Download or read book Fourier Transform Nuclear Magnetic Resonance Spectroscopy Applications of Chemical Interest written by Ruth Ross Inners and published by . This book was released on 1979 with total page 640 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Nuclear Magnetic Resonance written by R. K. Harris and published by Royal Society of Chemistry. This book was released on 1974-10 with total page 457 pages. Available in PDF, EPUB and Kindle. Book excerpt: As a spectroscopic method, Nuclear Magnetic Resonance (NMR) has seen spectacular growth over the past two decades, both as a technique and in its applications. Today the applications of NMR span a wide range of scientific disciplines, from physics to biology to medicine. Each volume of Nuclear Magnetic Resonance comprises a combination of annual and biennial reports which together provide comprehensive of the literature on this topic. This Specialist Periodical Report reflects the growing volume of published work involving NMR techniques and applications, in particular NMR of natural macromolecules which is covered in two reports: "NMR of Proteins and Acids" and "NMR of Carbohydrates, Lipids and Membranes". For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage. Seasoned practitioners of NMR will find this an in valuable source of current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading authorities in the relevant subject areas, the series creates a unique service for the active research chemist, with regular, in-depth accounts of progress in particular fields of chemistry. Subject coverage within different volumes of a given title is similar and publication is on an annual or biennial basis.
Download or read book Fourier Transform N M R Spectroscopy written by Derek Shaw and published by Elsevier Publishing Company. This book was released on 1984 with total page 364 pages. Available in PDF, EPUB and Kindle. Book excerpt: Now reprinted and available in paperback, this book is a comprehensive guide to the theory and practice of NMR spectroscopy in its many forms. It presents the whole range of Fourier Transform NMR techniques, including 2D NMR and NMR imaging. The first three chapters cover the basic physics of magnetic resonance and the mathematical background to Fourier techniques. The following chapters concentrate on pulsed NMR spectroscopy, including the new multipulse sequences, from a theoretical and practical approach. The final chapters deal with the important topic of nuclear relaxation and the novel technique of 2D NMR. The principles of NMR imaging are discussed in detail including medical applications. Containing a wealth of information on techniques and methods, the book provides the reader with a sound base from which to apply Fourier NMR techniques to the many areas of science where they are proving of most value. It is a must for undergraduate and postgraduate students in chemistry and physics, medical students involved in imaging and radiology, NMR spectrometer and NMR imaging manufacturers, and NMR research scientists.
Download or read book Nuclear Magnetic Resonance Spectroscopy written by Robin Kingsley Harris and published by Prentice Hall. This book was released on 1986 with total page 288 pages. Available in PDF, EPUB and Kindle. Book excerpt: Nuclear Magnetic Resonance Spectroscopy explains the NMR phenomenon from the point of view of a physical chemist interested in both fundamental principles and chemical applications. This rigorous but lucid text is highlighted by a large number of figures including illustrative spectra. Problems - with answers where appropriate - are also included. Table of contents: 1: The fundamentals; 2: Analysis of NMR spectra for isotropic solutions; 3: Relaxation and Fourier transform NMR; 4: Dipolar interactions and double resonance; 5: Chemical exchange and quadrupolar effects; 6: NMR of the solid state; 7: Special pulse sequences and two-dimensional NMR; 8: Chemical shifts and coupling constants. Appendices. Further reading. Answers to problems. Index.
Download or read book NMR Spectroscopy Data Acquisition written by Christian Schorn and published by John Wiley & Sons. This book was released on 2004-09-03 with total page 392 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume enables the newcomer to become familiar with the basic data acquisition procedures, modular pulse sequence units and complete sequences in NMR spectroscopy.
Download or read book Fourier Transforms in NMR Optical and Mass Spectrometry written by A.G. Marshall and published by Elsevier. This book was released on 2016-02-25 with total page 470 pages. Available in PDF, EPUB and Kindle. Book excerpt: Written by spectroscopists for spectroscopists, here is a book which is not only a valuable handbook and reference work, but also an ideal teaching text for Fourier transform methods as they are applied in spectroscopy. It offers the first unified treatment of the three most popular types of FT/spectroscopy, with uniform notation and complete indexing of specialized terms. All mathematics is self-contained, and requires only a knowledge of simple calculus. The main emphasis is on pictures and physical analogs rather than detailed algebra. Instructive problems, presented at the end of each chapter, offer extensions of the basic treatment. Solutions are given or outlined for all problems. The book offers a wealth of practical information to spectroscopists. Non-ideal effects are treated in detail: noise (source- and detector-limited); non-linear response; limits to spectrometer performance based on finite detection period, finite data size, mis-phasing, etc. Common puzzles and paradoxes are explained: e.g. use of mathematically complex variables to represent physically real quantities; interpretation of negative frequency signals; on-resonance vs. off-resonance response; interpolation (when it helps and when it doesn't); ultimate accuracy of the data; differences between linearly- and circularly-polarized radiation; multiplex advantage or disadvantage, etc. Chapter 1 introduces the fundamental line shapes encountered in spectroscopy, from a simple classical mass-on-a-spring model. The Fourier transform relationship between the time-domain response to a sudden impulse and the steady-state frequency-domain response (absorption and dispersion spectra) to a continuous oscillation is established and illustrated. Chapters 2 and 3 summarize the basic mathematics (definitions, formulas, theorems, and examples) for continuous (analog) and discrete (digital) Fourier transforms, and their practical implications. Experimental aspects which are common to the signal (Chapter 4) and noise (Chapter 5) in all forms of Fourier transform spectrometry are followed by separate chapters for treatment of those features which are unique to FT/MS, FT/optical, FT/NMR, and other types of FT/spectroscopy. The list of references includes both historical and comprehensive reviews and monographs, along with articles describing several key developments. The appendices provide instant access to FT integrals and fast algorithms as well as a pictorial library of common Fourier transform function pairs. The comprehensive index is designed to enable the reader to locate particular key words, including those with more than one name.
Download or read book Signal Treatment and Signal Analysis in NMR written by D.N. Rutledge and published by Elsevier. This book was released on 1996-06-10 with total page 567 pages. Available in PDF, EPUB and Kindle. Book excerpt: Signal analysis and signal treatment are integral parts of all types of Nuclear Magnetic Resonance. In the last ten years, much has been achieved in the development of dimensional spectra. At the same time new NMR techniques such as NMR Imaging and multidimensional spectroscopy have appeared, requiring entirely new methods of signal analysis. Up until now, most NMR texts and reference books limited their presentation of signal processing to a short introduction to the principles of the Fourier Transform, signal convolution, apodisation and noise reduction. To understand the mathematics of the newer signal processing techniques, it was necessary to go back to the primary references in NMR, chemometrics and mathematics journals. The objective of this book is to fill this void by presenting, in a single volume, both the theory and applications of most of these new techniques to Time-Domain, Frequency-Domain and Space-Domain NMR signals. Details are provided on many of the algorithms used and a companion CD-ROM is also included which contains some of the computer programs, either as source code or in executable form. Although it is aimed primarily at NMR users in the medical, industrial and academic fields, it should also interest chemometricians and programmers working with other techniques.
Download or read book Pulse Nuclear Magnetic Resonance Spectroscopy written by Thomas Charles Farrar and published by . This book was released on 1989 with total page 236 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Fourier Hadamard and Hilbert Transforms in Chemistry written by Alan Marshall and published by Springer Science & Business Media. This book was released on 2013-06-29 with total page 564 pages. Available in PDF, EPUB and Kindle. Book excerpt: In virtually all types of experiments in which a response is analyzed as a function of frequency (e. g. , a spectrum), transform techniques can significantly improve data acquisition and/or data reduct ion. Research-level nuclear magnet ic resonance and infra-red spectra are already obtained almost exclusively by Fourier transform methods, because Fourier transform NMR and IR spectrometers have been commercially available since the late 1960·s. Similar transform techniques are equally valuable (but less well-known) for a wide range of other chemical applications for which commercial instruments are only now becoming available: for example, the first corrmercial Fourier transform mass spectrometer was introduced this year (1981) by Nicolet Instrument Corporation. The purpose of this volume is to acquaint practicing chemists with the basis, advantages, and applica of Fourier, Hadamard, and Hilbert transforms in chemistry. For tions almost all chapters, the author is the investigator who was the first to apply such methods in that field. The basis and advantages of transform techniques are described in Chapter 1. Many of these aspects were understood and first applied by infrared astronomers in the 1950·s, in order to improve the otherwise unacceptably poor signal-to-noise ratio of their spec tra. However, the computations required to reduce the data were painfully slow, and required a 1 arge computer.
Download or read book ABC s of FT NMR written by John D. Roberts and published by University Science Books. This book was released on 2000 with total page 342 pages. Available in PDF, EPUB and Kindle. Book excerpt: The primary purpose of this book is to help you understand what is going on in Fourier Transform (FT) Nuclear Magnetic Resonance (NMR) spectroscopy. Modern life is now very largely life with 'black boxes' that carry warning labels: 'No user-serviceable parts inside.' Many find black boxes to be quite acceptable, at least as long as they work. But how willing should we be to accept black-box analyses without some understanding of how those analyses were obtained? NMR spectrometers are like 'black boxes' in that they offer many standardised procedures, but it can be dangerous to the quality of your data if you rely slavishly on such procedures without understanding how and why the proper parameter choices are critical. The scope of this book is broad rather than deep with the intention of providing helpful insight. Much can be understood in a more qualitative way and that is the approach taken here. For those few areas where a quantitative approach is needed, simple mathematics will usually suffice.
Download or read book Fourier Transform NMR Techniques written by K. Müllen and published by . This book was released on 1976 with total page 170 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book NMR for Liquid Fossil Fuels written by L. Petrakis and published by Elsevier. This book was released on 2012-12-02 with total page 253 pages. Available in PDF, EPUB and Kindle. Book excerpt: High resolution nuclear magnetic resonance (NMR) of liquid fuels has provided valuable information on the molecular structures present in these fuels. The chemical insight gained through NMR studies has the potential to enhance significantly the development of processes for the utilization of fossil energy. For this potential to be fully realized, users of NMR information must be able to communicate effectively with NMR experts. Conversely, NMR experts must understand the type of information that users will attempt to derive from their spectra. The goal of this book is to strengthen the lines of communication between NMR experts and users in the area of NMR of liquid fuels.The book comprises two parts. The first part presents elements of relevant NMR phenomenology, including a definition of the most important NMR parameters, an introduction to Fourier transform NMR and a discussion of newer pulse techniques. Sufficient background material is presented to enable the reader to follow such techniques as spin echo, two-dimensional and polarization transfer experiments. These techniques are illustrated by extensive examples derived from fuel chemistry. The second part of the book addresses the interpretation of NMR spectra and is based, to a very large extent, on the work of the authors who have used NMR in a variety of applications in fossil fuels. This part describes in detail the three basic methods for interpreting NMR spectra of liquid fuels: average structural parameter calculations, average molecule construction and functional group analysis. The use of NMR in engineering calculations is also presented and should be particularly useful to those interested in processing of fossil fuels. Extensive examples are drawn from petroleum, shale oils, coal liquids and model systems. Computer programs for performing the characterizations from the spectra are provided.The book will appeal to a wide range of professionals. With its emphasis on applications, it will be of particular interest to those who use NMR to characterize liquid fossil fuels or those who provide NMR assistance to fossil fuel scientists and technologists.
Download or read book Introduction to NMR Spectroscopy written by Raymond John Abraham and published by . This book was released on 1988-11-24 with total page 296 pages. Available in PDF, EPUB and Kindle. Book excerpt: Introduction to NMR Spectroscopy R. J. Abraham, School of Chemistry, University of Liverpool J. Fisher, Biological NMR Centre, University of Leicester P. Loftus, Stuart Pharmaceuticals, Delaware, USA This book is a new, extended edition of Proton and Carbon 13 NMR by R. J. Abraham and P. Loftus. The initial chapters cover the fundamentals of NMR spectroscopy commencing with an explanation of how the nuclear magnetic response occurs, followed by a detailed discussion of chemical shifts and coupling constants, parameters not discussed to any length in other textbooks aimed at a similar level of interest. Emphasis is given to the vectorial description of multipulse experiments, as this is probably the easiest way to grasp how different information may be gained simply by changing a pulse sequence. An understanding of multipulse NMR is a prerequisite for understanding 2D NMR. The section on 2D NMR begins with a discussion of the resolved experiment. This is a logical initial choice as the spectra produced by this experiment may be readily compared with 1D spectra. Following on from this both heteronuclear and homonuclear correlation spectroscopy are described and examples given. The final section of the book should be considered as an applications section. It is aimed at showing the reader that NMR is not just of use to the synthetic organic chemist but is also of use to biochemists for investigating the solution state structure and function of proteins, enzymes, etc. The application of high resolution NMR to the solid state is also discussed, thereby indicating the developments which have taken place as far as spectrometer hardware is concerned.
Download or read book Fourier Transform N M R Spectroscopy written by Derek Shaw and published by Elsevier Science Limited. This book was released on 1987 with total page 344 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Fourier Transform N M R Spectroscopy written by D. Shaw and published by . This book was released on 1984 with total page 355 pages. Available in PDF, EPUB and Kindle. Book excerpt:
Download or read book Transient Techniques in NMR of Solids written by Bernard C. Gerstein and published by . This book was released on 1985 with total page 320 pages. Available in PDF, EPUB and Kindle. Book excerpt: This volume is an ideal starting point for the graduate student seeking a basic introduction to the theory and uses of solid-state nuclear magnetic resonance (NMR) spectroscopy. Accessible to students with only a survey-level physics background, the material assumes little prior knowledge of the basic theory of electromagnetism. All the major areas are covered, including an introduction to concepts of time-dependent quantum mechanics as they apply to NMR spectroscopy of the solid state. Each chapter includes problems designed to enhance the reader's understanding of the material. Instructive and practical, this volume provides the basic knowledge needed to access the general literature and the more advanced monographs on this subject. In addition to assisting entrance into the field, Transient Techniques in NMR of Solids will be a useful guide for professionals already working in related areas of chemistry. FROM THE PREFACE: Nuclear magnetic resonance (NMR) is truly a remarkable phenomenon. Remarkable can imply different things to different people. From the point of view of a physicist, spin dynamics is an elegant example of the use of time-dependent quantum mechanics, and NMR absorption of energy is a prototype for spectroscopic transitions. From the point of view of the practicing chemist and materials scientist, NMR spectroscopy is an invaluable tool for the identification of chemical species and structures. Had NMR spectroscopic techniques commercially available in the early 1960s been the only result of investigations of this phenomenon, it would have had a major impact on the course of chemical analysis. The study of liquids and solutions for chemical shifts and couplings of protons had produced a rapid means of identifying chemical species nondestructively. The study of dynamical properties also could be addressed by study of temperature dependence of the spectra or of the saturation of the resonance by high-power irradiation. Even at that time, however, studies of the spin dynamics had already begun to indicate that there were many interesting facets of the NMR phenomenon left to exploit. For example, the Fourier-transform relationship of the free-induction decay and the absorption spectrum had been shown and the basis of the cross-polarization experiment was being investigated. A number of chemists had begun to study the spin*b1lattice relaxation times of species by pulse NMR techniques by utilizing methods that were not familiar at that time to the typical chemist but that are now commonly employed in NMR analysis. The principal characteristic of the NMR technique that makes it so useful for chemical analysis of liquids and solutions is the high resolution that allows one to observe very small interactions such as the chemical shift and the spin*b1spin coupling. These weak interactions are quite sensitive to the local environment of the spin and therefore may be used as a diagnostic for the environment. The connectivity of chemical structure is often mimicked closely in the NMR connectivity of the spectrum, and quantitative informaton is relatively easy to obtain. Nuclear magnetic resonance spectra of solids exhibit such resolution only in special cases. The primary (although not the exclusive) reason for the lack of resolution in the spectrum of a typical solid is the presence of the dipole*b1dipole interaction, which dominates the NMR spectroscopy of solids that have been of interest to chemists. One solution (no pun intended) to the problem of obtaining chemical-shift information about such solids is to dissolve them and to study them in solution. However, if the solid is insoluble or otherwise intractable or if the analysis involves questions about the properties of the substance in the solid state, then there arises a need for techniques to study the weaker interactions in the presence of the dipole*b1dipole interaction or other overwhelming interactions. This volume describes the means dev
Download or read book Scientific and Technical Aerospace Reports written by and published by . This book was released on 1979 with total page 1096 pages. Available in PDF, EPUB and Kindle. Book excerpt:
