Download or read book Introduction to Thermal Analysis written by M.E. Brown and published by Springer Science & Business Media. This book was released on 2006-01-10 with total page 268 pages. Available in PDF, EPUB and Kindle. Book excerpt: to Thermal Analysis Techniques and Applications Edited by Michael E. Brown Chemistry Department, Rhodes University, Grahamstown, South Africa KLUWER ACADEMIC PUBLISHERS NEW YORK, BOSTON, DORDRECHT, LONDON, MOSCOW eBook ISBN: 0-306-48404-8 Print ISBN: 1-4020-0472-9 ©2004 Kluwer Academic Publishers New York, Boston, Dordrecht, London, Moscow Print ©2001 Kluwer Academic Publishers Dordrecht All rights reserved No part of this eBook may be reproduced or transmitted in any form or by any means, electronic, mechanical, recording, or otherwise, without written consent from the Publisher Created in the United States of America Visit Kluwer Online at: http://kluweronline. com and Kluwer's eBookstore at: http://ebooks. kluweronline. com CONTENTS Preface to the First Edition, Chapman & Hall, London, 1988 ix About the First Edition of this Book x Preface to the Second Edition xi 1. INTRODUCTION 1. 1 Definition and History 1 1. 2 Thermal Analysis Instruments 4 References 11 2. THERMAL EVENTS 2. 1 Introduction 13 2. 2 The Solid State 13 2. 3 Reactions of Solids 14 2. 4 Decomposition of Solids 15 2. 5 Reaction with the Surrounding Atmosphere 16 2. 6 Solid-Solid Interactions 16 References 17 3. THERMOGRAVIMETRY (TG) Introduction 3. 1 19 3. 2 The Balance 19 3. 3 Heating the Sample 21 3. 4 The Atmosphere 24 3. 5 The Sample 26 3. 6 Temperature Measurement 26 3. 7 Temperature Control 28 Sample Controlled Thermal Analysis (SCTA) 29 3. 8 3. 9 Calibration 36 3. 10 Presentation of TG Data 37 3.
Download or read book Thermal Analysis written by El-Zeiny Ebeid and published by Elsevier. This book was released on 2021-06-23 with total page 324 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal Analysis: From Introductory Fundamentals to Advanced Applications presents an easy-to-understand introduction to Thermal Analysis (TA) principles alongside in-depth coverage of the wide variety of techniques currently in use across several industries. It covers differential scanning calorimetry (DSC), temperature modulated DSC (TMDSC), differential thermal analysis (DTA), thermogravimetry (TG) or thermogravimetric analysis (TGA), thermomechanical analysis (TMA), differential photo-calorimetry (DPC), dynamic mechanical analysis (DMA), thermodilatometry (TD), dielectric thermal analysis (DEA), thermally-stimulated current (TSC), emanation thermal analysis (ETA), thermoluminescence (TL), fast scanning calorimetry (FSC), and microcalorimetry. Chapters define the various TA techniques, report the Temperature-Modulated DSC (TMDSC) method and its applications, especially its use for studying the thermodynamic properties of polymers and pharmaceuticals, focus on the potential of TA in materials science with applications in chemistry and engineering, demonstrate, in detail, the various applications of TA in food, electronic industries, solid-state reactions, chemistry of polymers and large directing agents, kinetic studies, demonstrate the crystal structure and phase changes occurring upon heating by TA, and the potential of TA in recycling and waste management. Gives a solid introduction to the scientific principles of TA for those who are new to these techniques or need a deeper understanding Illustrates concepts with more than 100 schematic and analysis curves, several flow charts, process diagrams and photographs Contains chapters that cover the user of TA in materials science and crystal structures
Download or read book Principles and Applications of Thermal Analysis written by Paul Gabbott and published by John Wiley & Sons. This book was released on 2008-04-30 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal Analysis techniques are used in a wide range of disciplines, from pharmacy and foods to polymer science, materials and glasses; in fact any field where changes in sample behaviour are observed under controlled heating or controlled cooling conditions. The wide range of measurements possible provide fundamental information on the material properties of the system under test, so thermal analysis has found increasing use both in basic characterisation of materials and in a wide range of applications in research, development and quality control in industry and academia. Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides the reader with sound practical instruction on how to use the techniques and gives an up to date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including the new approach of Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then developing the discussion to encompass industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues and relating the measurements to the physical behaviour of the materials under test, the book will also serve as an important reference for experienced analysts.
Download or read book Thermal Analysis in Practice written by Matthias Wagner and published by . This book was released on 2017-12 with total page 352 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal analysis comprises a group of techniques used to determine the physical or chemical properties of a substance as it is heated, cooled, or held at constant temperature. It is particularly important for polymer characterization, but also has major application in analysis of pharmaceuticals and foodstuffs. This comprehensive handbook presents practical and theoretical aspects of the key techniques of DSC, TGA, TMA, DMA, and related methods. It also includes separate chapters on the glass transition, polymers, polymorphism, purity determination, and method development. The large number of practical examples included should inspire readers toward new ideas for applications in their own fields of work. The chapters are independent of one another and can be read individually in any desired order. Based on years of experience in thermal analysis of users, application specialists, consultants, and course instructors, this book provides practical help to newcomers, inexperienced users, and anyone else interested in the practical aspects of thermal analysis.
Download or read book Thermal Methods of Analysis written by P.J. Haines and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 297 pages. Available in PDF, EPUB and Kindle. Book excerpt: The wide range of applications of thermal methods of analysis in measuring physical properties, studying chemical reactions and determining the thermal behaviour of samples is of interest to academics and to industry. These applications prompted the writing of this book, in the hope that the descriptions, explanations and examples given would be of help to the analyst and would stimulate the investigation of other thermal techniques. Thermal studies are a fascinating means of examining the samples and the problems brought to us by colleagues, students and clients. If time allows, watching crystals change on a hot-stage microscope, or measuring the properties and changes on a DSC or TG or any thermal instrument can be a rewarding activity, besides providing valuable analytical information. This book started from a series of lectures delivered at Kingston University and at meetings of the Thermal Methods Group of the United Kingdom. The collaboration and information supplied to all the contribu tors by colleagues and instrument manufacturers is most gratefully ack nowledged, as are the valuable contributions made at meetings of the International Confederation for Thermal Analysis and Calorimetry (ICT AC) and at the European Symposia on Thermal Analysis and Calorimetry (ESTAC).
Download or read book Introduction to Thermal Analysis written by Michael E. Brown and published by Springer. This book was released on 1988-06-30 with total page 230 pages. Available in PDF, EPUB and Kindle. Book excerpt: Basic principles and practical requirements of the main techniques are discussed. The author also introduces less common techniques and gives examples of applications. Special attention is given to the use of computers in thermal analysis. Annotation copyright Book News, Inc. Portland, Or.
Download or read book Thermal Analysis written by Bernhard Wunderlich and published by Elsevier. This book was released on 2012-12-02 with total page 465 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal Analysis deals with the theories of thermal analysis (thermodynamics, irreversible thermodynamics, and kinetics) as well as instrumentation and techniques (thermometry, differential thermal analysis, calorimetry, thermomechanical analysis and dilatometry, and thermogravimetry). Applications of thermal analysis are also described. This book consists of seven chapters and begins with a brief outline of the history and meaning of heat and temperature before listing the techniques of thermal analysis. The reader is then introduced to the basis of thermal analysis, paying particular attention to the macroscopic theories of matter, namely, equilibrium thermodynamics, irreversible thermodynamics, and kinetics. The next chapter discusses thermometry, focusing on the international temperature scale and the techniques of measuring temperature. Examples of heating and cooling curves are linked to the discussion of transitions. The groundwork for a detailed understanding of transition temperature is given. The chapters that follow explore the principles of differential thermal analysis, calorimetry, thermomechanical analysis and dilatometry, and thermogravimetry. This book is intended for the senior undergraduate or beginning graduate student, as well as for the researcher and teacher interested in thermal analysis.
Download or read book Thermal Analysis of Polymers written by Joseph D. Menczel and published by John Wiley & Sons. This book was released on 2014-07-09 with total page 607 pages. Available in PDF, EPUB and Kindle. Book excerpt: Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background. Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation. Written by experts in the various areas of thermal analysis Relevant and detailed experiments and examples follow each chapter.
Download or read book Thermal Analysis of Materials written by Robert Speyer and published by CRC Press. This book was released on 1993-09-16 with total page 304 pages. Available in PDF, EPUB and Kindle. Book excerpt: Discussing the design and optimum use of thermal analysis instrumentation for materials' property measurement, this work details how the instruments work, what they measure, potential pitfalls and the fitting of experimental results to theoretical models. It presents a tutorial on writing computer programs for data manipulation, advanced thermoanalytical methods and case studies.
Download or read book Handbook of Thermal Analysis written by T. Hatakeyama and published by John Wiley & Sons. This book was released on 1998 with total page 480 pages. Available in PDF, EPUB and Kindle. Book excerpt: Handbook of Thermal Analysis Edited by T. Hatakeyama National Institute of Materials and Chemical Research, Ibaraki, Japan Zhenhai Liu Changchun Institute of Applied Chemistry, China This 425-page reference book covers a comprehensive description of the principles of thermal analysis (TA) instruments, operating conditions, and the nature of the experimental data. Presented in a compact and well-arranged style with a large number of figures and illustrations, this work is divided into two parts. Part I is designed to acquaint and orient newcomers with TA by providing a comprehensive introduction to the basic principles of instrument operation, with advice on sample preparation and optimization of operating conditions, and a guide to interpreting results. The text deals primarily with techniques such as differential scanning calorimetry (DSC), differential thermal analysis (DTA), and thermogravimetry (TG). Part II illustrates 500 TA curves covering metals, inorganic and organic minerals, polymers, construction materials, pharmaceuticals, explosives, etc. The appendices include a glossary of TA terms, a survey of reference materials, the current table of TA standards, and a TA database. This book is aimed at advanced users and specialists who utilize TA methods for practical purposes, especially in research laboratories both academic and industrial. With an emphasis on practical instruction, industrial research staff, undergraduates and postgraduate students in the relevant fields will find this work a useful introduction to principle TA techniques.
Download or read book Thermal Analysis written by Wesley William Wendlandt and published by Wiley-Interscience. This book was released on 1986-03-10 with total page 840 pages. Available in PDF, EPUB and Kindle. Book excerpt: Provides a comprehensive introduction to thermal analysis and its usefulness in every area of science from archeology to zoology. Covers many new applications of techniques in TG, DTA, DSC, EGD/EGA, and others. Describes instruments available for each technique, including microcomputers. Includes rewritten chapters on EGD/EGA, miscellaneous techniques, and the determination of purity by DSC.
Download or read book Handbook of Thermal Analysis of Construction Materials written by V.S. Ramachandran and published by William Andrew. This book was released on 2002-10-28 with total page 703 pages. Available in PDF, EPUB and Kindle. Book excerpt: This comprehensive book containing essential information on the applicability of thermal analysis techniques to evaluate inorganic and organic materials in construction technology should serve as a useful reference for the scientist, engineer, construction technologist, architect, manufacturer, and user of construction materials, standard-writing bodies, and analytical chemists. The material scientists at the National Research Council of Canada have established one of the best thermal analysis laboratories in the world. Various types of thermal analysis techniques have been applied successfully to the investigation of inorganic and organic construction materials. These studies have provided important information on the characterization of raw as well as finished materials, quality control, quantitative estimation, interrelationships between physical, chemical, mechanical, and durability characteristics. Information on the application of thermal analysis to construction materials is dispersed in literature and hence the IRC scientists embarked on producing a handbook, the first of its kind, incorporating the latest knowledge available in this field of activity. Almost all important construction materials have been included.
Download or read book Thermal Methods of Analysis written by Wesley William Wendlandt and published by Wiley-Interscience. This book was released on 1974 with total page 536 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Principles of Thermal Analysis and Calorimetry written by Simon Gaisford and published by Royal Society of Chemistry. This book was released on 2019-03-15 with total page 280 pages. Available in PDF, EPUB and Kindle. Book excerpt: The use of thermal and calorimetric methods has shown rapid growth over the past few decades, in an increasingly wide range of applications. The original text was published in 2001; since then there have been significant advances in various analytical techniques and their applications. This second edition supplies an up to date, concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis. Written by experts in their field, brief accounts of the basic theory are reinforced with detailed technical advances and contemporary developments. Where appropriate, applications are used to highlight particular operating principles or methods of interpretation. As an important source of information for many levels of readership in a variety of areas, this book will be an aid for students and lecturers through to industrial and laboratory staff and consultants.
Download or read book Introduction to Thermal and Fluid Engineering written by Allan D. Kraus and published by CRC Press. This book was released on 2011-09-06 with total page 972 pages. Available in PDF, EPUB and Kindle. Book excerpt: Introduction to Thermal and Fluid Engineering combines coverage of basic thermodynamics, fluid mechanics, and heat transfer for a one- or two-term course for a variety of engineering majors. The book covers fundamental concepts, definitions, and models in the context of engineering examples and case studies. It carefully explains the methods used t
Download or read book Thermal Analysis with SolidWorks Simulation 2013 written by Paul M. Kurowski and published by SDC Publications. This book was released on 2013 with total page 201 pages. Available in PDF, EPUB and Kindle. Book excerpt: Thermal Analysis with SolidWorks Simulation 2013 goes beyond the standard software manual. It concurrently introduces the reader to thermal analysis and its implementation in SolidWorks Simulation using hands-on exercises. A number of projects are presented to illustrate thermal analysis and related topics. Each chapter is designed to build on the skills and understanding gained from previous exercises. Thermal Analysis with SolidWorks Simulation 2013 is designed for users who are already familiar with basics of Finite Element Analysis (FEA) using SolidWorks Simulation or who have completed the book Engineering Analysis with SolidWorks Simulation 2013. Thermal Analysis with SolidWorks Simulation 2013 builds on these topics in the area of thermal analysis. Some understanding of FEA and SolidWorks Simulation is assumed.
Download or read book Introduction to Thermal Systems Engineering written by Michael J. Moran and published by John Wiley & Sons. This book was released on 2002-09-17 with total page 576 pages. Available in PDF, EPUB and Kindle. Book excerpt: This survey of thermal systems engineering combines coverage of thermodynamics, fluid flow, and heat transfer in one volume. Developed by leading educators in the field, this book sets the standard for those interested in the thermal-fluids market. Drawing on the best of what works from market leading texts in thermodynamics (Moran), fluids (Munson) and heat transfer (Incropera), this book introduces thermal engineering using a systems focus, introduces structured problem-solving techniques, and provides applications of interest to all engineers.
