Download or read book Spectroscopic Methods in Organic Chemistry written by Dudley H. Williams and published by McGraw-Hill Companies. This book was released on 1980 with total page 268 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Spectroscopic Techniques for Organic Chemists written by James W. Cooper and published by . This book was released on 1980-05-02 with total page 408 pages. Available in PDF, EPUB and Kindle. Book excerpt: "Spectroscopy has become the organic chemist's most important tool in identifying compounds and studying their interactions. The arsenal of techniques available to the research chemist has, over the years, expanded from the familiar infrared, proton nmr and mass spectroscopy, to include the routine use of carbon-13 nmr spectroscopy and such modern methods of data acquisition as Fourier transform nmr, laser Raman spectroscopy, and UV spectroscopy. This book serves as an introduction to all of the major spectroscopic techniques, using over 200 actual spectra as examples, and providing a substantial number of problems and completely worked-through solutions that demonstrate how spectral techniques are applied to analytical problems. The book represents a significant departure from the scope of general spectroscopy texts. In addition to the usual chapters on infrared, proton nmr and mass spectroscopy, a number of increasingly important techniques have been included for the first time. Chapter 4, for instance, introduces not only the analysis of proton nmr spectra, but also describes iteration of theoretical nmr spectra for a best fit with observed experimental spectra using the popular LAOCOON III program. A complete FORTRAN listing for a conversational pendix I. Chapter 5 presents a non-mathematical description of Fourier transform nmr, including signal averaging, decoupling methods, quadrature detection, and the Fourier transform itself, and Chapter 6 goes on to describe Fourier transform techniques in carbon-13 spectroscopy. Chapter 7 introduces simple Huckel M.O. theory and the SHMO program for calculating the resonance stabilization of various systems, material which lays the groundwork for Chapter 8's discussion of ultraviolet spectroscopy using examples of ways in which energies can be correlated with SHMO parameters. A SHMO timesharing conversational program is listed in Appendix II. Finally, Chapter 10 outlines the organic chemical applications of laser Raman spectroscopy and the functional groups most easily identified using this method. Both organic chemists and graduate and advanced undergraduate students will find in the book's breadth of coverage an ideal introduction to the identification of organic compounds by spectroscopic means."- Publisher.
Download or read book VCD Spectroscopy for Organic Chemists written by Philip J. Stephens and published by CRC Press. This book was released on 2012-06-25 with total page 372 pages. Available in PDF, EPUB and Kindle. Book excerpt: Stimulated by the increasing importance of chiral molecules as pharmaceuticals and the need for enantiomerically pure drugs, techniques in chiral chemistry have been expanded and refined, especially in the areas of chromatography, asymmetric synthesis, and spectroscopic methods for chiral molecule structural characterization. In addition to synthet
Download or read book Spectroscopic Methods in Organic Chemistry written by Dudley H. Williams and published by McGraw-Hill Companies. This book was released on 1989 with total page 292 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Spectroscopic Methods in Organic Chemistry written by Ian Fleming and published by Springer Nature. This book was released on 2020-01-17 with total page 438 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is a well-established guide to the interpretation of the mass, ultraviolet, infrared and nuclear magnetic resonance spectra of organic compounds. It is designed for students of organic chemistry taking a course in the application of these techniques to structure determination. The text also remains useful as a source of data for organic chemists to keep on their desks throughout their career. In the seventh edition, substantial portions of the text have been revised reflecting knowledge gained during the author's teaching experience over the last seven years. The chapter on NMR has been divided into two separate chapters covering the 1D and 2D experiments. The discussion is also expanded to include accounts of the physics at a relatively simple level, following the development of the magnetization vectors as each pulse sequence is introduced. The emphasis on the uses of NMR spectroscopy in structure determination is retained. Worked examples and problem sets are included on a chapter level to allow students to practise their skills by determining the chemical structures of unknown compounds.
Download or read book Organic Spectroscopy written by Lal Dhar Singh Yadav and published by Springer Science & Business Media. This book was released on 2013-08-30 with total page 334 pages. Available in PDF, EPUB and Kindle. Book excerpt: Organic Spectroscopy presents the derivation of structural information from UV, IR, Raman, 1H NMR, 13C NMR, Mass and ESR spectral data in such a way that stimulates interest of students and researchers alike. The application of spectroscopy for structure determination and analysis has seen phenomenal growth and is now an integral part of Organic Chemistry courses. This book provides: -A logical, comprehensive, lucid and accurate presentation, thus making it easy to understand even through self-study; -Theoretical aspects of spectral techniques necessary for the interpretation of spectra; -Salient features of instrumentation involved in spectroscopic methods; -Useful spectral data in the form of tables, charts and figures; -Examples of spectra to familiarize the reader; -Many varied problems to help build competence ad confidence; -A separate chapter on ‘spectroscopic solutions of structural problems’ to emphasize the utility of spectroscopy. Organic Spectroscopy is an invaluable reference for the interpretation of various spectra. It can be used as a basic text for undergraduate and postgraduate students of spectroscopy as well as a practical resource by research chemists. The book will be of interest to chemists and analysts in academia and industry, especially those engaged in the synthesis and analysis of organic compounds including drugs, drug intermediates, agrochemicals, polymers and dyes.
Download or read book High resolution NMR Techniques in Organic Chemistry written by T. Claridge and published by Elsevier. This book was released on 1999-12-24 with total page 408 pages. Available in PDF, EPUB and Kindle. Book excerpt: From the initial observation of proton magnetic resonance in water and in paraffin, the discipline of nuclear magnetic resonance has seen unparalleled growth as an analytical method. Modern NMR spectroscopy is a highly developed, yet still evolving, subject which finds application in chemistry, biology, medicine, materials science and geology. In this book, emphasis is on the more recently developed methods of solution-state NMR applicable to chemical research, which are chosen for their wide applicability and robustness. These have, in many cases, already become established techniques in NMR laboratories, in both academic and industrial establishments. A considerable amount of information and guidance is given on the implementation and execution of the techniques described in this book.
Download or read book Spectroscopic Methods in Organic Chemistry written by Stefan Bienz and published by Thieme. This book was released on 2021-07-09 with total page 510 pages. Available in PDF, EPUB and Kindle. Book excerpt: Boost your knowledge of modern spectroscopic methods! This reference work provides you with essential knowledge for the application of modern spectroscopic methods in organic chemistry. All methods are explained based on typical practical examples, theoretical aspects, and applications. The following spectroscopic methods are explained and examples are given: UV/Vis Spectroscopy Infrared (IR) and Raman Spectroscopy Nuclear Magnetic Resonance Spectroscopy (NMR) Mass Spectrometry (MS) The textbook has been a standard reference for decades. As it conveys necessary knowledge for examinations at all universities it is compulsory reading for every organic chemistry student!
Download or read book Tables of Spectral Data for Structure Determination of Organic Compounds written by Ernö Pretsch and published by Springer Science & Business Media. This book was released on 2013-06-29 with total page 325 pages. Available in PDF, EPUB and Kindle. Book excerpt: Although numerical data are, in principle, universal, the compilations presented in this book are extensively annotated and interleaved with text. This translation of the second German edition has been prepared to facilitate the use of this work, with all its valuable detail, by the large community of English-speaking scientists. Translation has also provided an opportunity to correct and revise the text, and to update the nomenclature. Fortunately, spectroscopic data and their relationship with structure do not change much with time so one can predict that this book will, for a long period of time, continue to be very useful to organic chemists involved in the identification of organic compounds or the elucidation of their structure. Klaus Biemann Cambridge, MA, April 1983 Preface to the First German Edition Making use of the information provided by various spectroscopic tech niques has become a matter of routine for the analytically oriented organic chemist. Those who have graduated recently received extensive training in these techniques as part of the curriculum while their older colleagues learned to use these methods by necessity. One can, therefore, assume that chemists are well versed in the proper choice of the methods suitable for the solution of a particular problem and to translate the experimental data into structural information.
Download or read book Introduction to Organic Spectroscopy written by Laurence M. Harwood and published by . This book was released on 1997 with total page 91 pages. Available in PDF, EPUB and Kindle. Book excerpt: An understanding of spectroscopic techniques in the analysis of chemical structures is essential to all chemistry degree courses. This new addition to the Oxford Chemistry Primers series provides the essential material needed by undergraduates, in a compact form. It will be beneficial to postgraduates in organic chemistry as reference material in their daily research.
Download or read book Circular Dichroism and Magnetic Circular Dichroism Spectroscopy for Organic Chemists written by Nagao Kobayashi and published by Royal Society of Chemistry. This book was released on 2011-11-10 with total page 216 pages. Available in PDF, EPUB and Kindle. Book excerpt: CD and MCD spectroscopy can provide key information about the conformations and electronic states of chromophore containing molecules. However, the theory has remained too challenging and inaccessible for many organic chemists and biochemists and only a few researchers have carried out detailed quantitative analyses of their spectral data. This is not surprising as people who excel at spectroscopic theory usually lack the skills set required to design and synthesise the molecules that would be most appropriate for describing and explaining the theory of CD and MCD spectroscopy. Most of the books that have been written on the subject have, therefore, been based on very dense sets of mathematical equations. This timely book rectifies that situation by summarizing the relationship between the different types of spectra and by describing in detail the qualitative and quantitative methods which can readily be used to analyse CD and MCD spectral data. During the last decade the authors have successfully synthesized several molecules to illustrate key points related to the theory of CD and MCD spectroscopy, resulting in this definitive book providing key practical knowledge in a readily accessible style. It is aimed primarily at organic chemists and biochemists and is required reading for researchers active in the field. In the introduction, the book describes the types of information that can be derived from CD and MCD spectroscopy. After a detailed explanation of the theory of electronic absorption spectroscopy, it then provides practical in depth examples of the various analytical methods that can be carried out with CD and MCD spectral data. This makes the theory of these techniques much more accessible for researchers who do not specialise in physical chemistry. The book concludes by briefly summarizing the key mathematical expressions associated with each technique.
Download or read book Inorganic Spectroscopic Methods written by Alan K. Brisdon and published by OUP Oxford. This book was released on 1998-06-18 with total page 100 pages. Available in PDF, EPUB and Kindle. Book excerpt: A knowledge of spectroscopic methods is required to interpret the shape and structure of compounds - this informative book concentrates on their application to inorganic compounds. The emphasis is placed on obtaining and interpreting the data rather than concentrating on the theory. To this end, examples are given in the text and worked through to show the processes involved in assigning spectra and obtaining information from them. This essential text for all undergraduate chemists will also benefit postgraduate students researching in the field of inorganic chemistry.
Download or read book Essential Practical NMR for Organic Chemistry written by S. A. Richards and published by John Wiley & Sons. This book was released on 2010-12-07 with total page 345 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book describes the use of NMR spectroscopy for dealing with problems of small organic molecule structural elucidation. It features a significant amount of vital chemical shift and coupling information but more importantly, it presents sound principles for the selection of the techniques relevant to the solving of particular types of problem, whilst stressing the importance of extracting the maximum available information from the simple 1-D proton experiment and of using this to plan subsequent experiments. Proton NMR is covered in detail, with a description of the fundamentals of the technique, the instrumentation and the data that it provides before going on to discuss optimal solvent selection and sample preparation. This is followed by a detailed study of each of the important classes of protons, breaking the spectrum up into regions (exchangeables, aromatics, heterocyclics, alkenes etc.). This is followed by consideration of the phenomena that we know can leave chemists struggling; chiral centres, restricted rotation, anisotropy, accidental equivalence, non-first-order spectra etc. Having explained the potential pitfalls that await the unwary, the book then goes on to devote chapters to the chemical techniques and the most useful instrumental ones that can be employed to combat them. A discussion is then presented on carbon-13 NMR, detailing its pros and cons and showing how it can be used in conjunction with proton NMR via the pivotal 2-D techniques (HSQC and HMBC) to yield vital structural information. Some of the more specialist techniques available are then discussed, i.e. flow NMR, solvent suppression, Magic Angle Spinning, etc. Other important nuclei are then discussed and useful data supplied. This is followed by a discussion of the neglected use of NMR as a tool for quantification and new techniques for this explained. The book then considers the safety aspects of NMR spectroscopy, reviewing NMR software for spectral prediction and data handling and concludes with a set of worked Q&As.
Download or read book Spectroscopic Methods in Organic Chemistry written by Manfred Hesse and published by Thieme Medical Publishers. This book was released on 2008 with total page 476 pages. Available in PDF, EPUB and Kindle. Book excerpt: Download Area for Lecturers:www.thieme.de/specials/hmz_en.html This book provides the necessary equipment for the application of spectroscopic methods in organic chemistry, as required as part of chemistry courses in all universities. The following methods are explained and examples given: UV/Vis Spectroscopy, derivative Spectroscopy, chirooptical methods CD and ORD. Aggregated molecules, charge transfer complexes, conjugated oligomers. Infrared (IR) and Raman Spectroscopy, Fourier transform IR spectroscopy, and GC/IRcombination methods. Nuclear Magnetic Resonance Spectroscopy (NMR), 1H-, 13C-, 19F-, 15N- und 31P-NMR, spin decoupling, triple resonance, INDOR difference spectroscopy, 2D- and 3D-NMR, COSY, TOCSY, ROESY and NOESY spectra, NOE, INEPT, and DEPT technique, DEPTQ, HETCOR, HRMAS, INADEQUATE and lanthanide shift reagents, simulation and calculation of spectra, and the combination of separation and NMR methods. The new 2D NMR techniques TOCSY, HMQC and HMBC, more examples and a guide to completely assign all 1H and 13C NMR signals of a given substrate. Mass spectrometry (MS), electron impact and chemical ionization (EI and CI), fast atom bombardment (FAB), electrospray und thermospray ionization (ESI and TSI), MS/MS technique (MSn), field ionization and field desorption (FI and FD), atmospheric pressure chemical ionization (APCI), MALDI TOF technique, GC/MS, LC/MS, and HPLC-UV(DAD)-APCI combination MS/MS technique. Fourier transform ion cyclotron resonance MS (FT-ICR-MS). The layout and many tables help to introduce the reader to spectroscopy.The extensive and thorough approach makes the text the first choice both as a companion for the professional chemists and as a refresher course in practical spectroscopy.The second English edition is a translation of the 7th German edition, in which several major alterations and didactic improvements have been made. For further information on our chemistry products, please visit: Thieme Chemistry.
Download or read book Techniques in Organic Chemistry written by Jerry R. Mohrig and published by Macmillan. This book was released on 2010-01-06 with total page 487 pages. Available in PDF, EPUB and Kindle. Book excerpt: "Compatible with standard taper miniscale, 14/10 standard taper microscale, Williamson microscale. Supports guided inquiry"--Cover.
Download or read book NMR Spectroscopy Explained written by Neil E. Jacobsen and published by John Wiley & Sons. This book was released on 2007-09-10 with total page 640 pages. Available in PDF, EPUB and Kindle. Book excerpt: NMR Spectroscopy Explained : Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology provides a fresh, practical guide to NMR for both students and practitioners, in a clearly written and non-mathematical format. It gives the reader an intermediate level theoretical basis for understanding laboratory applications, developing concepts gradually within the context of examples and useful experiments. Introduces students to modern NMR as applied to analysis of organic compounds. Presents material in a clear, conversational style that is appealing to students. Contains comprehensive coverage of how NMR experiments actually work. Combines basic ideas with practical implementation of the spectrometer. Provides an intermediate level theoretical basis for understanding laboratory experiments. Develops concepts gradually within the context of examples and useful experiments. Introduces the product operator formalism after introducing the simpler (but limited) vector model.
Download or read book Structural Identification of Organic Compounds with Spectroscopic Techniques written by Yong-Cheng Ning and published by Wiley-VCH. This book was released on 2005-05-06 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt: Clearly structured, easy to read and optimal to understand, this extensive compendium fills the gap between textbooks devoted to either spectra interpretation or basic physical principles. The original Chinese editions have already sold over 18,500 copies, and the material is taken from the latest literature from around the world, plus technical information provided by the manufacturers of spectroscopic instruments. Alongside basic methods, Professor Ning presents up-to-date developments in NMR, MS, IR and Raman spectroscopy, such as pulsed-field gradient technique, LC-NMR, and DOSY. He stresses the application of spectroscopic methods, interpreting them in great detail and depth since most of the selected spectra may be applied to practical work, as well as summarizing the rules for their interpretation. He also incorporates his original ideas, including a comparison of the common points in different spectroscopic techniques. This monograph features a unique structure, a typical example being the discussion of 2D NMR starting from pulse sequence units, which construct various pulse sequences for related 2D NMR. A complete chapter deals with the determination of configurations and conformations of organic compounds and even biological molecules from the viewpoint of spectroscopic methodologies, while one whole section is dedicated to the interpretation of mass spectra produced by soft ionization techniques. The principles of mass analyzers, especially the ion trap, are discussed in great depth, together with a concise summary of the MS fragmentation and rearrangement of common compounds, allowing readers to easily predict related mass spectrometric reactions. All the three kinds of library retrieval of mass spectra are presented in detail, together with recent developments in molecular vibration spectroscopy. The whole is rounded off with several appendices, including a subject index for rapid reference. With a foreword by the Nobel prizewinner, Richard R. Ernst.
