Download or read book Hydrodynamics of High Pressure and High Temperature Slurry Bubble Columns written by Xukun Luo and published by . This book was released on 1997 with total page 5 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Novel Techniques for Slurry Bubble Column Hydrodynamics Second Semiannual Report 1996 written by and published by . This book was released on 1997 with total page 16 pages. Available in PDF, EPUB and Kindle. Book excerpt: The overall objectives of this cooperative University (Washington University and Ohio State University) - Industry (Exxon Research and Engineering) research are to provide experimental tools for measurement of important fluid dynamic quantities (at high pressure and temperature) and to verify phenomenologically or fundamentally based hydrodynamic models for scale-up and operation of slurry bubble columns.
Download or read book Hydrodynamics and Mass Transfer in Downflow Slurry Bubble Columns written by Subrata Kumar Majumder and published by CRC Press. This book was released on 2019-01-02 with total page 168 pages. Available in PDF, EPUB and Kindle. Book excerpt: Slurry bubble column reactors are intensively used as a multiphase reactor in the chemical, biochemical, and petrochemical industries for carrying out reactions and mass transfer operations in which a gas, made up of one or several reactive components, comes into contact or reacts with a liquid. This volume describes the hydrodynamics of three-phase gas-liquid-solid flow in a downflow slurry bubble column. The efficiency of the downflow gas interacting system is characterized by the self-entrainment of secondary gas. The book covers the gas entrainment phenomena, gas holdup characteristics, pressure drop, gasliquid mixing characteristics, bubble size distribution, interfacial phenomena, and the mass transfer phenomena in the downflow slurry system. This volume will be useful in chemical and biochemical industries and in industrial research and development sectors, as well as in advanced education courses in this area. The book will be helpful for further understanding the multiphase behavior in gas interacting multiphase systems for research and development. The hydrodynamic and mass transfer characteristics discussed will be useful in the design and installation of the modified slurry bubble column in industry for specific applications.
Download or read book Hydrodynamics and Mass Transfer in Bubble Columns written by Onkar N. Manjrekar and published by . This book was released on 2016 with total page 101 pages. Available in PDF, EPUB and Kindle. Book excerpt: Bubble columns and slurry bubble columns are multiphase reactors used for a wide range of applications in the biochemical, chemical, petrochemical, and metallurgical industries. In spite of their widespread usage, the scale-up of bubble columns remains an ongoing challenge. Various scale-up approaches, based on concepts ranging from ideal mixing to complex 3-D multiphase CFD models, have been used for assessing the effect of column size and gas and liquid flow rates on column hydrodynamics and reactor performance. Among these approaches, phenomenological models based on either single-class or multi-class bubbles that were validated on cold flow systems have been successful in predicting the residence time distributions of gas and liquid in pilot-scale bubble columns (Chen et al., 2004) (Gupta, 2002). However, such models are not entirely predictive, since they are validated using columns having the same size as hot operating units. To provide better predictive capability, we need prior knowledge of local hold-up, transport coefficients, and bubble dynamics. This dissertation provides an improved understanding of the key design parameters (gas hold-up, volumetric mass transfer coefficients, gas-liquid interfacial area, and their spatial distribution) for predictive scale-up of bubble columns. In this work, a 4-point optical probe is used to estimate local gas hold-up and bubble dynamics (specific interfacial area, frequency, bubble velocity, and bubble chord-lengths) and their radial profiles in a cold-flow slurry bubble column and a bubble column photo-bioreactor. Along with local bubble dynamics, the effect of superficial gas velocity on volumetric mass transport coefficients in several sizes of bubble columns, with and without internals, and in slurry bubble columns and photo-bioreactors are studied. Key findings: In the bubbly flow regime, bubble dynamics in photo-bioreactors with suspended algae were dominated by the physicochemical properties of the liquid, as distinguished from the churn-turbulent flow regime in the slurry bubble columns, where bubble dynamics were mainly affected by turbulent intensities. In the bubbly-flow regime, volumetric mass transfer coefficients increased with an increase in superficial gas velocity. However, in the churn-turbulent flow regime, they approached a constant value with an increase in the superficial gas velocity. A new methodology was proposed to identify the flow regime from optical probe signals based on the support vector machine algorithm, which can uniquely classify flow regimes for various systems on a single flow regime map. A new model for the liquid phase mixing, that with a proper choice of the mass transfer coefficients enables a good match of the predicted and measured tracer response is described. This model provides a better prediction of volumetric mass transfer coefficients than the currently used well mixed model for the liquid phase (CSTR). The dissertation improves the fundamental understanding of the connection between bubble dynamics and mass transfer. Using the 4-point optical probe as a tool, it demonstrates a connection between bubble dynamics and volumetric mass transfer coefficients. Present work addresses the need of industries to have a method that can be used as an online process control tool to identify flow regime, this method has been tested at cold flow conditions and needs to be implemented at hot flow conditions. The parameters (radial distributions of gas hold-up, bubble velocities, and volumetric mass transfer coefficient) that are evaluated in the present work can be used to validate phenomenological models and CFD results at cold flow conditions, which can later be combined with process chemistry to accomplish scale-up (Chen et al., 2004). The open literature on multiphase reactors is mainly limited to cold flow condition, and techniques such as the optical probe need to be extended to hot flow conditions. The optical probe described here can withstand high temperature and pressure, but for hot flow conditions it requires a better binding agent to hold the probe tips together, one that will not dissolve in industrial solvents.
Download or read book Novel Techniques for Slurry Bubble Column Hydrodynamics written by and published by . This book was released on 1999 with total page 121 pages. Available in PDF, EPUB and Kindle. Book excerpt: The objective of this cooperative research effort between Washington University, Ohio State University and Exxon Research Engineering Company was to improve the knowledge base for scale-up and operation of slurry bubble column reactors for syngas conversion and other coal conversion processes by increased reliance on experimentally verified hydrodynamic models. During the first year (July 1, 1995--June 30, 1996) of this three year program novel experimental tools (computer aided radioactive particle tracking (CARPT), particle image velocimetry (PIV), heat probe, optical fiber probe and gamma ray tomography) were developed and tuned for measurement of pertinent hydrodynamic quantities, such as velocity field, holdup distribution, heat transfer and bubble size. The accomplishments were delineated in the First Technical Annual Report. The second year (July, 1996--June 30, 1997) was spent on further development and tuning of the novel experimental tools (e.g., development of Monte Carlo calibration for CARPT, optical probe development), building up the hydrodynamic data base using these tools and comparison of the two techniques (PIV and CARPT) for determination of liquid velocities. A phenomenological model for gas and liquid backmixing was also developed. All accomplishments were summarized in the Second Annual Technical Report. During the third and final year of the program (July 1, 1997--June 30, 1998) and during the nine months no cost extension, the high pressure facility was completed and a set of data was taken at high pressure conditions. Both PIV, CT and CARPT were used. More fundamental hydrodynamic modeling was also undertaken and model predictions were compared to data. The accomplishments for this period are summarized in this report.
Download or read book Population Balances written by Doraiswami Ramkrishna and published by Elsevier. This book was released on 2000-08-08 with total page 373 pages. Available in PDF, EPUB and Kindle. Book excerpt: Engineers encounter particles in a variety of systems. The particles are either naturally present or engineered into these systems. In either case these particles often significantly affect the behavior of such systems. This book provides a framework for analyzing these dispersed phase systems and describes how to synthesize the behavior of the population particles and their environment from the behavior of single particles in their local environments. Population balances are of key relevance to a very diverse group of scientists, including astrophysicists, high-energy physicists, geophysicists, colloid chemists, biophysicists, materials scientists, chemical engineers, and meteorologists. Chemical engineers have put population balances to most use, with applications in the areas of crystallization; gas-liquid, liquid-liquid, and solid-liquid dispersions; liquid membrane systems; fluidized bed reactors; aerosol reactors; and microbial cultures. Ramkrishna provides a clear and general treatment of population balances with emphasis on their wide range of applicability. New insight into population balance models incorporating random particle growth, dynamic morphological structure, and complex multivariate formulations with a clear exposition of their mathematical derivation is presented. Population Balances provides the only available treatment of the solution of inverse problems essential for identification of population balance models for breakage and aggregation processes, particle nucleation, growth processes, and more. This book is especially useful for process engineers interested in the simulation and control of particulate systems. Additionally, comprehensive treatment of the stochastic formulation of small systems provides for the modeling of stochastic systems with promising new areas of applications such as the design of sterilization systems and radiation treatment of cancerous tumors. - A clear and general treatment of population balances with emphasis on their wide range of applicability. Thus all processes involving solid-fluid and liquid-liquid dispersions, biological populations, etc. are encompassed - Provides new insight into population balance models incorporating random particle growth, dynamic morphological structure, and complex multivariate formulations with a clear exposition of their mathematical derivation - Presents a wide range of solution techniques, Monte Carlo simulation methods with a lucid exposition of their origin and scope for enhancing computational efficiency - An account of self-similar solutions of population balance equations and their significance to the treatment of data on particulate systems - The only available treatment of the solution of inverse problems essential for identification of population balance models for breakage and aggregation processes, particle nucleation and growth processes and so on - A comprehensive treatment of the stochastic formulation of small systems with several new applications
Download or read book Hydrodynamics and Transport Processes of Inverse Bubbly Flow written by Subrata Kumar Majumder and published by Elsevier. This book was released on 2016-03-31 with total page 464 pages. Available in PDF, EPUB and Kindle. Book excerpt: Hydrodynamics and Transport Processes of Inverse Bubbly Flow provides the science and fundamentals behind hydrodynamic characteristics, including flow regimes, gas entrainment, pressure drop, holdup and mixing characteristics, bubble size distribution, and the interfacial area of inverse bubble flow regimes. Special attention is given to mass and heat transfer. This book is an indispensable reference for researchers in academia and industry working in chemical and biochemical engineering. Hydrodynamics and Transport Processes of Inverse Bubbly Flow helps facilitate a better understanding of the phenomena of multiphase flow systems as used in chemical and biochemical industries. - A first book in the market dedicated to the hydrodynamics of inverse bubbly flows - Includes fundamentals of conventional and inverse bubble columns for different hydrodynamic parameters - Includes recommendations for future applications of bubble flows
Download or read book Fluid Dynamics of High Temperature Bubble and Slurry Bubble Columns written by Julie Chabot and published by . This book was released on 1993 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Hydrodynamics and Mass Transfer Studies in High Pressure Gas liquid and Gas liquid solid Fluidization written by Wai Man R. Lau and published by . This book was released on 2003 with total page pages. Available in PDF, EPUB and Kindle. Book excerpt: Abstract: Slurry bubble columns and gas-solid fluidized bed reactors are some of the most commonly used industrial processes. Considerable interests have been recognized in the field of physical, chemical, petrochemical, electrochemical, and biochemical operations (Fan, 1989). In these reactor systems, large axial dispersion of phases and high flow patterns can be achieved by the excellent macromixing characteristics. It also provides excellent heat and mass transfer without the aid of external mechanisms and relatively easy operation. Despite the advantages of operations, the transport behavior in these systems is very complex and a comprehensive knowledge of the hydrodynamics, heat and mass transfer and mixing are required for successful application of these systems. Some aspects of the fundamental characteristics of evaporative liquid jets in gas-liquid-solid flows are studied and some pertinent literature is reviewed. It is found that the injection of an evaporative liquid jet decreases the minimum fluidization velocity at a high pressure due to the additional gas flow generated from liquid evaporation. Fluidizing gas velocities have no significant effect on the jet penetration length in a dense phase fluidized bed while it reduces the radial dispersed distance of the evaporative liquid. The tomographic images of liquid nitrogen injection in a dense phase fluidized bed indicate a distribution of reduced bubble sizes compared to a dry bed. The hydrodynamics, gas-liquid mass transfer properties and liquid entrainment phenomena in a high pressure and high temperature bubble column is investigated. Effects of pressure on hydrodynamics and mass transfer properties are mainly through the change in gas and liquid physical properties, which in turn changes the bubble dynamics that govern the transport phenomena. Experimental results show that liquid velocities have a direct influence on kl while other factors have a dominant effect on the interfacial area over kl. Liquid entrainment in bubble columns is controlled by the droplet formation during bubble bursting at interface. Effect of pressure on liquid entrainment is to due to the higher drag force exerted on the liquid droplet with higher gas density and the formation of smaller droplet by the smaller bubbles at high pressure.
Download or read book Experimental Investigation of the Bubble Column Hydrodynamics written by Booncheng Ong and published by . This book was released on 2003 with total page 590 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Hydrodynamics Mixing and Mass Transfer in Bubble Columns with Internals written by Mohamed Hamed and published by . This book was released on 2012 with total page 123 pages. Available in PDF, EPUB and Kindle. Book excerpt: Bubble columns and slurry bubble columns are considered reactors of choice for a wide range of applications in the chemical, biochemical, and petrochemical industries. Most of the chemical applications of bubble columns include exothermic processes and hence they require some means of heat removal to maintain a steady process. The most practical means for heat removal in these reactors is the utilization of vertical cooling internals since they provide high heat transfer area per reactor volume. However, the effects of these internals on the reactor performance are poorly understood in the open literature. This causes the design of the internals to be based on empirical rules not on the applications of fundamentals. The main objective of this study is to enhance the understanding of the effects of vertical cooling internals on the gas hydrodynamics, gas mixing, and mass transfer. In addition, this study attempts to develop and validate models that can simulate the radial gas velocity profile and axial gas mixing in the presence and absence of internals. Finally, this work aims to validate all the observed experimental results and models in larger columns with and without internals to have a better understanding of the scale-up effects in the presence of internals. This is accomplished by carrying out experiments in a lab-scale 8-inch bubble column and a pilot-scale 18-inch bubble column in the absence and presence of internals. The studied % occluded area by internals (~ 25%) is chosen to match the % occluded area used in the Fischer-Tropsch synthesis. The radial gas velocity profiles are measured using the 4-point optical probe and are used to validate the 1-D gas velocity model developed by Gupta (2002). Gar tracer techniques are used to study the effect of internals on the overall axial gas mixing and mass transfer. A 2-D model, that considers the radial variations of the gas velocity and gas holdup, is developed and used to analyze the tracer data allowing the estimation of the turbulent diffusivities of the gas phase. The 2-D model along with the axial dispersion coefficient model developed by Degaleesan and Dudukovic (1998) are used to determine the contribution of different mixing mechanisms to the overall axial gas mixing. The effect of internals and column diameter on the gas velocity profile, gas mixing, and mass transfer is assessed. The presence of internals causes: The effect of internals and column diameter on the gas velocity profile, gas mixing, and mass transfer is assessed. The presence of internals causes: An increase in the center-line gas velocity. A significant decrease in axial gas mixing. A decrease in the gas-liquid mass transfer coefficient. The increase in column diameter causes: Enhancement of the gas circulation. An increase in axial gas mixing. The model developed by Gupta (2002) to predict radial gas velocity profiles is validated at different operating conditions in the presence and absence of internals. A 2-D convection-diffusion model is developed and proven useful in interpreting gas tracer data and simulating the overall axial gas mixing in the presence and absence of internals.
Download or read book Hydrodynamics and Gas liquid Mass Transfer Coefficient in a Slurry Bubble Column with High Solid Content written by A Yasunishi and published by . This book was released on 1988 with total page 19 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Hydrodynamics and Heat Transfer of Baffled and Unbaffled Slurry Bubble Columns written by S. C. Saxena and published by . This book was released on 1994 with total page 208 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Bubble Column Reactions written by Wolf-Dieter Deckwer and published by John Wiley & Sons. This book was released on 1992-04-08 with total page 564 pages. Available in PDF, EPUB and Kindle. Book excerpt: This technology, though used for many years, has shown great vitality recently and is still in a state of flux. Provides an account of developments up to the present and also an orderly evaluation of literature already published on the subject. Considerable space is devoted to bubble column reactor performance predictions based on mathematical models and the importance of each is explained with practical examples.
Download or read book Hydrodynamics and Mass Transfer in Bubble Columns at Elevated Pressures written by Hugo Martijn Letzel and published by . This book was released on 1998 with total page 136 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Novel Techniques for Slurry Bubble Column Hydrodynamics Annual Technical Progress Report No 1 July 1 1995 June 30 1996 written by and published by . This book was released on 1997 with total page 78 pages. Available in PDF, EPUB and Kindle. Book excerpt: The objective of this cooperative research effort between Washington University, Ohio State University and Exxon Research and Engineering Company is to improve the basis for scale-up and operation of slurry bubble column reactors for syngas conversion and other coal conversion processes by increased reliance on experimentally verified hydrodynamic models. The first year of this three year program was spent on developing and tuning the experimental tools that can provide accurate measurement of pertinent hydrodynamic quantities, such as velocity field and holdup distribution, for validation of hydrodynamic models. Advances made in preparing the unique Computer Automated Radioactive Particle Tracing (CARPT) technique for use in high pressure systems are described in this report The work done on developing a reliable beat transfer coefficient measurement probe at operating conditions of interest is also described. Finally, the work done in preparing the Exxon pilot plant facilities for high pressure runs and pertinent hydrodynamic measurements is outlined together with preliminary studies of matching the fluid dynamics program predictions and data in a two dimensional column.
Download or read book Modelling of Hydrodynamics in Heterogeneous Bubble Column written by Mohd Shahimie Selamat and published by . This book was released on 2010 with total page 42 pages. Available in PDF, EPUB and Kindle. Book excerpt: The applications of bubble columns are very important as multiphase contactors and reactors in process industry. They are wide and extensively used in chemical, petrochemical and biochemical industries. The advantages of bubble column are low maintenance and operating cost due to the compactness and no moving part. They also have an excellent mass and heat transfer characteristic or high heat and mass transfer coefficients, and high durability of catalyst or packing material. It is important to understand the nature of hydrodynamics and operational parameters to characterize their operation including pressure drop, gas superficial velocity, bubble rise velocity, etc., to do the design and scale-up process. Although experimental methods are available to elucidate the multiphase flow in bubble column by the means of advanced experimental methods i.e. X-ray tomography and laser doppler anemometry, the experimental setup is often expensive to develop. Alternatively, the computational fluid dynamics can be used to evaluate the performance of bubble column at lower cost compared to experimental setup. In this work commercial CFD software, FLUENT 6.3 was employed for modeling of gasliquid flow in a bubble column. Multiphase simulations were performed using an Eulerian-Eulerian two-fluid model and the drag coefficient of spherical and distorted bubbles was modeled using the Tomiyama (1995) and Schiller-Naumann (1935) models. The effect of the void fractions on the drag coefficient was modeled using the correlation by Behzadi (2004). The CFD predictions were compared to the experimental measurement adopted from literature. The CFD predicts the turbulent kinetic energy, gas hold-up and the liquid axial velocity fairly well, although the results seem to suggest that further improvement on the interfacial exchange models and possibly further refinement on the two-fluid modeling approaches are necessary especially for the liquid axial velocity and turbulent kinetic energy. It is clear from the modeling exercise performed in this work that CFD is a great method for modeling the performance of bubble column. Furthermore, the CFD method is certainly less expensive than the experimental characterization studies.
