Download or read book High temperature X ray diffraction written by Uel S. Clanton and published by . This book was released on 1960 with total page 118 pages. Available in PDF, EPUB and Kindle. Book excerpt: A high-temperature x-ray diffraction furnace for use with the General Electric Model XRD-3 x-ray diffraction unit has been developed. The furnace, which was designed and constructed by the author, has an angular range of 0-165° 20. A constant temperature or continuously increasing temperature may be programmed through the temperature range of 20°C to 1000°C. Data on the high-temperature modifications of illite obtained with the high-temperature x-ray diffraction furnace indicate a contraction of the (110) spacing at 300°C and expansions at 725°C and 880°C which were not identifiable using the quench method. The existence of interlayer water in the illite structure to temperatures over 800°C is indicated, based upon the continuous decrease of the (002) basal periodicity with increasing temperature. A skeleton illite structure or a high-temperature illite phase with a d-spacing of 9.87A survives the third endothermic reaction observed by differential thermal analysis and forms a phase which is stable at 900°C.
Download or read book X ray Diffraction at Elevated Temperatures written by Deborah D. L. Chung and published by Wiley-VCH. This book was released on 1993 with total page 288 pages. Available in PDF, EPUB and Kindle. Book excerpt: A textbook for a graduate or undergraduate course in programs such as x-ray diffraction, materials characterization, and thermal analysis. Introduces the principles and instrumentation of x-ray diffraction at elevated temperatures, and its application to crystallography, materials science, chemical and electrical engineering, and other fields. Focusing on intense sources and position-sensitive detectors, describes in-situ phase identification, texture analysis, and grain-size measurement. Annotation copyright by Book News, Inc., Portland, OR
Download or read book High temperature X ray Diffraction Techniques written by H. J. Goldschmidt and published by . This book was released on 1964 with total page 32 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book The Application of High Temperature X ray Diffraction to the Interpretation of the X ray Diffraction Pattern of Mullite and the Thermal Expansion of Mullite and Mullite Solid Solutions written by Thomas Gordon Godfrey and published by . This book was released on 1963 with total page 142 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Thermal Expansion written by Yeram Sarkis Touloukian and published by . This book was released on 1975 with total page 0 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book X Ray Diffraction Crystallography written by Yoshio Waseda and published by Springer Science & Business Media. This book was released on 2011-03-18 with total page 320 pages. Available in PDF, EPUB and Kindle. Book excerpt: X-ray diffraction crystallography for powder samples is a well-established and widely used method. It is applied to materials characterization to reveal the atomic scale structure of various substances in a variety of states. The book deals with fundamental properties of X-rays, geometry analysis of crystals, X-ray scattering and diffraction in polycrystalline samples and its application to the determination of the crystal structure. The reciprocal lattice and integrated diffraction intensity from crystals and symmetry analysis of crystals are explained. To learn the method of X-ray diffraction crystallography well and to be able to cope with the given subject, a certain number of exercises is presented in the book to calculate specific values for typical examples. This is particularly important for beginners in X-ray diffraction crystallography. One aim of this book is to offer guidance to solving the problems of 90 typical substances. For further convenience, 100 supplementary exercises are also provided with solutions. Some essential points with basic equations are summarized in each chapter, together with some relevant physical constants and the atomic scattering factors of the elements.
Download or read book Advances in X Ray Analysis written by Charles Barrett and published by Springer. This book was released on 1971-01-01 with total page 574 pages. Available in PDF, EPUB and Kindle. Book excerpt: The application of solid-state detectors of high energy resolution to x-ray spectrometry, and the increasing use of compu ters in both measurement and data evaluation, are giving a new stimulus to x-ray techniques in analytical chemistry. The Twentieth Annual Denver X-ray Conference reflects this renewed interest in several ways. The invited papers, grouped in Session I, review the charac teristics of the detectors used in the measurement of x-rays. One paper is dedicated to the detection of single ions. Although such a subject may appear to be marginal to the purposes of the Denver Conference, we must recognize the affinity of techniques applied to similar purposes. Ion probe mass spectrometry is dedicated to tasks similar to those performed by x-ray spectrometry with the electron probe microanalyzer. Scientists and technologists will see these two techniques discussed in the same meetings. The discussion of automation and programming is not limited to the two invited speakers, but extends to papers presented in more than one session. The matter of fluorescence analysis by isotope- and tube-excitation will also be of great interest to those concerned with the practical applications of x-ray techniques. The communications contained in this volume, and the lively discussions which frequently followed the presentation of papers, attest to the vitality of the subjects which are the concern of the Annual Denver X-ray Conference.
Download or read book Thermobalance with Common Use of High temperature X ray Diffraction written by H. Ohtsu and published by . This book was released on 1966 with total page 19 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Low Temperature X Ray Diffraction written by Reuben Rudman and published by Springer. This book was released on 1976-12 with total page 370 pages. Available in PDF, EPUB and Kindle. Book excerpt: Low-temperature X-ray diffraction (LTXRD) investigations offer many challenges to the diffractionist, not all of which are technical or scientific in nature. LTXRD studies can be frustrating: There are at least two reports of investigations ruined by the loss of crystals (grown with extreme difficulty) because of the widespread power failure and blackout in the northeastern United States in late 1965. LTXRD studies can cause discomfort: In several instances, "low temperatures" have been attained by opening all the windows in the X-ray laboratory. LTXRD studies can be dangerous: It was once reported that a crys tal was lost because a laboratory assistant fell down a flight of stairs and lay unconscious for about an hour on his way to refilling a liquid-nitrogen (LN2 ) dewar. This last report indicated the disposition of the crystal but not that of the laboratory assistant. However, in general, the results of low-temperature X-ray diffraction investigations cannot be obtained in any other manner, and one is well compensated for the effort expended in constructing and maintaining a low-temperature system. Crystal-structure analyses of solidified liquids and gases, phase transformation investigations, accurate crystal-structure analy ses and electron-density maps, thermal expansion measurements, and defect structure studies are a few of the many important applications of LTXRD.
Download or read book Electro Chemo Mechanics of Solids written by Sean R. Bishop and published by Springer. This book was released on 2017-03-18 with total page 197 pages. Available in PDF, EPUB and Kindle. Book excerpt: This book brings together a collection of chapters that focus on the relationship among electrical, chemical, and mechanical properties and the study of adjusting one property through the control of another, namely, Electro-Chemo-Mechanics (ECM). The authors examine how this relationship can result in beneficial properties, such as mixed ionic and electronic conductivity, in oxides, upon oxygen deficiency or lithium insertion (electro-chemo) and/or changes in ionic and electronic mobility observed in strained systems (electro-mechano). They also consider how ECM interactions can be responsible for large stresses from non-stoichiometry induced lattice dilation (chemo-mechano). While many volumes are available devoted to the study of the origins and characteristics of electro-chemical relationships, they form the well-known field of electrochemistry, this volume is highly novel in its examination of the corresponding electro-mechanical, chemo-mechanical, and electro-chemo-mechanical relationships. The book is ideal for researchers and design engineers interested in energy storage and conversion and the electrical and mechanical properties of materials.
Download or read book Platinum Expansion Values for Thermal Calibration of High temperature X ray Diffraction Cameras and Diffractometers written by William Joseph Campbell and published by . This book was released on 1962 with total page 18 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Elements of X Ray Diffraction written by Bernard D. Cullity and published by Pearson. This book was released on 2013-11-01 with total page 656 pages. Available in PDF, EPUB and Kindle. Book excerpt: Designed for Junior/Senior undergraduate courses. This revision of a classical text is intended to acquaint the reader, who has no prior knowledge of the subject, with the theory of x-ray diffraction, the experimental methods involved, and the main applications. The text is a collection of principles and methods designed directly for the student and not a reference tool for the advanced reader
Download or read book Theory of XRF getting acquainted with the principles written by Peter Brouwer and published by . This book was released on 2006 with total page 71 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Bibliography written by International Union of Crystallography. Commission on Crystallographic Apparatus and published by . This book was released on 1964 with total page 22 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book High Temperature Furnaces for X ray Diffractometers written by William Joseph Campbell and published by . This book was released on 1961 with total page 38 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book X ray Characterization of Materials written by Eric Lifshin and published by John Wiley & Sons. This book was released on 2008-07-11 with total page 277 pages. Available in PDF, EPUB and Kindle. Book excerpt: Linking of materials properties with microstructures is a fundamental theme in materials science, for which a detailed knowledge of the modern characterization techniques is essential. Since modern materials such as high-temperature alloys, engineering thermoplastics and multilayer semiconductor films have many elemental constituents distributed in more than one phase, characterization is essential to the systematic development of such new materials and understanding how they behave in practical applications. X-ray techniques play a major role in providing information on the elemental composition and crystal and grain structures of all types of materials. The challenge to the materials characterization expert is to understand how specific instruments and analytical techniques can provide detailed information about what makes each material unique. The challenge to the materials scientist, chemist, or engineer is to know what information is needed to fully characterize each material and how to use this information to explain its behavior, develop new and improved properties, reduce costs, or ensure compliance with regulatory requirements. This comprehensive handbook presents all the necessary background to understand the applications of X-ray analysis to materials characterization with particular attention to the modern approach to these methods.
Download or read book High Temperature and High Pressure Crystal Chemistry written by Robert M. Hazen and published by Walter de Gruyter GmbH & Co KG. This book was released on 2018-12-17 with total page 604 pages. Available in PDF, EPUB and Kindle. Book excerpt: Volume 41 of Reviews in Mineralogy and Geochemistry introduces to the field of high-temperature and high-pressure crystal chemistry, both as a guide to the dramatically improved techniques and as a summary of the voluminous crystal chemical literature on minerals at high temperature and pressure. The three parts of the book introduces crystal chemical considerations of special relevance to non-ambient crystallographic studies, reviews the temperature- and pressure-variation of structures in major mineral groups and presents experimental techniques for high-temperature and high-pressure studies of single crystals and polycrystalline samples as well as special considerations relating to diffractometry on samples at non-ambient conditions.
