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Book RAPID SEPARATION METHOD FOR EMERGENCY WATER AND URINE SAMPLES

Download or read book RAPID SEPARATION METHOD FOR EMERGENCY WATER AND URINE SAMPLES written by and published by . This book was released on 2008 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: The Savannah River Site Environmental Bioassay Lab participated in the 2008 NRIP Emergency Response program administered by the National Institute for Standards and Technology (NIST) in May, 2008. A new rapid column separation method was used for analysis of actinides and 9°Sr the NRIP 2008 emergency water and urine samples. Significant method improvements were applied to reduce analytical times. As a result, much faster analysis times were achieved, less than 3 hours for determination of 9°Sr and 3-4 hours for actinides. This represents a 25%-33% improvement in analysis times from NRIP 2007 and a ≈100% improvement compared to NRIP 2006 report times. Column flow rates were increased by a factor of two, with no significant adverse impact on the method performance. Larger sample aliquots, shorter count times, faster cerium fluoride microprecipitation and streamlined calcium phosphate precipitation were also employed. Based on initial feedback from NIST, the SRS Environmental Bioassay Lab had the most rapid analysis times for actinides and 9°Sr analyses for NRIP 2008 emergency urine samples. High levels of potential matrix interferences may be present in emergency samples and rugged methods are essential. Extremely high levels of 21°Po were found to have an adverse effect on the uranium results for the NRIP-08 urine samples, while uranium results for NRIP-08 water samples were not affected. This problem, which was not observed for NRIP-06 or NRIP-07 urine samples, was resolved by using an enhanced 21°Po removal step, which will be described.

Book NEW COLUMN SEPARATION METHOD FOR EMERGENCY URINE SAMPLES

Download or read book NEW COLUMN SEPARATION METHOD FOR EMERGENCY URINE SAMPLES written by and published by . This book was released on 2007 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: The Savannah River Site Environmental Bioassay Lab participated in the 2007 NRIP Emergency Response program administered by the National Institute for Standards and Technology (NIST) in May, 2007. A new rapid column separation method was applied directly to the NRIP 2007 emergency urine samples, with only minimal sample preparation to reduce preparation time. Calcium phosphate precipitation, previously used to pre-concentrate actinides and Sr-90 in NRIP 2006 urine and water samples, was not used for the NRIP 2007 urine samples. Instead, the raw urine was acidified and passed directly through the stacked resin columns (TEVA+TRU+SR Resins) to separate the actinides and strontium from the NRIP urine samples more quickly. This improvement reduced sample preparation time for the NRIP 2007 emergency urine analyses significantly. This approach works well for small volume urine samples expected during an emergency response event. Based on initial feedback from NIST, the SRS Environmental Bioassay Lab had the most rapid analysis times for actinides and strontium-90 analyses for NRIP 2007 urine samples.

Book RAPID ANALYSIS OF EMERGENCY URINE AND WATER SAMPLES

Download or read book RAPID ANALYSIS OF EMERGENCY URINE AND WATER SAMPLES written by and published by . This book was released on 2007 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: There is a need for fast, reliable methods for the determination of actinides and Sr-89/90 analysis on environmental and bioassay samples in response to an emergency radiological incident. The SRS (Savannah River Site) Environmental Bioassay Laboratory participated in the National Institute of Standards and Technology Radiochemistry Intercomparison Program (NRIP-06) and analyzed water and urine samples within 8 hours of receipt. The SRS Environmental Laboratory was the only lab that participated in the program that analyzed these samples for both actinides and Sr-89/90 within the requested 8 hour turnaround time. A new, rapid actinide and strontium 89/90 separation method was used for both urine and water samples. This method uses stacked TEVA Resin{reg_sign}, TRU Resin{reg_sign} and Sr-Resin{reg_sign} cartridges from Eichrom Technologies (Darien, IL, USA) that allows the rapid separation of plutonium (Pu), neptunium (Np), uranium (U), and americium (Am), curium (Cm) and thorium (Th) using a single multi-stage column combined with alpha spectrometry. By using vacuum box cartridge technology and stacked cartridges with rapid flow rates, sample preparation time was minimized. This paper discusses the technology and conditions employed for both water and urine samples and presents the SRS performance data on the NRIP-06 samples.

Book Handbook of Radioactivity Analysis

Download or read book Handbook of Radioactivity Analysis written by Michael F. L'Annunziata and published by Academic Press. This book was released on 2012-08-16 with total page 1420 pages. Available in PDF, EPUB and Kindle. Book excerpt: Authoritative reference providing the principles, practical techniques, and procedures for the accurate measurement of radioactivity.

Book Handbook on Radiation Environment  Volume 2

Download or read book Handbook on Radiation Environment Volume 2 written by Dinesh Kumar Aswal and published by Springer Nature. This book was released on with total page 776 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Uranium and Plant Metabolism

Download or read book Uranium and Plant Metabolism written by Gerhard Geipel and published by Springer Nature. This book was released on 2021-09-13 with total page 60 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book explores the uranium uptake by plants and its impact on plant physiology and biochemistry. In the first part of this work, the author summarizes the chemistry of uranium, its use and its environmental distribution. Then, particular attention is given to the methods for uranium detection, and to the plant biochemical reactions that influence the uranium uptake. Readers will also discover several strategies adopted by cells to immobilize and handle uranium.

Book Selected Water Resources Abstracts

Download or read book Selected Water Resources Abstracts written by and published by . This book was released on 1982 with total page 928 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Selected Water Resources Abstracts

Download or read book Selected Water Resources Abstracts written by and published by . This book was released on 1982 with total page 498 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book U S  Government Research Reports

Download or read book U S Government Research Reports written by and published by . This book was released on 1963 with total page 262 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Selected Methods of Emergency Toxicology

Download or read book Selected Methods of Emergency Toxicology written by Willard R. Faulkner and published by American Association for Clinical Chemistry, Incorporated. This book was released on 1986 with total page 128 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Public Works for Water  Pollution Control  and Power Development  and Atomic Energy Commission Appropriation Bill  1971  Atomic Energy Commission     Tennessee Valley Authority

Download or read book Public Works for Water Pollution Control and Power Development and Atomic Energy Commission Appropriation Bill 1971 Atomic Energy Commission Tennessee Valley Authority written by United States. Congress. House. Committee on Appropriations. Subcommittee on Public Works and published by . This book was released on 1970 with total page 1224 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Nuclear Science Abstracts

Download or read book Nuclear Science Abstracts written by and published by . This book was released on 1975 with total page 764 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Modern Environmental Analysis Techniques for Pollutants

Download or read book Modern Environmental Analysis Techniques for Pollutants written by Chaudhery Mustansar Hussain and published by Elsevier. This book was released on 2019-08-20 with total page 424 pages. Available in PDF, EPUB and Kindle. Book excerpt: Modern Environmental Analysis Techniques for Pollutants presents established environmental analysis methods, rapidly emerging technologies, and potential future research directions. As methods of environmental analysis move toward lower impact, lower cost, miniaturization, automation, and simplicity, new methods emerge and ultimately improve the accuracy of their analytical results. This book gives in-depth, step-by-step descriptions of a variety of techniques, including methods used in sampling, field sample handling, sample preparation, quantification, and statistical evaluation. Modern Environmental Analysis Techniques for Pollutants aims to deliver a comprehensive and easy-to-read text for students and researchers in the environmental analysis arena and to provide essential information to consultants and regulators about analytical and quality control procedures helpful in their evaluation and decision-making procedures. Bridges the gap in current literature on analytical chemistry techniques and their application to environmental analysis Covers the use of nanomaterials in environmental analysis, as well as the monitoring and analysis of nanomaterials in the environment Looks to the past, present and future of environmental analysis, with chapters on historical background, established and emerging techniques and instrumentation, and predictions

Book Cumulated Index Medicus

Download or read book Cumulated Index Medicus written by and published by . This book was released on 1976 with total page 1574 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Book Rethinking Faecal Sludge Management in Emergency Settings

Download or read book Rethinking Faecal Sludge Management in Emergency Settings written by Fiona Zakaria and published by CRC Press. This book was released on 2019-07-24 with total page 208 pages. Available in PDF, EPUB and Kindle. Book excerpt: The development of technology in the emergency sanitation sector has not been emphasised sufficiently considering that the management of human excreta is a basic requirement for every person. The lack of technology tailored to emergency situations complicates efforts to cater for sanitation needs in challenging humanitarian crisis. Concerns persists on the lack of faecal sludge management that considers the whole sanitation chain from containment until treatment. This study focused on the development of a smart emergency toilet termed the eSOS (emergency sanitation operation system) smart toilet to address the limitation in technical options. This toilet is based on the eSOS concept that takes into account the entire sanitation chain. This study also addresses the limited time for planning in emergencies by developing a decision support system (DSS) to help quick selection of optimal sanitation options. The aim was to enable users of the DSS to plan their emergency sanitation response within the shortest time possible. The study aims to contribute toward a better emergency sanitation response by application of technology advances.

Book Henry s Clinical Diagnosis and Management by Laboratory Methods E Book

Download or read book Henry s Clinical Diagnosis and Management by Laboratory Methods E Book written by Richard A. McPherson and published by Elsevier Health Sciences. This book was released on 2021-06-09 with total page 1960 pages. Available in PDF, EPUB and Kindle. Book excerpt: For more than 100 years, Henry's Clinical Diagnosis and Management by Laboratory Methods has been recognized as the premier text in clinical laboratory medicine, widely used by both clinical pathologists and laboratory technicians. Leading experts in each testing discipline clearly explain procedures and how they are used both to formulate clinical diagnoses and to plan patient medical care and long-term management. Employing a multidisciplinary approach, it provides cutting-edge coverage of automation, informatics, molecular diagnostics, proteomics, laboratory management, and quality control, emphasizing new testing methodologies throughout. Remains the most comprehensive and authoritative text on every aspect of the clinical laboratory and the scientific foundation and clinical application of today's complete range of laboratory tests. Updates include current hot topics and advances in clinical laboratory practices, including new and extended applications to diagnosis and management. New content covers next generation mass spectroscopy (MS), coagulation testing, next generation sequencing (NGS), transfusion medicine, genetics and cell-free DNA, therapeutic antibodies targeted to tumors, and new regulations such as ICD-10 coding for billing and reimbursement. Emphasizes the clinical interpretation of laboratory data to assist the clinician in patient management. Organizes chapters by organ system for quick access, and highlights information with full-color illustrations, tables, and diagrams. Provides guidance on error detection, correction, and prevention, as well as cost-effective test selection. Includes a chapter on Toxicology and Therapeutic Drug Monitoring that discusses the necessity of testing for therapeutic drugs that are more frequently being abused by users.

Book Applications of LC MS in Toxicology

Download or read book Applications of LC MS in Toxicology written by Aldo Polettini and published by Pharmaceutical Press. This book was released on 2006 with total page 310 pages. Available in PDF, EPUB and Kindle. Book excerpt: Analytical toxicologists are involved in the analysis of drugs and poisons in biological samples in different environments. Many scientists in the field of analytical toxicology have adopted LC-MS in their daily work, and this is illustrated by the increasing numbers of research papers published and presented at relevant conferences.