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Book Surface Polishing of Niobium for Superconducting Radio Frequency  SRF  Cavity Applications

Download or read book Surface Polishing of Niobium for Superconducting Radio Frequency SRF Cavity Applications written by and published by . This book was released on 2014 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Niobium cavities are important components in modern particle accelerators based on superconducting radio frequency (SRF) technology. The interior of SRF cavities are cleaned and polished in order to produce high accelerating field and low power dissipation on the cavity wall. Current polishing methods, buffered chemical polishing (BCP) and electro-polishing (EP), have their advantages and limitations. We seek to improve current methods and explore laser polishing (LP) as a greener alternative of chemical methods. The topography and removal rate of BCP at different conditions (duration, temperature, sample orientation, flow rate) was studied with optical microscopy, scanning electron microscopy (SEM), and electron backscatter diffraction (EBSD). Differential etching on different crystal orientations is the main contributor to fine grain niobium BCP topography, with gas evolution playing a secondary role. The surface of single crystal and bi-crystal niobium is smooth even after heavy BCP. The topography of fine grain niobium depends on total removal. The removal rate increases with temperature and surface acid flow rate within the rage of 0~20 °C, with chemical reaction being the possible dominate rate control mechanism. Surface flow helps to regulate temperature and avoid gas accumulation on the surface. The effect of surface flow rate on niobium EP was studied with optical microscopy, atomic force microscopy (AFM), and power spectral density (PSD) analysis. Within the range of 0~3.7 cm/s, no significant difference was found on the removal rate and the macro roughness. Possible improvement on the micro roughness with increased surface flow rate was observed. The effect of fluence and pulse accumulation on niobium topography during LP was studied with optical microscopy, SEM, AFM, and PSD analysis. Polishing on micro scale was achieved within fluence range of 0.57~0.90 J/cm2, with pulse accumulation adjusted accordingly. Larger area treatment was proved possible by overlapping laser tracks at proper ratio. Comparison of topography and PSD indicates that LP smooths the surface in a way similar to EP. The optimized LP parameters were applied to different types of niobium surfaces representing different stages in cavity fabrication. LP reduces the sharpness on rough surfaces effectively, while doing no harm to smooth surfaces. Secondary ion mass spectrometer (SIMS) analysis showed that LP reduces the oxide layer slightly and no contamination occurred from LP. EBSD showed no significant change on crystal structure after LP.

Book Superconducting Technology  10 Case Studies

Download or read book Superconducting Technology 10 Case Studies written by K Fossheim and published by World Scientific. This book was released on 1991-07-22 with total page 251 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book contains an interdisciplinary selection of timely articles which cover a wide range of superconducting technologies ranging from high tech medicine (10-12 Gauss) to multipurpose sensors, microwaves, radio engineering, magnet technology for accelerators, magnetic energy storage, and power transmission on the 109 watt scale. It is aimed primarily at the non-specialist and will be suitable as an introductory course book for those in the relevant fields and related industries. As shown in the title several examples of high-Tc applications are included. While low-Tc is still the leading technology, for instance, in cables and SQUIDS, case studies in these areas are presented.

Book Surface Studies of Acid treated Niobium for Superconducting Radio Frequency Cavities

Download or read book Surface Studies of Acid treated Niobium for Superconducting Radio Frequency Cavities written by David R. Smith and published by . This book was released on 2004 with total page 94 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Fastest Electropolishing Technique on Niobium for Particle Accelerators

Download or read book Fastest Electropolishing Technique on Niobium for Particle Accelerators written by and published by . This book was released on 2011 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Field emission on the inner surfaces of niobium (Nb) superconducting radio frequency (SRF) cavities is still one of the major obstacles for reaching high accelerating gradients for SRF community. Our previous experimental results [1] seemed to imply that the threshold of field emission was related to the thickness of Nb surface oxide layers. In this contribution, a more detailed study on the influences of the surface oxide layers on the field emission on Nb surfaces will be reported. By anodization technique, the thickness of the surface pentoxide layer was artificially fabricated from 3nm up to 460nm. A home-made scanning field emission microscope (SFEM) was employed to perform the scans on the surfaces. Emitters were characterized using a scanning electron microscope together with an energy dispersive x-ray analyzer. The experimental results could be understood by a simple model calculation based on classic electromagnetic theory as shown in Ref. 1. Possibly implications for Nb SRF cavity applications from this study will be discussed.

Book RF Superconductivity for Accelerators

Download or read book RF Superconductivity for Accelerators written by Hasan Padamsee and published by John Wiley & Sons. This book was released on 2008-02-26 with total page 548 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book introduces some of the key ideas of this exciting field, using a pedagogic approach, and presents a comprehensive overview of the field. It is divided into four parts. The first part introduces the basic concepts of microwave cavities for particle acceleration. The second part is devoted to the observed behavior of superconducting cavities. In the third part,general issues connected with beam-cavity interaction and the related issues for the critical components are covered. The final part discusses applications of superconducting cavities to frontier accelerators of the future, drawing heavily on the examples that are in their most advanced stage. Each part of the book ends in a Problems section to illustrate and amplify text material as well as draw on example applications of superconducting cavities to existing and future accelerators.

Book RF Superconductivity

Download or read book RF Superconductivity written by Hasan Padamsee and published by John Wiley & Sons. This book was released on 2009-04-20 with total page 465 pages. Available in PDF, EPUB and Kindle. Book excerpt: This is the second book to RF Superconducting, written by one of the leading experts. The book provides fast and up-to-date access to the latest advances in the key technology for future accelerators. Experts as well as newcomers to the field will benefit from the discussion of progress in the basic science, technology as well as recent and forthcoming applications. Researchers in accelerator physics will also find much that is relevant to their discipline.

Book Superconducting Radiofrequency Technology for Accelerators

Download or read book Superconducting Radiofrequency Technology for Accelerators written by Hasan Padamsee and published by John Wiley & Sons. This book was released on 2023-05-15 with total page 405 pages. Available in PDF, EPUB and Kindle. Book excerpt: Superconducting Radiofrequency Technology for Accelerators Single source reference enabling readers to understand and master state-of-the-art accelerator technology Superconducting Radiofrequency Technology for Accelerators provides a quick yet thorough overview of the key technologies for current and future accelerators, including those projected to enable breakthrough developments in materials science, nuclear and astrophysics, high energy physics, neutrino research and quantum computing. The work is divided into three sections. The first part provides a review of RF superconductivity basics, the second covers new techniques such as nitrogen doping, nitrogen infusion, oxide-free niobium, new surface treatments, and magnetic flux expulsion, high field Q slope, complemented by discussions of the physics of the improvements stemming from diagnostic techniques and surface analysis as well as from theory. The third part reviews the on-going applications of RF superconductivity in already operational facilities and those under construction such as light sources, proton accelerators, neutron and neutrino sources, ion accelerators, and crab cavity facilities. The third part discusses planned accelerator projects such as the International Linear Collider, the Future Circular Collider, the Chinese Electron Positron Collider, and the Proton Improvement Plan-III facility at Fermilab as well as exciting new developments in quantum computing using superconducting niobium cavities. Written by the leading expert in the field of radiofrequency superconductivity, Superconducting Radiofrequency Technology for Accelerators covers other sample topics such as: Fabrication and processing on Nb-based SRF structures, covering cavity fabrication, preparation, and a decade of progress in the field SRF physics, covering zero DC resistance, the Meissner effect, surface resistance and surface impedance in RF fields, and non-local response of supercurrent N-doping and residual resistance, covering trapped DC flux losses, hydride losses, and tunneling measurements Theories for anti-Q-slope, covering the Xiao theory, the Gurevich theory, non-equilibrium superconductivity, and two fluid model based on weak defects Superconducting Radiofrequency Technology for Accelerators is an essential reference for high energy physicists, power engineers, and electrical engineers who want to understand the latest developments of accelerator technology and be able to harness it to further research interest and practical applications.

Book Integrated Surface Topography Characterization of Variously Polished Niobium for Superconducting Particle Accelerators

Download or read book Integrated Surface Topography Characterization of Variously Polished Niobium for Superconducting Particle Accelerators written by and published by . This book was released on 2009 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: As superconducting niobium radio-frequency (SRF) cavities approach fundamental material limits, there is increased interest in understanding the details of topographical influences on realized performance limitations. Micro-and nano-roughness are implicated in both direct geometrical field enhancements as well as complications of the composition of the 50 nm surface layer in which the super-currents flow. Interior surface chemical polishing (BCP/EP) to remove mechanical damage leaves surface topography, including pits and protrusions of varying sharpness. These may promote RF magnetic field entry, locally quenching superconductivity, so as to degrade cavity performance. A more incisive analysis of surface topography than the widely-used average roughness is needed. In this study, a power spectral density (PSD) approach based on Fourier analysis of surface topography data acquired by both stylus profilometry and atomic force microscopy (AFM) is being used to distinguish the scale-dependent smoothing effects. The topographical evolution of the Nb surface as a function of different steps of EP is reported, resulting in a novel qualitative and quantitative description of Nb surface topography.

Book Spectroscopic Studies of Surface Treatments for Nb SRF Cavities

Download or read book Spectroscopic Studies of Surface Treatments for Nb SRF Cavities written by Tyagi Puneet Veer and published by LAP Lambert Academic Publishing. This book was released on 2015-12-31 with total page 124 pages. Available in PDF, EPUB and Kindle. Book excerpt: The superconducting radio frequency (SRF) cavities are being used worldwide in particle accelerators to achieve a high energy beam of charged particles. These cavities are made of high purity niobium (Nb) material and work at 2 K temperature. The inner surface of these cavities plays the most important role in order to obtain good performances in terms of the high field gradient. Therefore, the surface treatments associated with SRF cavities are the key issues toward the achievement of the high field gradient larger than 35 MV/m during vertical test of the nine-cell cavity for International Linear Collider (ILC). In the recent years, extensive research has been done to enhance the cavity performance by applying improved surface treatments such as mechanical grinding, buffered chemical polishing (BCP), electropolishing (EP), electrochemical buffing (ECB), mechanochemical polishing (MCP), tumbling, etc., followed by various post-treatment methods such as ultrasonic pure water rinse, alcoholic rinse, high pressure water rinse (HPR), hydrogen per oxide rinse and baking etc. to obtain smooth and contaminant free surface.

Book Laser Nitriding for Niobium Superconducting Radio frequency Accelerator Cavities

Download or read book Laser Nitriding for Niobium Superconducting Radio frequency Accelerator Cavities written by and published by . This book was released on 2010 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Particle accelerators are a key tool for scientific research ranging from fundamental studies of matter to analytical studies at light sources. Cost-forperformance is critical, both in terms of initial capital outlay and ongoing operating expense, especially for electricity. It depends on the niobium superconducting radiofrequency (SRF) accelerator cavities at the heart of most of these machines. Presently Nb SRF cavities operate near 1.9 K, well (and expensively) below the 4.2 K atmospheric boiling point of liquid He. Transforming the 40 nm thick active interior surface layer from Nb to delta NbN (Tc = 17 K instead of 9.2 K) appears to be a promising approach. Traditional furnace nitriding appears to have not been successful for this. Further, exposing a complete SRF cavity to the time-temperature history required for nitriding risks mechanical distortion. Gas laser nitriding instead has been applied successfully to other metals [P. Schaaf, Prog. Mat. Sci. 47 (2002) 1]. The beam dimensions and thermal diffusion length permit modeling in one dimension to predict the time course of the surface temperature for a range of per-pulse energy densities. As with the earlier work, we chose conditions just sufficient for boiling as a reference point. We used a Spectra Physics HIPPO nanosecond laser (l = 1064 nm, Emax= 0.392 mJ, beam spot@ 34 microns, PRF =15 - 30 kHz) to obtain an incident fluence of 1.73 - 2.15 J/cm2 for each laser pulse at the target. The target was a 50 mm diameter SRF-grade Nb disk maintained in a nitrogen atmosphere at a pressure of 550 - 625 torr and rotated at a constant speed of 9 rpm. The materials were examined by scanning electron microscopy (SEM), electron probe microanalysis (EPMA) and x-ray diffraction (XRD). The SEM images show a sharp transition with fluence from a smooth, undulating topography to significant roughening, interpreted here as the onset of ablation. EPMA measurements of N/Nb atom ratio as a function of depth found a constant value to depths greater than the SRF active layer thickness. Certain irradiation conditions resulted in values consistent with formation of delta NbN. Under certain irradiation conditions, XRD data were consistent only with delta NbN on top of Nb metal. Funding: authored by Jefferson Science Associates LLC under US DOE Contract De-AC05-06OR23177. We are indebted to Prof. P. Schaaf (Goettingen) for the simulation code and helpful discussions.

Book Surface Characterization of Impurities in Superconducting Niobium for Radio Frequency  RF  Cavities Used in Particle Accelerators

Download or read book Surface Characterization of Impurities in Superconducting Niobium for Radio Frequency RF Cavities Used in Particle Accelerators written by Prateek Maheshwari and published by . This book was released on 2012 with total page 236 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Superconducting Thin Films for the Enhancement of Superconducting Radio Frequency Accelerator Cavities

Download or read book Superconducting Thin Films for the Enhancement of Superconducting Radio Frequency Accelerator Cavities written by Matthew C. Burton and published by . This book was released on 2017 with total page 151 pages. Available in PDF, EPUB and Kindle. Book excerpt: Bulk niobium (Nb) superconducting radio frequency (SRF) cavities are currently the preferred method for acceleration of charged particles at accelerating facilities around the world. However, bulk Nb cavities have poor thermal conductance, impose material and design restrictions on other components of a particle accelerator, have low reproducibility and are approaching the fundamental material-dependent accelerating field limit of approximately 50MV/m. Since the SRF phenomena occurs at surfaces within a shallow depth of ~1 μm, a proposed solution to this problem has been to utilize thin film technology to deposit superconducting thin films on the interior of cavities to engineer the active SRF surface in order to achieve cavities with enhanced properties and performance. Two proposed thin film applications for SRF cavities are: 1) Nb thin films coated on bulk cavities made of suitable castable metals (such as copper or aluminum) and 2) multilayer films designed to increase the accelerating gradient and performance of SRF cavities. While Nb thin films on copper (Cu) cavities have been attempted in the past using DC magnetron sputtering (DCMS), such cavities have never performed at the bulk Nb level. However, new energetic condensation techniques for film deposition, such as High Power Impulse Magnetron Sputtering (HiPIMS), offer the opportunity to create suitably thick Nb films with improved density, microstructure and adhesion compared to traditional DCMS. Clearly use of such novel technique requires fundamental studies to assess surface evolution and growth modes during deposition and resulting microstructure and surface morphology and the correlation with RF superconducting properties. Here we present detailed structure-property correlative research studies done on Nb/Cu thin films and NbN- and NbTiN-based multilayers made using HiPIMS and DCMS, respectively.

Book Roughness Analysis of Variously Polished Niobium Surfaces

Download or read book Roughness Analysis of Variously Polished Niobium Surfaces written by and published by . This book was released on 2008 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Niobium superconducting radio frequency (SRF) cavities have gained widespread use in accelerator systems. It has been shown that surface roughness is a determining factor in the cavities' effi ciency and maximum accelerating potential achievable through this technology. Irregularities in the surface can lead to spot heating, undesirable local electrical fi eld enhancement and electron multipacting. Surface quality is typically ensured through the use of acid etching in a Buffered Chemical Polish (BCP) bath and electropolishing (EP). In this study, the effects of these techniques on surface morphology have been investigated in depth. The surface of niobium samples polished using different combinations of these techniques has been characterized through atomic force microscopy (AFM) and stylus profi lometry across a range of length scales. The surface morphology was analyzed using spectral techniques to determine roughness and characteristic dimensions. Experimentation has shown that this method is a valuable tool that provides quantitative information about surface roughness at different length scales. It has demonstrated that light BCP pretreatment and lower electrolyte temperature favors a smoother electropolish. These results will allow for the design of a superior polishing process for niobium SRF cavities and therefore increased accelerator operating effi ciency and power.

Book Topographic Power Spectral Density Study of the Effect of Surface Treatment Processes on Niobium for Superconducting Radio Frequency Accelerator Cavities

Download or read book Topographic Power Spectral Density Study of the Effect of Surface Treatment Processes on Niobium for Superconducting Radio Frequency Accelerator Cavities written by and published by . This book was released on 2012 with total page 43502 pages. Available in PDF, EPUB and Kindle. Book excerpt: Microroughness is viewed as a critical issue for attaining optimum performance of superconducting radio frequency accelerator cavities. The principal surface smoothing methods are buffered chemical polish (BCP) and electropolish (EP). The resulting topography is characterized by atomic force microscopy (AFM). The power spectral density (PSD) of AFM data provides a more thorough description of the topography than a single-value roughness measurement. In this work, one dimensional average PSD functions derived from topography of BCP and EP with different controlled starting conditions and durations have been fitted with a combination of power law, K correlation, and shifted Gaussian models to extract characteristic parameters at different spatial harmonic scales. While the simplest characterizations of these data are not new, the systematic tracking of scale-specific roughness as a function of processing is new and offers feedback for tighter process prescriptions more knowledgably targeted at beneficial niobium topography for superconducting radio frequency applications.

Book Production of Seamless Superconducting Radio Frequency Cavities from Ultra fine Grained Niobium  Phase II Final Report

Download or read book Production of Seamless Superconducting Radio Frequency Cavities from Ultra fine Grained Niobium Phase II Final Report written by and published by . This book was released on 2009 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: The positron and electron linacs of the International Linear Collider (ILC) will require over 14,000, nine-cell, one meter length, superconducting radio frequency (SRF) cavities [ILC Reference Design Report, 2007]. Manufacturing on this scale will benefit from more efficient fabrication methods. The current methods of fabricating SRF cavities involve deep drawing of the halves of each of the elliptical cells and joining them by high-vacuum, electron beam welding, with at least 19 circumferential welds per cavity. The welding is costly and has undesirable effects on the cavity surfaces, including grain-scale surface roughening at the weld seams. Hydroforming of seamless tubes avoids welding, but hydroforming of coarse-grained seamless tubes results in strain-induced surface roughening. Surface roughness limits accelerating fields, because asperities prematurely exceed the critical magnetic field and become normal conducting. This project explored the technical and economic feasibility of an improved processing method for seamless tubes for hydroforming. Severe deformation of bulk material was first used to produce a fine structure, followed by extrusion and flow-forming methods of tube making. Extrusion of the randomly oriented, fine-grained bulk material proceeded under largely steady-state conditions, and resulted in a uniform structure, which was found to be finer and more crystallographically random than standard (high purity) RRR niobium sheet metal. A 165 mm diameter billet of RRR grade niobium was processed into five, 150 mm I.D. tubes, each over 1.8 m in length, to meet the dimensions used by the DESY ILC hydroforming machine. Mechanical properties met specifications. Costs of prototype tube production were approximately twice the price of RRR niobium sheet, and are expected to be comparable with economies of scale. Hydroforming and superconducting testing will be pursued in subsequent collaborations with DESY and Fermilab. SRF Cavities are used to construct particle accelerators for high-energy physics research, as well as for lower energy particle accelerators, and Free Electron Lasers. These machines have applications in the fields of basic science, industrial processing, medical diagnostics, pharmaceutical research and weapons systems. The scientific community and the general public will benefit from the implementation of this technology since lower production costs will increase the availability of SRF particle accelerators.