Download or read book Microstructure and Mechanical Properties of Nickel based Superalloy Hastelloy X Fabricated by Laser Powder Bed Fusion written by Oscar Sanchez Mata and published by . This book was released on 2022 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt: "Additive manufacturing (AM), particularly laser powder bed fusion (LPBF) has been used to process Ni-based superalloys as an alternative to traditional manufacturing methods. However, they can be prone to cracking when fabricated through LPBF. Hastelloy X (HX) is a solid solution strengthened (SSS) alloy that although being categorized as readily weldable, suffers from cracking during LPBF. This document presents a study of crack-free LPBF HX microstructures, their behaviour after post-processing and their relationship with mechanical properties. Moreover, the application of unique microstructural features that result from LPBF processing to scale from bulk to more complex parts and tailor mechanical properties is documented. Crack-free HX fabricated through LPBF from powder having a standard chemical composition is reported. Electron backscatter diffraction (EBSD) analysis evidenced columnar grains parallel to the building direction (BD). The columnar sub-grain solidification microstructure was found to be finer than reported elsewhere. Mo-enriched carbides (~50 nm), were identified along interdendritic regions. The crack-free condition was maintained after heat treatment at 1177 °C for 1 h and its microstructure was analyzed. Dense and crack-free specimens were printed in both horizontal and vertical orientations. Samples were analyzed in as-built (AB), hot isostatic pressing treatment (HIP), and conventional heat treatment (HT) conditions. Tensile testing was done at room and elevated temperature (RT, ET = 750°C). AB samples showed columnar grains and a partial fiber texture aligned with the BD, which was reduced after HIP and HT. Mo and Cr carbides were found at RT which grew after ET. AB samples displayed high ultimate tensile strength (UTS) up to 924 ± 10 MPa, while strength values remained close to a reference HX wrought alloy after HIP and HT. Although lower ductility was observed for AB samples at ET, elongation was improved after HIP and HT. Strength and elongation comparable to that of the wrought alloy at RT can be obtained by only performing conventional HT, without the need of HIP. Dense and crack-free LPBF HX thin cylindrical struts with diameters from 0.25 to 2 mm were built. Their crystallographic texture transitioned from a 110 || BD fiber texture (2 mm), to a single crystal 110 || BD (0.25 mm). The size of cellular sub-grain microstructure increased as strut diameter decreased and was linked with an inverse trend in microhardness, which was the highest in the 2 mm strut due to a smaller cell size. Lower hardness in regions close to the strut edges was also related to a larger observed cell size. From tensile testing, elongation was measured at 35-50%. Deformation twinning and lattice rotation after testing were observed. Differences in strength between struts of different diameter were discussed. Fractography analysis confirmed the ductile fracture behavior. Finally, the unique strong crystallographic texture behaviour of LPBF HX was studied in more detail. Tensile properties at RT were investigated along the 100, 110, and 111 crystallographic orientations. Tensile behavior was highly dependent on crystallographic orientation and showed a good combination of strength and ductility when compared with other LPBF HX. EBSD analysis after fracture revealed deformation twinning in 110 and 111 samples, but not in 100. Crystallographic orientation had an impact on the effective stacking fault energies and on the critical stress for deformation twinning. The latter was near or below the yield strength (YS) value for 110 and 111, while it was above the UTS of the 100 orientation. The YS value of 111 (807 ± 28 MPa) was higher than for 100 (693 ± 8 MPa) and 110 (648 ± 13 MPa). Results suggest that deformation twinning can occur in SSS Ni-based superalloys at RT. In contrast to the 100 and 111 orientations, rotation of the lattice after deformation was found for the 110 direction"--

Download or read book Nickel Cobalt and Their Alloys written by Joseph R. Davis and published by ASM International. This book was released on 2000-01-01 with total page 450 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is a comprehensive guide to the compositions, properties, processing, performance, and applications of nickel, cobalt, and their alloys. It includes all of the essential information contained in the ASM Handbook series, as well as new or updated coverage in many areas in the nickel, cobalt, and related industries.

Download or read book Alloy Design and Characterization of Strengthened Nickel based Superalloys for Additive Manufacturing written by Jinghao Xu and published by Linköping University Electronic Press. This book was released on 2021-01-28 with total page 63 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nickel-based superalloys, an alloy system bases on nickel as the matrix element with the addition of up to 10 more alloying elements including chromium, aluminum, cobalt, tungsten, molybdenum, titanium, and so on. Through the development and improvement of nickel-based superalloys in the past century, they are well proved to show excellent performance at the elevated service temperature. Owing to the combination of extraordinary high-temperature mechanical properties, such as monotonic and cyclic deformation resistance, fatigue crack propagation resistance; and high-temperature chemical properties, such as corrosion and oxidation resistance, phase stability, nickel-based superalloys are widely used in the critical hot-section components in aerospace and energy generation industries. The success of nickel-based superalloy systems attributes to both the well-tailored microstructures with the assistance of carefully doped alloying elements, and the intently developed manufacturing processes. The microstructure of the modern nickel-based superalloys consists of a two-phase configuration: the intermetallic precipitates (Ni,Co)3(Al,Ti,Ta) known as γ′ phase dispersed into the austenite γ matrix, which is firstly introduced in the 1940s. The recently developed additive manufacturing (AM) techniques, acting as the disruptive manufacturing process, offers a new avenue for producing the nickel-based superalloy components with complicated geometries. However, γ′ strengthened nickel-based superalloys always suffer from the micro-cracking during the AM process, which is barely eliminated by the process optimization. On this basis, the new compositions of γ′ strengthened nickel-based superalloy adapted to the AM process are of great interest and significance. This study sought to design novel γ′ strengthened nickel-based superalloys readily for AM process with limited cracking susceptibility, based on the understanding of the cracking mechanisms. A two-parameter model is developed to predict the additive manufacturability for any given composition of a nickel-based superalloy. One materials index is derived from the comparison of the deformation-resistant capacity between dendritic and interdendritic regions, while another index is derived from the difference of heat resistant capacity of these two spaces. By plotting the additive manufacturability diagram, the superalloys family can be categorized into the easy-to-weld, fairly-weldable, and non-weldable regime with the good agreement of the existed knowledge. To design a novel superalloy, a Cr-Co-Mo-W-Al-Ti-Ta-Nb-Fe-Ni alloy family is proposed containing 921,600 composition recipes in total. Through the examination of additive manufacturability, undesired phase formation propensity, and the precipitation fraction, one composition of superalloy, MAD542, out of the 921,600 candidates is selected. Validation of additive manufacturability of MAD542 is carried out by laser powder bed fusion (LPBF). By optimizing the LPBF process parameters, the crack-free MAD542 part is achieved. In addition, the MAD542 superalloy shows great resistance to the post-processing treatment-induced cracking. During the post-processing treatment, extensive annealing twins are promoted to achieve the recrystallization microstructure, ensuring the rapid reduction of stored energy. After ageing treatment, up to 60-65% volume fraction of γ′ precipitates are developed, indicating the huge potential of γ′ formation. Examined by the high-temperature slow strain rate tensile and constant loading creep testing, the MAD542 superalloy shows superior strength than the LPBF processed and hot isostatic pressed plus heat-treated IN738LC superalloy. While the low ductility of MAD542 is existed, which is expected to be improved by modifying the post-processing treatment scenarios and by the adjusting building direction in the following stages of the Ph.D. research. MAD542 superalloy so far shows both good additive manufacturability and mechanical potentials. Additionally, the results in this study will contribute to a novel paradigm for alloy design and encourage more γ′-strengthened nickel-based superalloys tailored for AM processes in the future.

Download or read book Proceedings of the 12th International Conference on Advanced Materials and Engineering Materials written by Laichang Zhang and published by Springer Nature. This book was released on with total page 798 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Download or read book Superalloys written by Matthew J. Donachie and published by ASM International. This book was released on 2002 with total page 439 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book covers virtually all technical aspects related to the selection, processing, use, and analysis of superalloys. The text of this new second edition has been completely revised and expanded with many new figures and tables added. In developing this new edition, the focus has been on providing comprehensive and practical coverage of superalloys technology. Some highlights include the most complete and up-to-date presentation available on alloy melting. Coverage of alloy selection provides many tips and guidelines that the reader can use in identifying an appropriate alloy for a specific application. The relation of properties and microstructure is covered in more detail than in previous books.

Download or read book Welding Metallurgy and Weldability of Nickel Base Alloys written by John C. Lippold and published by John Wiley & Sons. This book was released on 2011-09-20 with total page 370 pages. Available in PDF, EPUB and Kindle. Book excerpt: The most up-to-date coverage of welding metallurgy aspects and weldability issues associated with Ni-base alloys Welding Metallurgy and Weldability of Nickel-Base Alloys describes the fundamental metallurgical principles that control the microstructure and properties of welded Ni-base alloys. It serves as a practical how-to guide that enables engineers to select the proper alloys, filler metals, heat treatments, and welding conditions to ensure that failures are avoided during fabrication and service. Chapter coverage includes: Alloying additions, phase diagrams, and phase stability Solid-solution strengthened Ni-base alloys Precipitation strengthened Ni-base alloys Oxide dispersion strengthened alloys and nickel aluminides Repair welding of Ni-base alloys Dissimilar welding Weldability testing High-chromium alloys used in nuclear power applications With its excellent balance between the fundamentals and practical problem solving, the book serves as an ideal reference for scientists, engineers, and technicians, as well as a textbook for undergraduate and graduate courses in welding metallurgy.

Download or read book Fundamentals of Laser Powder Bed Fusion of Metals written by Igor Yadroitsev and published by Elsevier. This book was released on 2021-05-23 with total page 678 pages. Available in PDF, EPUB and Kindle. Book excerpt: Laser powder bed fusion of metals is a technology that makes use of a laser beam to selectively melt metal powder layer-by-layer in order to fabricate complex geometries in high performance materials. The technology is currently transforming aerospace and biomedical manufacturing and its adoption is widening into other industries as well, including automotive, energy, and traditional manufacturing. With an increase in design freedom brought to bear by additive manufacturing, new opportunities are emerging for designs not possible previously and in material systems that now provide sufficient performance to be qualified in end-use mission-critical applications. After decades of research and development, laser powder bed fusion is now enabling a new era of digitally driven manufacturing. Fundamentals of Laser Powder Bed Fusion of Metals will provide the fundamental principles in a broad range of topics relating to metal laser powder bed fusion. The target audience includes new users, focusing on graduate and undergraduate students; however, this book can also serve as a reference for experienced users as well, including senior researchers and engineers in industry. The current best practices are discussed in detail, as well as the limitations, challenges, and potential research and commercial opportunities moving forward. - Presents laser powder bed fusion fundamentals, as well as their inherent challenges - Provides an up-to-date summary of this advancing technology and its potential - Provides a comprehensive textbook for universities, as well as a reference for industry - Acts as quick-reference guide

Download or read book The Microstructure of Superalloys written by Madeleine Durand-Charre and published by Routledge. This book was released on 2017-11-22 with total page 139 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presents all the main aspects of the microstructure of nickel-base superalloys, and includes micrographs chosen from among a large range of commercial and academic alloys, from the as-cast product to in-situ components, worn from in-service use. Including more than 100 illustrations, the text explains all the transformation mechanisms involved in the origination (creation) of microstructures during solidification or heat treatments (crystallization paths, segregation, crystal orientation, precipitation, TCP, coarsening and rafting, etc.). It includes up-to-date information and data such as phase diagrams, crystallographic structures, and relationships with functional properties. Nearly 300 references provide a key to further investigation.

Download or read book Superalloys 2024 written by Jonathan Cormier and published by Springer Nature. This book was released on with total page 1121 pages. Available in PDF, EPUB and Kindle. Book excerpt:

Download or read book Superalloys 2020 written by Sammy Tin and published by Springer Nature. This book was released on 2020-08-28 with total page 1098 pages. Available in PDF, EPUB and Kindle. Book excerpt: The 14th International Symposium on Superalloys (Superalloys 2020) highlights technologies for lifecycle improvement of superalloys. In addition to the traditional focus areas of alloy development, processing, mechanical behavior, coatings, and environmental effects, this volume includes contributions from academia, supply chain, and product-user members of the superalloy community that highlight technologies that contribute to improving manufacturability, affordability, life prediction, and performance of superalloys.

Download or read book Superalloys 2012 written by Eric S. Huron and published by John Wiley & Sons. This book was released on 2012-10-02 with total page 952 pages. Available in PDF, EPUB and Kindle. Book excerpt: A superalloy, or high-performance alloy, is an alloy that exhibits excellent mechanical strength at high temperatures. Superalloy development has been driven primarily by the aerospace and power industries. This compilation of papers from the Twelfth International Symposium on Superalloys, held from September 9-13, 2012, offers the most recent technical information on this class of materials.

Download or read book Modern Manufacturing Processes for Aircraft Materials written by Selim Gurgen and published by Elsevier. This book was released on 2023-11-15 with total page 371 pages. Available in PDF, EPUB and Kindle. Book excerpt: Approx.530 pages Provides detailed explanation of modern manufacturing processes used in the aircraft industry Covers additive manufacturing both for polymeric and metallic materials, electrical discharge machining, laser welding, electron-beam welding, and micro-machining Explains manufacturing operations for not only metallic materials but also polymers and composites

Download or read book Additively Manufactured Inconel 718 written by Dunyong Deng and published by Linköping University Electronic Press. This book was released on 2018-01-24 with total page 69 pages. Available in PDF, EPUB and Kindle. Book excerpt: Additive manufacturing (AM), also known as 3D printing, has gained significant interest in aerospace, energy, automotive and medical industries due to its capabilities of manufacturing components that are either prohibitively costly or impossible to manufacture by conventional processes. Among the various additive manufacturing processes for metallic components, electron beam melting (EBM) and selective laser melting (SLM) are two of the most widely used powder bed based processes, and have shown great potential for manufacturing high-end critical components, such as turbine blades and customized medical implants. The futures of the EBM and SLM are doubtlessly promising, but to fully realize their potentials there are still many challenges to overcome. Inconel 718 (IN718) is a nickel-base superalloy and has impressive combination of good mechanical properties and low cost. Though IN718 is being mostly used as a turbine disk material now, the initial introduction of IN718 was to overcome the poor weldability of superalloys in 1960s, since sluggish precipitation of strengthening phases ?’/?’’ enables good resistance to strain-age cracking during welding or post weld heat treatment. Given the similarity between AM and welding processes, IN718 has been widely applied to the metallic AM field to facilitate the understandings of process-microstructure-property relationships. The work presented in this licentiate thesis aims to better understand microstructures and mechanical properties EBM and SLM IN718, which have not been systematically investigated. Microstructures of EBM and SLM IN718 have been characterized with scanning electron microscopy (SEM), transmission electron microscopy (TEM) and correlated with the process conditions. Monotonic mechanical properties (e.g., Vickers microhardness and tensile properties) have also been measured and rationalized with regards to the microstructure evolutions before and after heat treatments. For EBM IN718, the results show the microstructure is not homogeneous but dependant on the location in the components, and the anisotropic mechanical properties are probably attributed to alignment of porosities rather than texture. Post heat treatment can slightly increase the mechanical strength compared to the as-manufactured condition but does not alter the anisotropy. SLM IN718 shows significantly different microstructure and mechanical properties to EBM IN718. The as-manufactured SLM IN718 has very fine dendritic microstructure and Laves phases in the interdendrites, and is “work-hardened” by the residual strains and dislocations present in the material. Mechanical properties are different between horizontally and vertically built samples, and heat treatment can minimize this difference. Results from this licentiate thesis provide the basis for the further research on the cyclic mechanical properties of EBM and SLM IN718, which would be the focus of following phase of the Ph.D. research.

Download or read book TMS 2019 148th Annual Meeting Exhibition Supplemental Proceedings written by The Minerals, Metals & Materials Series and published by Springer. This book was released on 2019-02-27 with total page 1731 pages. Available in PDF, EPUB and Kindle. Book excerpt: This collection features papers presented at the 147th Annual Meeting & Exhibition of The Minerals, Metals & Materials Society.

Download or read book Laser Cladding of Metals written by Pasquale Cavaliere and published by Springer Nature. This book was released on 2020-11-05 with total page 444 pages. Available in PDF, EPUB and Kindle. Book excerpt: Laser cladding is an additive manufacturing technology capable of producing coatings due to the surface fusion of metals. The selected powder is fed into a focused laser beam to be melted and deposited as coating. This allows to apply material in a selected way onto those required sections of complex components. The process main properties are the production of a perfect metallurgically bonded and fully dense coatings; the minimal heat affected zone and low dilution between the substrate and filler material resulting in functional coatings that perform at reduced thickness, so fewer layers are applied; fine, homogeneous microstructure resulting from the rapid solidification rate that promotes wear resistance of carbide coatings; near net-shape weld build-up requires little finishing effort; extended weldability of sensitive materials like carbon-rich steels or nickel-based superalloys that are difficult or even impossible to weld using conventional welding processes; post-weld heat treatment is often eliminated as the small heat affected zone minimizes component stress; excellent process stability and reproducibility because it is numerical controlled welding process. The typical applications are the dimensional restoration; the wear and corrosion protection; additive manufacturing. The wide range of materials that can be deposited and its suitability for treating small areas make laser cladding particularly appropriate to tailor surface properties to local service requirements and it opens up a new perspective for surface engineered materials. The main key aspect to be scientifically and technologically explored are the type of laser; the powders properties; the processing parameters; the consequent microstructural and mechanical properties of the processed material; the capability of fabrication of prototypes to rapid tooling and rapid manufacturing. Distills critical concepts, methods, and applications from leading full-length chapters, along with the authors’s own deep understanding of the material taught, into a concise yet rigorous graduate and advanced undergraduate text; Reinforces concepts covered with detailed solutions to illuminating and challenging industrial applications; Discusses current and future applications of laser cladding in additive manufacturing.

Download or read book Additive Manufacturing written by Juan Pou and published by Elsevier. This book was released on 2021-05-21 with total page 770 pages. Available in PDF, EPUB and Kindle. Book excerpt: Additive Manufacturing explains the background theory, working principles, technical specifications, and latest developments in a wide range of additive manufacturing techniques. Topics addressed include treatments of manufactured parts, surface characterization, and the effects of surface treatments on mechanical behavior. Many different perspectives are covered, including design aspects, technologies, materials and sustainability. Experts in both academia and industry contribute to this comprehensive guide, combining theoretical developments with practical improvements from R&D. This unique guide allows readers to compare the characteristics of different processes, understand how they work, and provide parameters for their effective implementation. This book is part of a four-volume set entitled Handbooks in Advanced Manufacturing. Other titles in the set include Advanced Machining and Finishing, Advanced Welding and Deformation, and Sustainable Manufacturing Processes. - Provides theory, operational parameters, and latest developments in 20 different additive manufacturing processes - Includes contributions from experts in industry and academia with a wide range of disciplinary backgrounds, providing a comprehensive survey of this diverse and influential subject - Includes case studies of innovative additive manufacturing practices from industry

Download or read book Springer Handbook of Additive Manufacturing written by Eujin Pei and published by Springer Nature. This book was released on 2023-11-25 with total page 994 pages. Available in PDF, EPUB and Kindle. Book excerpt: This Handbook is the ultimate definitive guide that covers key fundamentals and advanced applications for Additive Manufacturing. The Handbook has been structured into seven sections, comprising of a thorough Introduction to Additive Manufacturing; Design and Data; Processes; Materials; Post-processing, Testing and Inspection; Education and Training; and Applications and Case Study Examples. The general principles and functional relationships are described in each chapter and supplemented with industry use cases. The aim of this book is to help designers, engineers and manufacturers understand the state-of-the-art developments in the field of Additive Manufacturing. Although this book is primarily aimed at students and educators, it will appeal to researchers and industrial professionals working with technology users, machine or component manufacturers to help them make better decisions in the implementation of Additive Manufacturing and its applications.