion scanning microscopy Organized into relatively self-contained modules – no need to "read it all" to understand a topic Includes an online supplement—an extensive "Database of Electron–Solid Interactions"—which can be accessed on SpringerLink, in Chapter 3

Download or read book 4d Electron Microscopy Imaging In Space And Time written by Ahmed H Zewail and published by World Scientific. This book was released on 2009-12-24 with total page 359 pages. Available in PDF, EPUB and Kindle. Book excerpt: The modern electron microscope, as a result of recent revolutionary developments and many evolutionary ones, now yields a wealth of quantitative knowledge pertaining to structure, dynamics, and function barely matched by any other single scientific instrument. It is also poised to contribute much new spatially-resolved and time-resolved insights of central importance in the exploration of most aspects of condensed matter, ranging from the physical to the biological sciences.Whereas in all conventional EM methods, imaging, diffraction, and chemical analyses have been conducted in a static — time-integrated — manner, now it has become possible to unite the time domain with the spatial one, thereby creating four-dimensional (4D) electron microscopy. This advance is based on the fundamental concept of timed, coherent single-electron packets, or electron pulses, which are liberated with femtosecond durations. Structural phase transitions, mechanical deformations, and the embryonic stages of melting and crystallization are examples of phenomena that can now be imaged in unprecedented structural detail with high spatial resolution, and ten orders of magnitude as fast as hitherto.No monograph in existence attempts to cover the revolutionary dimensions that EM in its various modes of operation nowadays makes possible. The authors of this book chart these developments, and also compare the merits of coherent electron waves with those of synchrotron radiation. They judge it prudent to recall some important basic procedural and theoretical aspects of imaging and diffraction so that the reader may better comprehend the significance of the new vistas and applications now afoot.This book is not a vade mecum — numerous other texts are available for the practitioner for that purpose. It is instead an in-depth exposé of the paradigm concepts and the developed techniques that can now be executed to gain new knowledge in the entire domain of biological and physical science, and in the four dimensions of space and time./a

Download or read book User Facilities of the Office of Basic Energy Sciences written by and published by . This book was released on 2009 with total page 72 pages. Available in PDF, EPUB and Kindle. Book excerpt: "This brochure overviews the scientific infrastructure that is constructed, maintained, and operated at Department of Energy laboratories for the pursuit of energy-related research." -- cf p. 4

Download or read book Publications of the National Institute of Standards and Technology Catalog written by National Institute of Standards and Technology (U.S.) and published by . This book was released on 1991 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt: