Download or read book High Pressure Organic Synthesis written by Davor Margetic and published by Walter de Gruyter GmbH & Co KG. This book was released on 2019-07-08 with total page 326 pages. Available in PDF, EPUB and Kindle. Book excerpt: High pressure chemistry is a widely used methodology in organic synthesis which helps to increase the rate and to improve the efficiency of chemical processes. The current publication outlines the impact of pressure on many types of chemical reactions important from synthetic point of view and gives practical considerations how to plan and perform synthetic experiments under high pressure in the lab.

Download or read book High Pressure Chemical Synthesis written by Janusz Jurczak and published by Elsevier Publishing Company. This book was released on 1989 with total page 528 pages. Available in PDF, EPUB and Kindle. Book excerpt: The high pressure method of chemical synthesis is one of the most developed, unconventional tools for preparation of either new or known compounds and as a result there are a large number of interesting reviews in this field of chemistry. Developments in high-pressure inorganic and organic chemistry have been especially numerous and have been the subject of two earlier books Organic High Pressure Chemistry (W. le Noble, Elsevier, 1988) and Inorganic High Pressure Chemistry (R. van Eldik, Elsevier, 1986). This book, intended as a companion volume, highlights the specific problems of chemical synthesis. It has been written to increase the awareness of practising chemists of techniques which could prove advantageous, and to provide a useful summary of information to those engaged in high-pressure research.

Download or read book High Pressure Organic Synthesis written by Davor Margetic and published by Walter de Gruyter GmbH & Co KG. This book was released on 2019-07-08 with total page 265 pages. Available in PDF, EPUB and Kindle. Book excerpt: High pressure chemistry is a widely used methodology in organic synthesis which helps to increase the rate and to improve the efficiency of chemical processes. The current publication outlines the impact of pressure on many types of chemical reactions important from synthetic point of view and gives practical considerations how to plan and perform synthetic experiments under high pressure in the lab.

Download or read book High Pressure Technology written by Spain and published by Routledge. This book was released on 2017-11-22 with total page 560 pages. Available in PDF, EPUB and Kindle. Book excerpt: High pressure technology is used so extensively that it is almost impossible to catalogue the manyways in which our lives are enhanced by it. From pneumatic tires and household water supplies tomaterials such as crystals, plastics, and even synthetic diamond, there are countless materialsfabricated or shaped using high pressure technology. High Pressure Technology (in two volumes)presents the most up-to-date information available on the main features of this broad technology andthe processes which utilize it.Volume I: Equipment Design, Materials, and Properties covers three broad areas: the general operationof high pressure systems, including standard operating procedures and safety codes and measures;the technology of high pressure systems, such as components, vessel design, and materials of construction;and applied science at high pressure, including the properties of fluids and solids andmechanical properties. Volume II: Applications and Processes covers processes at high pressure andencompasses such topics as: catalytic chemical synthesis; polymerization; phase changes; criticalphenomena; liquefaction of gases; synthesis of single-crystal materials, diamond, and superhardmaterials; isostatic compacting; isostatic hot-pressing; hydrostatic forming of metals; hydraulic cutting;and applications of shock techniques.Written by recognized authorities in industry, government laboratories, and universities, High PressureTechnology is essential reading for the industrial practitioner, high pressure engineer, and researchscientist. In addition, it is a valuable textbook for students in mechanical, chemical, and materialsengineering courses.

Download or read book Industrial High Pressure Applications written by Rudolf Eggers and published by John Wiley & Sons. This book was released on 2012-07-11 with total page 408 pages. Available in PDF, EPUB and Kindle. Book excerpt: Industrial high pressure processes open the door to many reactions that are not possible under 'normal' conditions. These are to be found in such different areas as polymerization, catalytic reactions, separations, oil and gas recovery, food processing, biocatalysis and more. The most famous high pressure process is the so-called Haber-Bosch process used for fertilizers and which was awarded a Nobel prize. Following an introduction on historical development, the current state, and future trends, this timely and comprehensive publication goes on to describe different industrial processes, including methanol and other catalytic syntheses, polymerization and renewable energy processes, before covering safety and equipment issues. With its excellent choice of industrial contributions, this handbook offers high quality information not found elsewhere, making it invaluable reading for a broad and interdisciplinary audience.

Download or read book Activation Methods written by Jean-Philippe Goddard and published by John Wiley & Sons. This book was released on 2020-02-26 with total page 166 pages. Available in PDF, EPUB and Kindle. Book excerpt: Activation Methods examines recent improvements in the utilization of ultrasonic waves and pressurized gases to generate reactions. A straightforward method to use, sonochemistry allows chemical reactions to be carried out under ultrasound without the need for external heat, reagents or catalysts – leading to high yields and the production of a minimum amount of waste. This book presents an overview of the main applications of sonochemistry in green organic chemistry, with an emphasis on texts published within the last few years. High-pressure chemical reactions offer innovative solutions to problems relating to synthesis. They allow access to new products and a further understanding of reaction mechanisms. This book presents the characteristics of hyperbaric activation, which allow the integration of an arsenal of tools for green chemistry, such as the lowering of energy costs and of by-products, as well as the possibility of using substrates that are sterically congested and generally inert.

Download or read book Modern Inorganic Synthetic Chemistry written by Ruren Xu and published by Elsevier. This book was released on 2017-02-11 with total page 808 pages. Available in PDF, EPUB and Kindle. Book excerpt: Modern Inorganic Synthetic Chemistry, Second Edition captures, in five distinct sections, the latest advancements in inorganic synthetic chemistry, providing materials chemists, chemical engineers, and materials scientists with a valuable reference source to help them advance their research efforts and achieve breakthroughs. Section one includes six chapters centering on synthetic chemistry under specific conditions, such as high-temperature, low-temperature and cryogenic, hydrothermal and solvothermal, high-pressure, photochemical and fusion conditions. Section two focuses on the synthesis and related chemistry problems of highly distinct categories of inorganic compounds, including superheavy elements, coordination compounds and coordination polymers, cluster compounds, organometallic compounds, inorganic polymers, and nonstoichiometric compounds. Section three elaborates on the synthetic chemistry of five important classes of inorganic functional materials, namely, ordered porous materials, carbon materials, advanced ceramic materials, host-guest materials, and hierarchically structured materials. Section four consists of four chapters where the synthesis of functional inorganic aggregates is discussed, giving special attention to the growth of single crystals, assembly of nanomaterials, and preparation of amorphous materials and membranes. The new edition’s biggest highlight is Section five where the frontier in inorganic synthetic chemistry is reviewed by focusing on biomimetic synthesis and rationally designed synthesis. Focuses on the chemistry of inorganic synthesis, assembly, and organization of wide-ranging inorganic systems Covers all major methodologies of inorganic synthesis Provides state-of-the-art synthetic methods Includes real examples in the organization of complex inorganic functional materials Contains more than 4000 references that are all highly reflective of the latest advancement in inorganic synthetic chemistry Presents a comprehensive coverage of the key issues involved in modern inorganic synthetic chemistry as written by experts in the field

Download or read book High Pressure Chemistry written by Rudi van Eldik and published by John Wiley & Sons. This book was released on 2008-07-11 with total page 474 pages. Available in PDF, EPUB and Kindle. Book excerpt: It is a basic law of chemistry that pressure influences reactions. Thus, high-pressure reactions are no longer a rarity in chemistry today, but rather are indispensable tools - whether for innovative syntheses, new products or for explaining reaction mechanisms. The expert editors, Rudi van Eldik and Frank-Gerrit Klärner, provide a comprehensive overview of this fascinating field, ranging from the influence of high pressure on organic and inorganic reactions, via concrete applications in synthesis for metal catalytic and stereoselective processes right up to the use of supercritical liquids. Written by renowned experts, this volume contains a wealth of vital and practical information, for both newcomers to the field as well as experienced high-pressure chemists. Whether in academia or industry, this book belongs on the shelf of every chemist concerned with high-pressure chemistry either now or in the future.

Download or read book High Pressure Technology written by Spain and published by Routledge. This book was released on 2017-11-22 with total page 567 pages. Available in PDF, EPUB and Kindle. Book excerpt: High pressure technology is used so extensively that it is almost impossible to catalogue the manyways in which our lives are enhanced by it. From pneumatic tires and household water supplies tomaterials such as crystals, plastics, and even synthetic diamond, there are countless materialsfabricated or shaped using high pressure technology. High Pressure Technology (in two volumes)presents the most up-to-date information available on the main features of this broad technology andthe processes which utilize it.Volume I: Equipment Design, Materials, and Properties covers three broad areas: the general operationof high pressure systems, including standard operating procedures and safety codes and measures;the technology of high pressure systems, such as components, vessel design, and materials of construction;and applied science at high pressure, including the properties of fluids and solids andmechanical properties. Volume II: Applications and Processes covers processes at high pressure andencompasses such topics as: catalytic chemical synthesis; polymerization; phase changes; criticalphenomena; liquefaction of gases; synthesis of single-crystal materials, diamond, and superhardmaterials; isostatic compacting; isostatic hot-pressing; hydrostatic forming of metals; hydraulic cutting;and applications of shock techniques.Written by recognized authorities in industry, government laboratories, and universities, High PressureTechnology is essential reading for the industrial practitioner, high pressure engineer, and researchscientist. In addition, it is a valuable textbook for students in mechanical, chemical, and materialsengineering courses.

Download or read book Beyond the Molecular Frontier written by National Research Council and published by National Academies Press. This book was released on 2003-03-19 with total page 238 pages. Available in PDF, EPUB and Kindle. Book excerpt: Chemistry and chemical engineering have changed significantly in the last decade. They have broadened their scopeâ€"into biology, nanotechnology, materials science, computation, and advanced methods of process systems engineering and controlâ€"so much that the programs in most chemistry and chemical engineering departments now barely resemble the classical notion of chemistry. Beyond the Molecular Frontier brings together research, discovery, and invention across the entire spectrum of the chemical sciencesâ€"from fundamental, molecular-level chemistry to large-scale chemical processing technology. This reflects the way the field has evolved, the synergy at universities between research and education in chemistry and chemical engineering, and the way chemists and chemical engineers work together in industry. The astonishing developments in science and engineering during the 20th century have made it possible to dream of new goals that might previously have been considered unthinkable. This book identifies the key opportunities and challenges for the chemical sciences, from basic research to societal needs and from terrorism defense to environmental protection, and it looks at the ways in which chemists and chemical engineers can work together to contribute to an improved future.

Download or read book Chemical Synthesis Using Supercritical Fluids written by Philip G. Jessop and published by John Wiley & Sons. This book was released on 2008-07-11 with total page 500 pages. Available in PDF, EPUB and Kindle. Book excerpt: For 'better solutions' - this practical guide describes how to take advantage of supercritical fluids in chemical synthesis. Well-established in extractions and materials processing, supercritical fluids are becoming increasingly popular as media for modern chemical syntheses. Historically, the application of compressed gases has been restricted mainly to the production of bulk chemicals. In the last decade, however, research has turned to exploiting the unique properties of supercritical fluids for the synthesis of fine chemicals and specialized materials. Now that the necessary equipment is more readily available, the use of supercritical fluids should become more widespread in both laboratory and industrial scale syntheses. More than merely a concise introduction to the properties of supercritical fluids, here leading experts give a thorough, up-to-date account of chemistry in these alternative media. In-depth scientific commentary, detailed reaction protocols, descriptions of necessary equipment, and an outline of spectroscopic techniques add to the value of this handbook aimed at innovative synthetic chemists.

Download or read book Analysis Synthesis and Design of Chemical Processes written by Richard Turton and published by Pearson Education. This book was released on 2008-12-24 with total page 1562 pages. Available in PDF, EPUB and Kindle. Book excerpt: The Leading Integrated Chemical Process Design Guide: Now with New Problems, New Projects, and More More than ever, effective design is the focal point of sound chemical engineering. Analysis, Synthesis, and Design of Chemical Processes, Third Edition, presents design as a creative process that integrates both the big picture and the small details–and knows which to stress when, and why. Realistic from start to finish, this book moves readers beyond classroom exercises into open-ended, real-world process problem solving. The authors introduce integrated techniques for every facet of the discipline, from finance to operations, new plant design to existing process optimization. This fully updated Third Edition presents entirely new problems at the end of every chapter. It also adds extensive coverage of batch process design, including realistic examples of equipment sizing for batch sequencing; batch scheduling for multi-product plants; improving production via intermediate storage and parallel equipment; and new optimization techniques specifically for batch processes. Coverage includes Conceptualizing and analyzing chemical processes: flow diagrams, tracing, process conditions, and more Chemical process economics: analyzing capital and manufacturing costs, and predicting or assessing profitability Synthesizing and optimizing chemical processing: experience-based principles, BFD/PFD, simulations, and more Analyzing process performance via I/O models, performance curves, and other tools Process troubleshooting and “debottlenecking” Chemical engineering design and society: ethics, professionalism, health, safety, and new “green engineering” techniques Participating successfully in chemical engineering design teams Analysis, Synthesis, and Design of Chemical Processes, Third Edition, draws on nearly 35 years of innovative chemical engineering instruction at West Virginia University. It includes suggested curricula for both single-semester and year-long design courses; case studies and design projects with practical applications; and appendixes with current equipment cost data and preliminary design information for eleven chemical processes–including seven brand new to this edition.

Download or read book High Pressure Techniques in Chemistry and Physics written by Wilfried B. Holzapfel and published by Oxford University Press on Demand. This book was released on 1997 with total page 388 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume provides a practical introduction to the use of high-pressure techniques in chemistry and physics. The authors provide details of the experimental methods and equipment needed to carry out observations and measurements at very high pressures. The pressures involved range from a fewthousand bars for some chemical studies to hundreds of thousands of bars for some physical experimentation.High-pressure techniques may be used to learn more about the structure of matter and mechanisms of chemical reactions. This volume includes detailed descriptions of equipment to measure the following criteria under high pressure conditions: compressibility and equations of state; dielectricconstants and conductance; viscocity; X-ray and neutron diffraction; optical absorption and luminescence; Mossbauer spectra; NMR. IR. and UV spectra; molecular dynamics; kinetics; organic and inorganic synthesis; electro-chemistry and electrophoresis. Applications such as the preservation of foodare also discussed.High-pressure techniques in chemistry and physics: a practical approach is a comprehensive and detailed guide for all those engaged in high-pressure research and a valuable source of information for newcomers to the field. Each chapter contains useful toptics on specific equipment and techniques, aswell as step-by-step protocols, essential background information, and key citations in the literature.

Download or read book High Pressure Chemical Engineering written by P.R. von Rohr and published by Elsevier. This book was released on 1996-09-23 with total page 707 pages. Available in PDF, EPUB and Kindle. Book excerpt: This present volume contains the text of all contributions (oral and posters), except for the four invited papers, which were presented at the 3rd International Symposium on High Pressure Chemical Engineering on October 7-9, 1996. The symposium was divided into three major sections, namely - Chemical reaction engineering - Separation processes and phase equilibria - Plant, apparatus, machinery, measurements, control.

Download or read book Chemistry Under Extreme and Non Classical Conditions written by Rudi van Eldik and published by John Wiley & Sons. This book was released on 1996-12-06 with total page 586 pages. Available in PDF, EPUB and Kindle. Book excerpt: The very best and latest advances compiled in a single volume-an ideal resource for graduate students and researchers . . . Here is the perfect introduction to chemistry under extreme or non-classical conditions, including use of high temperature species, high pressure, supercritical media, sonochemistry, and microwave chemistry. Written by leading experts in their respective fields, this unique text applies a unified approach to each method, including background, instrumentation, examples, information on industrial applications (where relevant), and sources for further reading. Featured topics: * Chemical Synthesis Using High Temperature Species * Effect of Pressure on Inorganic Reactions * Effect of Pressure on Organic Reactions * Organic Synthesis at High Pressure * Inorganic and Related Chemical Reactions in Supercritical Fluids * Organic Chemistry in Supercritical Fluids * Industrial and Environmental Applications of Supercritical Fluids * Ultrasound as a New Tool for Synthetic Chemists * Applications of High Intensity Ultrasound in Polymer Chemistry * Chemistry Under Extreme Conditions in Water Induced Electrohydraulic Cavitation and Pulsed-Plasma Discharges * Microwave Dielectric Heating Effects in Chemical Synthesis * Biomolecules Under Extreme Conditions

Download or read book High Pressure Crystallography written by Andrzej Katrusiak and published by Springer Science & Business Media. This book was released on 2004-03-31 with total page 574 pages. Available in PDF, EPUB and Kindle. Book excerpt: Despite the tremendous advances in the techniques and equipment for carrying out high-pressure crystallography, the application or exploration of the high-pressure variable in detailed structural studies remains rare. The chapters in this book provide a set of lecture notes and supplementary material for a course on high pressure crystallography. The material comprises state-of-the-art reviews of high-pressure experiments using X-ray and neutron diffraction techniques at synchrotron and neutron facilities and in the laboratory, as well as complementary experimental high-pressure techniques and theoretical methods for investigating matter at elevated pressures. The materials studies range from elemental solids and liquids to inorganic compounds, minerals, organic compounds, clathrates and pharmaceutical compounds, to large biological molecules such as proteins and viruses. The book provides a reference for workers in high-pressure science wishing to learn more about crystallography and for established crystallographers potentially interested in high pressure as a variable, as well as an introductory guide to new researchers in the field.

Download or read book Solids Under High Pressure Shock Compression written by R.A. Graham and published by Springer Science & Business Media. This book was released on 2012-12-06 with total page 224 pages. Available in PDF, EPUB and Kindle. Book excerpt: Since the 1950s shock compression research contributed greatly to scientific knowledge and industrial technology. As a result, for example, our understanding of meteorite impacts has substantially improved, and shock processes have become standard industrial methods in materials synthesis and processing. Investigations of shock-compressed matter involve physics,electrical engineering, solid mechanics, metallurgy, geophysics and materials science. The description of shock-compressed matter presented here, which is derived from physical and chemical observations, differs significantly from the classical descriptions derived from strictly mechanical characteristics. This volume, with over 900 references, provides an introduction for scientists and engineers interested in the present state of shock compression science.