Download or read book Microstructural Characterization of Reaction Formed Silicon Carbide Ceramics Materials Characterization written by National Aeronautics and Space Adm Nasa and published by . This book was released on 2018-10-23 with total page 28 pages. Available in PDF, EPUB and Kindle. Book excerpt: Microstructural characterization of two reaction-formed silicon carbide ceramics has been carried out by interference layering, plasma etching, and microscopy. These specimens contained free silicon and niobium disilicide as minor phases with silicon carbide as the major phase. In conventionally prepared samples, the niobium disilicide cannot be distinguished from silicon in optical micrographs. After interference layering, all phases are clearly distinguishable. Back scattered electron (BSE) imaging and energy dispersive spectrometry (EDS) confirmed the results obtained by interference layering. Plasma etching with CF4 plus 4% O2 selectively attacks silicon in these specimens. It is demonstrated that interference layering and plasma etching are very useful techniques in the phase identification and microstructural characterization of multiphase ceramic materials. Singh, M. and Leonhardt, T. A. Glenn Research Center ...
Download or read book Characterization of Ceramics written by Ronald E. Loehman and published by Momentum Press. This book was released on 2010 with total page 316 pages. Available in PDF, EPUB and Kindle. Book excerpt: Ceramics are, in a general definition, materials that consist of man-made, inorganic, non-metallic solid material - either existing in a crystalline state or non-crystalline state (i.e., glasses). Materials characterization techniques are used to ensure the structural and surface integrity of ceramics for their use in a wide variety of applications, from thermal resistance to advanced electronic and optical technologies like fiber optics to structural uses. This book presents those techniques along with views on future trends in ceramics processing and advanced characterization technologies particularly appropriate to ceramics materials. Readers will find more on: Ceramic Materials preparation routes, including powder preparation by solution techniques and gas-phase techniques Formation techniques for ceramic films and coatings, thick films and bulk ceramics A review of ceramic microstructure, reactions, phase behavior, mechanical properties and electronic and magnetic ceramics
Download or read book Mechanical Chemical and Microstructural Characterization of Monazite Coated Silicon Carbide Fibers written by Narottam P. Bansal and published by . This book was released on 2000 with total page 26 pages. Available in PDF, EPUB and Kindle. Book excerpt: Tensile strengths of as-received Hi-Nicalon and Sylramic fibers and those having monazite surface coatings, deposited by atmospheric pressure chemical vapor deposition, were measured at room temperature and the Weibull statistical parameters determined. The average tensile strengths of uncoated Hi-Nicalon and Sylramic fibers were 3.19 +/- 0.73 and 2.78 +/- 0.53 GPa with a Weibull modulus of 5.41 and 5.52, respectively. The monazite-coated Hi-Nicalon and Sylramic fibers showed strength loss of approx. 10 and 15 percent, respectively, compared with the as-received fibers. The elemental compositions of the fibers and the coatings were analyzed using scanning Auger microprobe and energy dispersive X-ray spectroscopy. The LaPO4 coating on Hi-Nicalon fibers was approximately stoichiometric and about 50 nm thick. The coating on the Sylramic fibers extended to a depth of about 100 to 150 nm. The coating may have been stoichiometric LaPO4 in the first 30 to 40 nm of the layer. However, the surface roughness of Sylramic fiber made this profile somewhat difficult to interpret. Microstructural analyses of the fibers and the coatings were done by scanning electron microscopy, transmission electron microscopy, and selected area electron diffraction.
Download or read book Process Development for Silicon Carbide Based Structural Ceramics written by Edward E. Hucke and published by . This book was released on 1982 with total page 61 pages. Available in PDF, EPUB and Kindle. Book excerpt: The objective of this program is to develop a process for making shaped silicon carbide based ceramic materials with reduced microstructural flaw size by in situ reaction of silicon with fine, ultra-uniform pored carbon skeletons that are produced from liquid polymer solutions without particulate additions. Subsidiary objectives are: (1) delineation of the maximum section size producible while maintaining microstructural uniformity; (2) production of microstructures with characteristic features reduced from the current level of approximately 5-10 microns to the level of 1 micron or less; (3) characterization of microstructure, corresponding strength levels, and statistical uniformity; and (4) delineation of dimensional tolerances and surface finish that can be held during processing without finished machining. Very uniform and reproducible carbon skeletons have been produced and modified to provide for easy siliconization without extensive grain coarsening or formation of silicon veins and/or lakes have been achieved from 1 cm thick samples of carbon skeleton with particle size of 3.2 microns and pore size of 1.9 micrometers. The siliconized material has a maximum grain size of
Download or read book Metal Matrix Composities written by Composite Materials Handbook – 17 (CMH-17) and published by SAE International. This book was released on 2013-09-18 with total page 451 pages. Available in PDF, EPUB and Kindle. Book excerpt: The fourth volume of this six-volume compendium includes properties on metal matrix composite material systems for which data meeting the specific requirements of the handbook are available. In addition, it provides selected guidance on other technical topics related to this class of composites, including material selection, material specification, processing, characterization testing, data reduction, design, analysis, quality control, and repair of typical metal matrix composite materials. The Composite Materials Handbook, referred to by industry groups as CMH-17, is a six-volume engineering reference tool that contains over 1,000 records of the latest test data for polymer matrix, metal matrix, ceramic matrix, and structural sandwich composites. CMH-17 provides information and guidance necessary to design and fabricate end items from composite materials. It includes properties of composite materials that meet specific data requirements as well as guidelines for design, analysis, material selection, manufacturing, quality control, and repair. The primary purpose of the handbook is to standardize engineering methodologies related to testing, data reduction, and reporting of property data for current and emerging composite materials. It is used by engineers worldwide in designing and fabricating products made from composite materials.
Download or read book Characterization and Control of Interfaces for High Quality Advanced Materials written by Kevin Ewsuk and published by John Wiley & Sons. This book was released on 2012-04-11 with total page 486 pages. Available in PDF, EPUB and Kindle. Book excerpt: Interface characterization and control are critical in the design and manufacture of high quality advanced materials, particularly, for nanomaterials. This proceedings features papers on interface science and technology that provide a unique and state-of-the art perspective on interface characterization and control. Articles from scientists and engineers from 11 different countries address interface control, high temperature interfaces, nanoparticle design, nanotechnology, suspension control, novel processing, particulate materials, microstructure, and hot gas cleaning. This unique volume will serve as a valuable reference for scientists and engineers interested in interfaces, particulate materials, and nanotechnology. Proceedings of the International Conference on ICCCI 2003, Kurashiki, Japan, 2003; Ceramic Transactions, Volume 146.
Download or read book Ceramic Microstructures 86 written by Joseph A. Pask and published by Springer Science & Business Media. This book was released on 2013-11-11 with total page 980 pages. Available in PDF, EPUB and Kindle. Book excerpt: The Proceedings of the International Materials Symposium on Ceramic Microstructures '86: Role of Interfaces presents a comprehensive coverage of the past decade's advances in ceramic science and technology related to microstructures. The term microstructure is used in the broad sense and is synonymous with char~cter. Character is defined as a complete detailed description of chemical and physical characteristics of a material. This symposium is the third in a series, held every ten years, on ceramic microstructures. The first symposium, in 1966, had as a subtitle "Their Analysis, Significance and Production" and emphasized the need and importance of characterization in order to fully understand the chemical and physical properties of materials. The second Symposium, in 1976, placed emphasis on the exploration of characters most suited and needed for "Energy-Related Applications." By the time of that conference, the sequence of processing--characterization--properties was fully accepted. It was recognized that characterization was the basis of materials science; the objective of processing was to produce a desired character that was considered necessary to realize a given property or behavior. To further emphasize the importance of character, the symposium dealt primarily with the property/character coupling.
Download or read book Ceramic Microstructures written by Antoni P. Tomsia and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 841 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume, titled Proceedings of the International Materials Symposium on Ce ramic Microstructures: Control at the Atomic Level summarizes the progress that has been achieved during the past decade in understanding and controlling microstructures in ceram ics. A particular emphasis of the symposium, and therefore of this volume, is advances in the characterization, understanding, and control of micro structures at the atomic or near-atomic level. This symposium is the fourth in a series of meetings, held every ten years, devoted to ceramic microstructures. The inaugural meeting took place in 1966, and focussed on the analysis, significance, and production of microstructure; the symposium emphasized the need for, and importance of characterization in achieving a more complete understanding of the physical and chemical characteristics of ceramics. A consensus emerged at that meeting on the critical importance of characterization in achieving a more complete understanding of ceramic properties. That point of view became widely accepted in the ensuing decade. The second meeting took place in 1976 at a time of world-wide energy shortages and thus emphasized energy-related applications of ceramics, and more specifically, microstructure-property relationships of those materials. The third meeting, held in 1986, was devoted to the role that interfaces played both during processing, and in influencing the ultimate properties of single and polyphase ceramics, and ceramic-metal systems.
Download or read book Silicon Carbide Ceramics written by S. Somiya and published by Springer Science & Business Media. This book was released on 1991-08-31 with total page 328 pages. Available in PDF, EPUB and Kindle. Book excerpt: Silicon carbides have major industrial uses as high temperature structural ceramic materials. These two volumes are translated from the Japanese and provide a comprehensive account of the seminal work going on in Japan.
Download or read book Characterization of Ceramics and Intermetallics Fabricated by Self propagating High temperature Synthesis written by and published by . This book was released on 1989 with total page 24 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book 21st Annual Conference on Composites Advanced Ceramics Materials and Structures A Volume 18 Issue 3 written by J. P. Singh and published by John Wiley & Sons. This book was released on 2009-09-28 with total page 812 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume is part of the Ceramic Engineering and Science Proceeding (CESP) series. This series contains a collection of papers dealing with issues in both traditional ceramics (i.e., glass, whitewares, refractories, and porcelain enamel) and advanced ceramics. Topics covered in the area of advanced ceramic include bioceramics, nanomaterials, composites, solid oxide fuel cells, mechanical properties and structural design, advanced ceramic coatings, ceramic armor, porous ceramics, and more.
Download or read book 25th Annual Conference on Composites Advanced Ceramics Materials and Structures A Volume 22 Issue 3 written by Mrityunjay Singh and published by John Wiley & Sons. This book was released on 2009-09-28 with total page 746 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume is part of the Ceramic Engineering and Science Proceeding (CESP) series. This series contains a collection of papers dealing with issues in both traditional ceramics (i.e., glass, whitewares, refractories, and porcelain enamel) and advanced ceramics. Topics covered in the area of advanced ceramic include bioceramics, nanomaterials, composites, solid oxide fuel cells, mechanical properties and structural design, advanced ceramic coatings, ceramic armor, porous ceramics, and more.
Download or read book Ceramic Microstructures written by W.E. Lee and published by Springer Science & Business Media. This book was released on 1994-10-31 with total page 618 pages. Available in PDF, EPUB and Kindle. Book excerpt: This text deals with the effect of processing on the microstructure and properties of advanced structural and electroceramic materials. It fulfils the need for a well illustrated book explaining the relation between microstructure and properties in structural ceramics, featuring high quality micrographs and characterization techniques.
Download or read book Mechanical Properties and Performance of Engineering Ceramics and Composites VI Volume 32 Issue 2 written by Dileep Singh and published by John Wiley & Sons. This book was released on 2011-11-11 with total page 322 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book is a collection of papers from The American Ceramic Society's 35th International Conference on Advanced Ceramics and Composites, held in Daytona Beach, Florida, January 23-28, 2011. This issue includes papers presented in the Mechanical Behavior and Performance of Ceramics & Composites Symposium on topics such as processing-microstructure properties correlations; fracture mechanics, modeling and testing; tribological properties; applications; and processing.
Download or read book Silicon Carbide Ceramics 1 written by S. Somiya and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 300 pages. Available in PDF, EPUB and Kindle. Book excerpt: Discovered by Edward G. Acheson about 1890, silicon carbide is one of the oldest materials and also a new material. It occurs naturally in meteorites, but in very small amounts and is not in a useable state as an industrial material. For industrial require ments, large amounts of silicon carbide must be synthesized by solid state reactions at high temperatures. Silicon carbide has been used for grinding and as an abrasive material since its discovery. During World War II, silicon carbide was used as a heating element; however, it was difficult to obtain high density sintered silicon carbide bodies. In 1974, S. Prochazka reported that the addition of small amounts of boron compounds and carbide were effective in the sintering process to obtain high density. It was then possible to produce high density sintered bodies by pressureless sintering methods in ordinary atmosphere. Since this development, silicon carbide has received great attention as one of the high temperature structural ceramic materials. Since the 1970s, many research papers have appeared which report studies of silicon carbide and silicon nitride for structural ceramics.
Download or read book Structural and Microstructural Characterization of III Nitrides on 6H SiC 0001 Substrates written by Edward Alfred Preble and published by . This book was released on 2001 with total page 136 pages. Available in PDF, EPUB and Kindle. Book excerpt: Keywords: silicon carbide, gallium nitride, contacts, pendeo, hydrogen etching, x-ray, transmission electron microscopy, GaN, SiC, AlN.
Download or read book Proceedings of the 42nd International Conference on Advanced Ceramics and Composites Ceramic Engineering and Science Proceedings written by Jonathan Salem and published by John Wiley & Sons. This book was released on 2018-11-27 with total page 268 pages. Available in PDF, EPUB and Kindle. Book excerpt: Proceeding of the 42nd International Conference on Advanced Ceramics and Composites, Ceramic Engineering and Science Proceedings Volume 39, Issue 2, 2018 Jonathan Salem, Dietmar Koch, Peter Mechnich, Mihails Kusnezoff, Narottam Bansal, Jerry LaSalvia, Palani Balaya, Zhengyi Fu, and Tatsuki Ohji, Editors Valerie Wiesner and Manabu Fukushima, Volume Editors This proceedings contains a collection of 25 papers from The American Ceramic Society’s 41st International Conference on Advanced Ceramics and Composites, held in Daytona Beach, Florida, January 21-26, 2018. This issue includes papers presented in the following symposia: • Symposium 1: Mechanical Behavior and Performance of Ceramics and Composites • Symposium 2: Advanced Ceramic Coatings for Structural, Environmental, and Functional Applications • Symposium 3: 15th International Symposium on Solid Oxide Fuel Cells (SOFC) • Symposium 4: Armor Ceramics: Challenges and New Developments • Symposium 6: Advanced Materials and Technologies for Direct Thermal Energy Conversion and Rechargeable Energy Storage • Symposium 8: 12th International Symposium on Advanced Processing & Manufacturing
